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Novel reverse-osmosis scale inhibitor

A reverse osmosis and antiscalant technology, applied in the field of antiscalants, can solve the problems of low antiscaling performance and uneven product performance, and achieve the effect of long storage period, less dosage and stable properties

Active Publication Date: 2015-09-16
浙江川宁环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the main reverse osmosis antiscalants include the products of Kinglee Company, Argo Company, and FMC Company of the United States, and there are also some domestic products.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] In the embodiment of the present invention, the new reverse osmosis scale inhibitor weighs the following raw materials: 2kg of sodium citrate, 33kg of hydrolyzed polymaleic anhydride, 28kg of polyepoxy succinate, 9kg of urotropine, 13kg of polylactic acid, and 40kg of water .

[0024] Concrete steps during preparation include:

[0025] (1) Feeding: Put sodium citrate, hydrolyzed polymaleic anhydride, polyepoxysuccinate, urotropine and half of the mass of water into the reaction kettle, raise the temperature to 40°C, stir and dissolve evenly;

[0026] (3) Dissolution: dissolve polylactic acid with the remaining water;

[0027] (4) Dropping: Raise the temperature of the materials in the reactor to 70°C, add the polylactic acid solution dropwise, and control the flow rate so that the polylactic acid solution is dripped at the same time, and the dropping time is 5 hours;

[0028] (5) Heat preservation: After the polylactic acid solution is added dropwise, keep heat for 3 ...

Embodiment 2

[0031] In the embodiment of the present invention, the new reverse osmosis antiscalant, weigh the following raw materials: sodium citrate 8kg, hydrolyzed polymaleic anhydride 45kg, polyepoxy succinate 37kg, urotropine 15kg, polylactic acid 20kg, water 50kg .

[0032] Concrete steps during preparation include:

[0033] (1) Feeding: Put sodium citrate, hydrolyzed polymaleic anhydride, polyepoxysuccinate, urotropine and half of the mass of water into the reaction kettle, raise the temperature to 50°C, stir and dissolve evenly;

[0034] (3) Dissolution: dissolve polylactic acid with the remaining water;

[0035] (4) Dropping: Raise the temperature of the materials in the reactor to 75°C, add the polylactic acid solution dropwise, and control the flow rate so that the polylactic acid solution is dripped at the same time, and the dropping time is 6 hours;

[0036] (5) Heat preservation: After the polylactic acid solution is added dropwise, keep heat for 4 hours;

[0037] (6) Cool...

Embodiment 3

[0039] In the embodiment of the present invention, the new reverse osmosis scale inhibitor weighs the following raw materials: 3kg of sodium citrate, 36kg of hydrolyzed polymaleic anhydride, 30kg of polyepoxy succinate, 11kg of urotropine, 15kg of polylactic acid, and 42kg of water .

[0040] Concrete steps during preparation include:

[0041] (1) Feeding: Put sodium citrate, hydrolyzed polymaleic anhydride, polyepoxysuccinate, urotropine and half of the mass of water into the reaction kettle, raise the temperature to 42°C, stir and dissolve evenly;

[0042](3) Dissolution: dissolve polylactic acid with the remaining water;

[0043] (4) Dropping: Raise the temperature of the materials in the reactor to 71°C, add the polylactic acid solution dropwise, and control the flow rate so that the polylactic acid solution is dropped at the same time, and the dropping time is 5.2 hours;

[0044] (5) Heat preservation: After the polylactic acid solution is added dropwise, keep heat for ...

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PUM

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Abstract

The invention discloses a novel reverse-osmosis scale inhibitor which comprises the following raw materials in parts by weight: 2-8 parts of sodium citrate, 33-45 parts of hydrolytic polymaleic anhydride, 28-37 parts of polyepoxysuccinic acid salt, 9-15 parts of urotropine, 13-20 parts of polylactic acid, and 40-50 parts of water. A preparation method comprises the following steps: adding sodium citrate, hydrolytic polymaleic anhydride, polyepoxysuccinic acid salt, urotropine and half of water into a reaction kettle, heating to 40-50 DEG C, and stirring for uniformly dissolving; dissolving polylactic acid with the rest water to obtain a polylactic acid solution; heating the materials in the reaction kettle to 70-75 DEG C, dropwise adding the polylactic acid solution, and keeping the temperature for 3-4h after the dropwise adding is finished; and cooling to room temperature so as to obtain the novel reverse-osmosis scale inhibitor. The novel reverse-osmosis scale inhibitor disclosed by the invention has the scale inhibition rate being up to 95%, is small in adding amount, environmentally friendly, stable in property, and long in storage period, and can be used for solving the problems that existing reverse-osmosis inhibitors mainly are foreign products and are limited in treatment capacity, complex in synthesis, relatively high in production cost, and the like in the prior art.

Description

technical field [0001] The invention relates to a scale inhibitor, in particular to a novel reverse osmosis scale inhibitor. Background technique [0002] With the advancement of membrane science and technology, reverse osmosis water treatment technology has been widely used in electric power, food, electronics, and chemical industries, and has a wide range of applications in the fields of advanced treatment of industrial water supply and sewage reuse. During the long-term operation of reverse osmosis equipment, due to the high concentration of various ions in the concentrated water, it is easy to generate scale and breed bacteria and algae, which will cause membrane blockage and affect the stable operation of the reverse osmosis system. Membrane fouling and the growth of bacteria and algae can reduce the water production rate of equipment and cause energy waste. In severe cases, membrane elements must be replaced. Membrane elements are the main components of reverse osmosis...

Claims

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Application Information

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IPC IPC(8): B01D65/08C02F5/12C02F5/10
Inventor 邵永富
Owner 浙江川宁环保科技有限公司
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