Preparation method of ultrahigh-molecular-weight polyacrylamide
A technology of polyacrylamide and ultra-high molecular weight, which is applied in the field of preparation of ultra-high molecular weight polyacrylamide, can solve the problems that it is difficult to stably prepare ultra-high molecular weight polyacrylamide, and the reaction temperature is difficult to control uniformly, and achieves High yield, stable polymerization reaction temperature and simple process
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Embodiment 1
[0020] A preparation method of ultra-high molecular weight polyacrylamide includes the following steps:
[0021] 1) Prepare an aqueous solution of acrylamide with a mass fraction of 27% and a temperature of 0°C;
[0022] 2) Add the acrylamide aqueous solution prepared in step 1) to a reactor equipped with an in-liquid heat conduction device, such as Figure 1-2 As shown, the in-liquid heat conduction device includes a circular substrate 1, on which a plurality of layers of annular hole arrays concentric with the circular substrate 1 are provided; each hole of the annular hole array is provided with a circular substrate 1 1 Vertical straight water pipe 2; The circular base plate 1 is also provided with a stirrer shaft 3 connected to the stirrer and penetrates the center of the circular base plate 1, and an annular water pipe 4 surrounding the side wall of the circular base plate 1; inside the straight water pipe 2 A partition plate 5 is provided for dividing the straight water pipe...
Embodiment 2
[0030] A preparation method of ultra-high molecular weight polyacrylamide includes the following steps:
[0031] 1) Prepare an aqueous solution of acrylamide with a mass fraction of 28% and a temperature of 2°C;
[0032] 2) Add the acrylamide aqueous solution prepared in step 1 to a reactor equipped with an in-liquid heat conduction device, such as Figure 1-2 As shown, the in-liquid heat conduction device includes a circular substrate 1, on which a plurality of layers of annular hole arrays concentric with the circular substrate 1 are provided; each hole of the annular hole array is provided with a circular substrate 1 1 Vertical straight water pipe 2; The circular base plate 1 is also provided with a stirrer shaft 3 connected to the stirrer and penetrates the center of the circular base plate 1, and an annular water pipe 4 surrounding the side wall of the circular base plate 1; inside the straight water pipe 2 A partition plate 5 is provided for dividing the straight water pipe ...
Embodiment 3
[0040] A preparation method of ultra-high molecular weight polyacrylamide includes the following steps:
[0041] 1) Prepare an aqueous acrylamide solution with a mass fraction of 27% and a temperature of 3°C;
[0042] 2) Add the acrylamide aqueous solution prepared in step 1 to a reactor equipped with an in-liquid heat conduction device, such as Figure 1-2 As shown, the in-liquid heat conduction device includes a circular substrate 1, on which a plurality of layers of annular hole arrays concentric with the circular substrate 1 are provided; each hole of the annular hole array is provided with a circular substrate 1 1 Vertical straight water pipe 2; The circular base plate 1 is also provided with a stirrer shaft 3 connected to the stirrer and penetrates the center of the circular base plate 1, and an annular water pipe 4 surrounding the side wall of the circular base plate 1; inside the straight water pipe 2 A partition plate 5 is provided for dividing the straight water pipe 2 i...
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