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Lightweight conductive shielding composite material and preparation method thereof

A technology of conductive shielding and composite materials, which is applied in the field of lightweight conductive shielding composite materials and its preparation, can solve the problems of affecting the electromagnetic shielding performance of the product, easily polluting the environment, and degrading the mechanical properties of the product, so as to be suitable for large-scale The effect of industrialized production, reliable electromagnetic shielding performance and reasonable structure

Active Publication Date: 2017-03-01
HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, no matter the product or its manufacturing method, there are deficiencies. First, the carbon nanotubes in the polymer foam are easy to agglomerate, so it is extremely difficult to distribute evenly in the foam, thereby affecting the conductivity of the product. It especially affects the electromagnetic shielding performance of the product; secondly, the product formed due to foaming not only easily makes the carbon nanotubes in it further agglomerate during foaming, but also makes the mechanical properties of the product worse, which affects its application. Thirdly, the manufacturing method can neither obtain products with reliable electromagnetic shielding performance and good mechanical properties, but also requires surfactants, catalysts, foaming agents, curing agents and other raw materials, which are easy to pollute the environment

Method used

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  • Lightweight conductive shielding composite material and preparation method thereof
  • Lightweight conductive shielding composite material and preparation method thereof
  • Lightweight conductive shielding composite material and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0038] The specific steps of preparation are:

[0039] Step 1. First, mix the fluoroplastics, etched phases, carbon nanotubes and hollow glass beads at a weight ratio of 20:60:0.5:40 at 15°C to obtain a mixture; where the fluoroplastic is poly Vinyl fluoride, the etching phase is polyvinyl chloride, and the carbon nanotubes are multi-walled carbon nanotubes. Then put the mixture in a torque rheometer, and knead at 150°C and 100r / min for 20 minutes to obtain a mixture.

[0040] Step 2: Put the mixed material on a plate vulcanizing machine, and heat-press at 200°C and 10MPa for 60 minutes to obtain a composite board. The composite board was soaked in a solvent for 2 hours and then dried at 60°C for 15 hours. The solvent was xylene. Before drying the solvent-soaked composite board, ethanol was used to rinse the surface deposits. The system is similar to figure 1 with figure 2 As shown, and as image 3 Lightweight conductive shielding composite material shown in the curve.

Embodiment 2

[0042] The specific steps of preparation are:

[0043] Step 1. Firstly mix the fluoroplastic, etched phase, carbon nanotubes and hollow glass beads at a weight ratio of 30:50:5:30 at 19°C to obtain a mixture; where the fluoroplastic is polypolarized Vinyl fluoride, the etching phase is polyvinyl chloride, and the carbon nanotubes are multi-walled carbon nanotubes. Then put the mixture in a torque rheometer, and knead at 175°C and 83r / min for 17 minutes to obtain a mixture.

[0044] Step 2: Put the mixed material on a plate vulcanizing machine, and heat-press at 220°C and 8MPa for 48 minutes to obtain a composite board. The composite board was soaked in a solvent for 6 hours and then dried at 65°C for 18 hours; the solvent was xylene. Before drying the composite board soaked in the solvent, ethanol was used to rinse the surface deposits. The system is similar to figure 1 with figure 2 As shown, and as image 3 Lightweight conductive shielding composite material shown in the curv...

Embodiment 3

[0046] The specific steps of preparation are:

[0047] Step 1. Firstly mix the fluoroplastics, etched phases, carbon nanotubes and hollow glass beads at a weight ratio of 40:40:10:20 at 23°C to obtain a mixture; where the fluoroplastic is poly Vinyl fluoride, the etching phase is polyvinyl chloride, and the carbon nanotubes are multi-walled carbon nanotubes. Then put the mixture in a torque rheometer and knead at 200°C and 75r / min for 13 minutes to obtain a mixture.

[0048] Step 2: Put the mixed material on a plate vulcanizing machine, and hot press at 240°C and 5MPa for 35 minutes to obtain a composite board. The composite board was soaked in a solvent for 11 hours and then dried at 70°C for 10 hours; the solvent was xylene. Before drying the composite board soaked in the solvent, ethanol was used to rinse the surface deposits. Made like figure 1 with figure 2 As shown, and as image 3 Lightweight conductive shielding composite material shown in the curve.

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Abstract

The invention discloses a light, conducting and shielding composite material and a preparation method thereof. The light, conducting and shielding composite material is composed of fluoroplastic, carbon nano tubes and hollow glass beads in a weight ratio of (20-60):(0.5-20):(0.5-40), wherein the fluoroplastic is foamed, and the carbon nano tubes are arranged in the fluoroplastic and are of a network structure. The preparation method of the light, conducting and shielding composite material comprises the following steps: firstly uniformly mixing the fluoroplastic, an etching phase, the carbon nano tubes and the hollow glass beads, so as to obtain a mixture; then mixing the mixture in a torque rheometer, so as to obtain a mixed material; and then carrying out hot pressing on the mixed material on a plate vulcanization machine, so as to obtain a composite board, then soaking the composite board in a solvent for removing the etching phase, and drying, so as to obtain the target product, namely the light, conducting and shielding composite material. The light, conducting and shielding composite material has the advantages of light weight, reliable electromagnetic shielding performance, good mechanical properties, simple technology, no pollution, low cost and applicability in large-scale industrial production, and can be easily and widely applied to electronic equipment and intensive systems in the fields of spaceflight, aviation, automobiles and the like.

Description

Technical field [0001] The invention relates to a conductive shielding composite material and a preparation method, in particular to a lightweight conductive shielding composite material and a preparation method thereof. Background technique [0002] Electromagnetic shielding materials are widely used in some electronic equipment and dense systems. Traditional electromagnetic shielding materials are generally made of metal. Although their shielding effect is good, they also have the defects of heavy quality, easy corrosion, and poor processing performance; it is difficult to apply them in aerospace, aviation, automotive and other fields. Recently, people have made some beneficial attempts and efforts in order to obtain lightweight electromagnetic shielding materials. For example, the Chinese Patent Application Publication CN 1656574A published on August 17, 2005 a conductive polymer foam and elastomer and its Production method. The conductive polymer foam described in the publi...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L27/16C08L27/06C08K7/24C08K7/28B29C35/02
Inventor 王慧郑康张献包超丁欣郭乐田兴友
Owner HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI
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