Unlock instant, AI-driven research and patent intelligence for your innovation.

Polyethylene wax coated stable potassium ferrate and preparation method thereof

A technology of polyethylene wax and potassium ferrate, which is applied in the direction of flocculation/sedimentation water/sewage treatment, sterilization/microdynamic water/sewage treatment, etc., can solve problems such as the use method and effect not given, and achieve improved coating The effect of high efficiency and stability, easy operation and simple process

Active Publication Date: 2018-12-14
NANJING UNIV OF SCI & TECH
View PDF4 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

US patents US 20130034594 and US 20130034594 introduced several resin materials such as polyolefin, polyester, polyether, etc. that can be used to coat potassium ferrate, but did not give specific usage methods and effects

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Polyethylene wax coated stable potassium ferrate and preparation method thereof
  • Polyethylene wax coated stable potassium ferrate and preparation method thereof
  • Polyethylene wax coated stable potassium ferrate and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] According to the mass ratio of polyethylene wax and potassium ferrate of 3:1, respectively weigh 30g polyethylene wax and potassium ferrate with a purity of 10g above 95%, first place the polyethylene wax in a beaker, and the polyethylene wax It is a commercially available product with a molecular weight of 2000-3000, a melting point of 90-110°C and a density of 0.95g / cm 3 , the viscosity is 650mPa·s. Put it on a constant temperature heating magnetic stirrer and heat it to 110°C to make it melt completely, keep it in a molten state at a constant temperature of 100°C, add potassium ferrate, stir and disperse at a stirring speed of 600r / min for 40min, and move the beaker to another unheated magnetic stirrer Continue to stir on the mixer until the speed slows down, and then let it cool naturally. After solidification, grind to 170-200 mesh, and dry in a vacuum oven at 40°C for 2 hours to obtain polyethylene wax-coated stable potassium ferrate. Determination of the coatin...

Embodiment 2

[0025] According to the mass ratio of polyethylene wax and potassium ferrate of 5:1, weigh 50g polyethylene wax and potassium ferrate of 10g purity more than 95% respectively, repeat the preparation method of Example 1, measure the coating of this finished product Rate, 10-day water absorption rate and release data in water are listed in Table 1, and the scanning electron micrograph is shown in figure 2 , the results of infrared absorption spectroscopy are shown in image 3 shown. The release curve of the finished product in water is shown in Figure 4 Shown, its sustained-release kinetic equation and related data are shown in Table 2.

Embodiment 3

[0027] According to the mass ratio of polyethylene wax and potassium ferrate of 8:1, take by weighing 80g polyethylene wax and potassium ferrate of 10g purity more than 95% respectively, repeat the preparation method of Example 1, measure the coating of this finished product Rate, 10-day water absorption rate and release data in water are listed in Table 1, and the scanning electron micrograph is shown in figure 2 shown. The release curve of the finished product in water is shown in Figure 4 Shown, its sustained-release kinetic equation and related data are shown in Table 2.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
melting pointaaaaaaaaaa
densityaaaaaaaaaa
viscosityaaaaaaaaaa
Login to View More

Abstract

The invention discloses a polyethylene wax coated stable potassium ferrate and a preparation method thereof. The polyethylene wax coated stable potassium ferrate is composed of potassium ferrate and polyethylene wax. The preparation method comprises the steps of: heating polyethylene wax to melt it completely, and adding purified potassium ferrate; under a stirring condition, dispersing the potassium ferrate in the polyethylene wax melt liquid uniformly; stopping heating, and subjecting the potassium ferrate / polyethylene wax disperse system to natural cooling and curing; and finally carrying out crushing and drying, thus obtaining the polyethylene wax coated stable potassium ferrate. The polyethylene wax coated stable potassium ferrate prepared by the method provided by the invention has high coating rate, controllable slow-release property and stability. The method provided by the invention employs melting-stirring dispersion-condensation technique to prepare coated potassium ferrate, does not use organic solvent as the dispersant, and has the advantages of good environmental protection property, simple process and easy operation.

Description

technical field [0001] The invention relates to a coagulation disinfectant used in the field of water treatment, in particular to a polyethylene wax-coated stable potassium ferrate with a slow-release function and a preparation method thereof. Background technique [0002] Potassium ferrate (K 2 FeO 4 ) as a new type of high-efficiency and multifunctional green water treatment agent integrating oxidation, adsorption, flocculation, sterilization and deodorization, compared with other similar water treatment agents with a single function, it has the advantages of less dosage, high efficiency, and coagulation Due to the advantages of less amount of sedimented sludge and no toxic by-products, it has broad application prospects in the field of water treatment. At present, potassium ferrate has been industrially produced on a certain scale at home and abroad, but because potassium ferrate is extremely oxidizing, it is easy to decompose when it is exposed to moisture or heat, and...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C08J3/12C08L23/06C08K3/24C02F1/56C02F1/52C02F1/50
Inventor 李新杰章秋菊唐淑娟张跃军于文敦
Owner NANJING UNIV OF SCI & TECH