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Methods for refining decaffeinated EGCG and for preparing decaffeinated EGCG tea granules

A technology of decaffeination and tea granules, which is applied in tea extraction and tea alkali reduction, can solve the problems of difficulty in extracting and purifying EGCG, lack of competitiveness of products, residual organic solvents, etc., and achieves good market prospects, low cost and high production efficiency. short cycle effect

Inactive Publication Date: 2015-09-09
上海强圣医药科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The common methods of decaffeination are organic solvent method, ion precipitation method, column chromatography and other methods. Most of the processes use organic solvent treatment, which has the disadvantages of organic solvent residue and high cost.
[0004] The supercritical value of carbon dioxide is low, and small changes in pressure and temperature will cause a large change in fluid density, and it can easily penetrate into the tea leaves, so that the extraction components can be fully dissolved through distribution and diffusion, thereby achieving the purpose of extraction; but this method is industrialized. There are still many deficiencies in production, especially the refined EGCG with a purity of more than 90%, it is difficult to achieve the goal through pure carbon dioxide supercritical fluid extraction; secondly, the product cost is too high and the product lacks competitiveness
[0005] Tea contains more polyphenols such as caffeine and catechins, all of which contain more phenolic hydroxyl groups, which pose certain difficulties for the extraction and purification of EGCG

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Example 1 Preparation of Decaffeinated EGCG Tea Granules 1

[0034]Take 100g of decaffeinated EGCG (content 92.2%), add 280g of lactose, 20g of soluble starch, 1g of sucralose, sieve, mix evenly, add an appropriate amount of water, granulate with 20 mesh, and dry at 60°C for 4-5 hours to make the moisture less than 5%, 20 mesh whole grains, decaffeinated EGCG tea granules, 1g per bag, containing 250mg of EGCG.

Embodiment 2

[0035] Example 2 Preparation of decaffeinated EGCG tea granules 2

[0036] Take 50g of decaffeinated EGCG raw material (content 93.1%), add 150g of sucrose, 1g of stevioside, add appropriate amount of water to make EGCG tea granules, granulate at 20 mesh, dry at 60°C for 4-5 hours, make the moisture less than 5%, and make 20 mesh Whole grains, spray appropriate amount of green tea essence to get decaffeinated EGCG tea granules, 1g per bag, containing 250mg of EGCG.

Embodiment 3

[0037] Example 3 Preparation of decaffeinated EGCG tea granules 3

[0038] Get decaffeinated EGCG raw material 50g (content 92.8%), add mannitol 150g, sucralose 0.5g, add 50% sucrose solution high-speed stirring to make EGCG tea granule, 20 order granulation, 60 ℃ dry to 4 hours, make Moisture content is less than 6%, 20 mesh whole grains, to obtain decaffeinated EGCG tea granules, each bag 1g, containing EGCG 250mg.

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PUM

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Abstract

Provided are methods for refining a decaffeinated (-)-epigallocatechin gallate (EGCG for short, similarly hereinafter) effective component and for preparing decaffeinated EGCG tea granules, wherein the methods comprise extracting and refining the decaffeinated EGCG from tea leaves, tea dust or tea tree pruned branches and leaves and preparing the decaffeinated EGCG tea granules from the decaffeinated EGCG and combinative auxiliary materials; the process technology for preparing the decaffeinated EGCG is relatively mature, operations are simple, the cost is relatively low, and the market prospects are promised.

Description

technical field [0001] A refined (-)-epigallocatechin gallate (abbreviated as EGCG, the same below) active ingredient and a method for preparing decaffeinated EGCG tea granules, including extracting refined decaffeinated from tea leaves, tea powder or tea tree pruned branches and leaves EGCG and a method for preparing decaffeinated EGCG tea granules with adjuvants that can be combined. Background technique [0002] People advocate "return to nature" and pursue "natural, safe, nutritious and effective" food, and natural food is increasingly popular. Since caffeine is harmful to special populations such as pregnant women, children, the elderly, heart disease, insomnia, and neurasthenia, low-caffeine or decaffeinated tea drinks can reduce the adverse effects of caffeine on health , to expand the scope of use of the crowd. Therefore, decaffeinated products are more and more accepted by users at home and abroad, and the consumption in developed countries such as Europe and Nort...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23F3/30A23F3/36
Inventor 黎俊汤瑞梅
Owner 上海强圣医药科技有限公司
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