A kind of preparation method of chemical residue-free wallpaper base paper
A wallpaper and base paper technology, applied in paper, papermaking, textiles and papermaking, etc., can solve the problems of poor water solubility and less application of chitin natural polymer materials, increase stiffness and tensile strength, protect and resist The effect of good tensile energy and water solubility
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Embodiment 1
[0018] A method for preparing wallpaper base paper without chemical residues, comprising the following preparation steps:
[0019] (1) Preparation of modified chitin slurry: Weigh 50g of chitin, add 400ml of potassium hydroxide with a mass concentration of 25%, heat the reaction in a water bath for 30min, control the temperature of the water bath at 98°C, then adjust the pH to 7.0, and pump it with a vacuum pump filter, then add 15 g of chitin deacetylase, and react for 12 hours at a pH of 4.0 and a temperature of 40°C;
[0020] (2) Add the modified chitin slurry of step (1) in the pulp mixing tank, the amount of modified chitin slurry is 20% of the pulp weight;
[0021] (3) Internet surfing, pressing and drying;
[0022] (4) Add paper stiffness improver: the formula of the paper stiffness improver is: 2 parts by weight of chitosan alkenoic acid aqueous solution with a mass concentration of 3%, 1 part by weight of polyacrylamide aqueous solution, 2 parts by weight of acetic a...
Embodiment 2
[0025] A method for preparing wallpaper base paper without chemical residues, comprising the following preparation steps:
[0026] (1) Preparation of modified chitin slurry: Weigh 55g of chitin, add 450ml of potassium hydroxide with a mass concentration of 28%, heat the reaction in a water bath for 35min, control the temperature of the water bath at 99°C, then adjust the pH to 7.1, and use a vacuum pump Suction filtration, then add 16 g of chitin deacetylase, and react for 14 hours under the conditions of pH 4.2 and temperature 45°C;
[0027] (2) Add the modified chitin slurry of step (1) in the pulp mixing tank, the amount of the modified chitin slurry is 25% of the pulp weight;
[0028] (3) Internet surfing, pressing and drying;
[0029] (4) Add paper stiffness improver: the formula of the paper stiffness improver is: 2.5 parts by weight of chitosan alkenoic acid aqueous solution with a mass concentration of 3%, 1.5 parts by weight of polyacrylamide aqueous solution, 2 part...
Embodiment 3
[0032] A method for preparing wallpaper base paper without chemical residues, comprising the following preparation steps:
[0033] (1) Preparation of modified chitin slurry: Weigh 60g of chitin, add 500ml of potassium hydroxide with a mass concentration of 30%, heat the reaction in a water bath for 40min, control the temperature of the water bath at 100°C, then adjust the pH to 7.2, and use a vacuum pump Suction filtration, then add 18 g of chitin deacetylase, and react for 16 hours under the conditions of pH 4.5 and temperature 50°C;
[0034] (2) Add the modified chitin slurry of step (1) in the pulp mixing tank, the amount of the modified chitin slurry is 30% of the pulp weight;
[0035] (3) Internet surfing, pressing and drying;
[0036] (4) Add paper stiffness improver: the formula of the paper stiffness improver is: 3 parts by weight of chitosan alkenoic acid aqueous solution with a mass concentration of 3%, 2 parts by weight of polyacrylamide aqueous solution, 3 parts by ...
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