Multifunctional pressure difference type method for testing compatibility of high-pressure hydrogen and materials

A test method and technology of high-pressure hydrogen, applied in the direction of applying stable tension/pressure to test the strength of materials, using repetitive force/pulse force to test the strength of materials, etc., can solve the problems of difficult measurement, signal drift, hydrogen leakage, etc., Achieve the effect of improving reliability and safety, avoiding servo test mechanisms, and reducing the probability of leakage

Active Publication Date: 2015-09-02
ZHEJIANG UNIV
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Problems solved by technology

[0004] (1) The equipment structure is complicated, the cost is high, and the operation is complicated
[0005] Most of the hydrogen compatibility test devices currently developed are based on traditional material testing machines, plus an environment box that can provide a high-pressure hydrogen environment. The samples and their fixtures are contained inside the environment box. Therefore, the internal volume of the environment box Large, coupled with its usually high pressure (up to 100MPa), resulting in expensive equipment
In addition, a large-volume environmental chamber also needs to be equipped with a corresponding hydrogen gas supply system. The operation of the entire equipment is complicated, and the cost of hydrogen and labor is high.
Such as the test device proposed in the patent [201110259252.2], not only the cost of the equipment itself is high, but each test requires multiple people to operate the equipment, and the hydrogen consumption is also large
[0006] (2) The

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  • Multifunctional pressure difference type method for testing compatibility of high-pressure hydrogen and materials
  • Multifunctional pressure difference type method for testing compatibility of high-pressure hydrogen and materials
  • Multifunctional pressure difference type method for testing compatibility of high-pressure hydrogen and materials

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Embodiment Construction

[0054] Below in conjunction with accompanying drawing and specific embodiment the present invention is described in further detail:

[0055] Such as figure 1 The shown multifunctional differential pressure high-pressure hydrogen and material compatibility test device includes a test chamber, a pneumatic booster pump 4, a low-pressure storage tank 2, a high-pressure storage tank 5, a vacuum pump 9, a hydrogen cylinder set 1, an argon gas Bottle set 19 and control system module 17. The test device uses a disc-shaped thin slice as a sample, and can use the pressure difference between the upper and lower surfaces of the disc sample 23 under a high-pressure hydrogen environment (up to 100 MPa) to apply a load to the disc sample 23 for mechanical performance testing.

[0056] Such as figure 2 As shown, the test chamber includes an end cover 11, an upper chamber 12, a lower chamber 13, and a pressure ring 24. The design pressure of the test chamber is 35-100 MPa; the upper chamber...

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Abstract

The invention relates to the field of development of material mechanical property testing devices, and aims at providing a multifunctional pressure difference type method for testing the compatibility of high-pressure hydrogen and materials. The method includes a bursting test method, a variable-hydrogen-pressure fatigue test method and a constant-hydrogen-pressure fatigue test method. By means of the method for applying loads on a disc sample through the pressure difference of the upper surface and the lower surface of the disc sample, complex servo test mechanisms are avoided, the device size is greatly reduced, the device input is reduced, operation is easy and convenient, and the test efficiency is improved; in the test process, parameters such as strain and displacement of the disc sample can be conveniently measured, and corresponding tested elements are not influenced by high-pressure hydrogen.

Description

technical field [0001] The invention relates to the field of development of testing equipment for mechanical properties of materials, in particular to a testing method for compatibility between multifunctional differential pressure high-pressure hydrogen and materials. Background technique [0002] Hydrogen is an important part of the clean utilization of fossil energy and the development of new energy. Hydrogen is usually stored and transported in gaseous form under high pressure. In recent years, due to the development trend of higher pressure of high-pressure hydrogen system and complex service environment, the compatibility problem of materials used in high-pressure hydrogen system and hydrogen (ie hydrogen embrittlement problem) has gradually become prominent. Hydrogen embrittlement will reduce the toughness of the material and increase the crack growth rate, which will cause a sudden and serious failure of the high-pressure hydrogen system during service, causing grea...

Claims

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Application Information

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IPC IPC(8): G01N3/12G01N3/36
Inventor 郑津洋花争立赵永志顾超华刘鹏飞崔天成黄改
Owner ZHEJIANG UNIV
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