Preparation method of novel composite solid gum
A solid glue, a new type of technology, applied in the direction of adhesives, adhesive types, adhesive additives, etc., can solve the problems of heat resistance, application limitations, etc., and achieve the effect of increasing thermal performance, strong reactivity, and good compatibility
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[0017] Example
[0018] According to the ratio in Table 1, the hydroxy acrylic resin and the epoxy resin were reacted at 120° C. for 30 minutes to obtain an epoxy resin prepolymer; the aluminum phosphate was ground and mixed with talc as a filler.
[0019] Table 1 Quality of raw materials
[0020]
[0021] According to the ratio in Table 2, mix the filler, ethylene glycol butyl ether, and silica sol (with a solid content of 45%; the particle size of silicon dioxide is 150-430 nm) for 1 hour to obtain a mixture; sequentially add sodium metaborate and sulfuric acid Add ester dispersant and succinic anhydride to the mixture, stir for 0.5 hours, then add epoxy resin prepolymer, stir at 140°C for 3 hours; finally add polyvinylpyrrolidone and hydrated zinc chloride, stir at 60°C for 8 hours, The compound is obtained; the compound is placed in a mold and cold pressed (0.3MPa; room temperature) to obtain a new composite solid glue.
[0022] Table 2 Quality of raw materials
[0023]
[0024] N...
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