A kind of halogen-free flame-retardant composite material and preparation method thereof
A flame retardant composite material and composite material technology, applied in the field of halogen-free flame retardant composite material and its preparation, can solve non-polar and other problems, achieve good adhesion, improve mechanical strength, increase wear resistance and oil resistance sexual effect
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Embodiment 1
[0038] A preparation method of a halogen-free flame-retardant composite material, comprising the following steps:
[0039] (1) According to the percentage by weight, after mixing and stirring 54% PP, 10% TPU, 20% aluminum hypophosphite, 10% flame retardant synergist, 5% EDPM-g-MAH and 1% coupling agent, the obtained Mixture; wherein, the flame retardant synergist is a composite flame retardant of MCA and zinc borate, wherein the mass ratio of MCA to zinc borate is 1:1; the coupling agent is KH560 silane coupling agent.
[0040] (2) Send the mixture uniformly stirred through step (1) into an extruder, the reaction time of the mixture in the extruder is 3-5min, and the reaction temperature is 180-190° C. to obtain a mixture in a molten state;
[0041] (3) The mixture in the molten state is extruded into strips by an extruder to flow out, and then pelletized after being cooled under water to obtain PP / TPU composite material pellets. The product performance is detailed in Table 1...
Embodiment 2
[0043] A preparation method of a halogen-free flame-retardant composite material, comprising the following steps:
[0044] (1) According to the percentage by weight, after mixing and stirring 44% PP, 20% TPU, 20% aluminum hypophosphite, 10% flame retardant synergist, 5% EDPM-g-MAH and 1% coupling agent, the obtained Mixture; wherein, the flame retardant synergist is a composite flame retardant with a mass ratio of MCA and zinc borate of 1:1; the coupling agent is KH560 silane coupling agent.
[0045] (2) Sending the homogeneously stirred mixture through step (1) into an extruder, the reaction time of the mixture in the extruder is 3-5min, and the reaction temperature is 180-190° C. to obtain a mixture in a molten state;
[0046] (3) The mixture in the molten state is extruded into strips by an extruder to flow out, and then pelletized after being cooled under water to obtain PP / TPU composite material pellets. The product performance is detailed in Table 1.
Embodiment 3
[0048] A preparation method of a halogen-free flame-retardant composite material, comprising the following steps:
[0049] According to weight percentage, after mixing and stirring 54% PP, 10% TPU, 20% aluminum hypophosphite, 10% flame retardant synergist, 5% POE-g-MAH, and 1% coupling agent evenly, a mixture is obtained. Wherein, the flame retardant synergist is a composite flame retardant with a mass ratio of MCA and zinc borate of 1:1; the coupling agent is KH560 silane coupling agent.
[0050] Others are the same as in Example 1. The product properties are detailed in Table 1.
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