Method for treatment of titanium dioxide nanotubes with curcumin derivative
A curcumin derivative, titanium dioxide technology, applied in chemical instruments and methods, preparation of organic compounds, organic chemistry and other directions, can solve problems such as poor water solubility, patient danger, solvent residue, etc., and achieve long-lasting antibacterial effect, good antibacterial ability and Anticancer ability, effect of simple preparation method
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Embodiment 1
[0024] This program utilizes curcumin derivatives to process the method for titanium dioxide nanotubes, comprising the following steps:
[0025] 1) Dissolve 3 parts by weight of p-hydroxybenzaldehyde in 7 parts by weight of ethyl acetate, add 1 part by weight of 4-nitrobenzyl chloride, control 70 ° C, stir for 2 hours, and obtain a compound with formula (1), which is p-(4-nitrobenzyloxy)benzaldehyde;
[0026]
[0027] 2) Dissolve 2 parts by weight of p-(4-nitrobenzyloxy)benzaldehyde and 2 parts by weight of tributyl borate in 3 parts by weight of ethyl acetate, stir at room temperature for 5 minutes, add 0.5 parts by weight of acetylacetone and oxidize For the mixed solution of 0.5 parts by weight of boron, continue to stir at room temperature for 25 minutes, add 0.5 parts by weight of n-butylamine, continue to stir for 4 hours, then stop stirring and let it stand for 12 hours, then add 6 parts by weight of hydrochloric acid with a concentration of 0.4mol / L, and control the...
Embodiment 2
[0033] This program utilizes curcumin derivatives to process the method for titanium dioxide nanotubes, comprising the following steps:
[0034] 1) Dissolve 2 parts by weight of p-hydroxybenzaldehyde in 5 parts by weight of ethyl acetate, add 1 part by weight of 4-nitrobenzyl chloride, control 60 ° C, stir for 2 hours, and obtain a compound with formula (1), which is p-(4-nitrobenzyloxy)benzaldehyde;
[0035]
[0036] 2) Dissolve 1 part by weight of p-(4-nitrobenzyloxy)benzaldehyde and 1 part by weight of tributyl borate in 2 parts by weight of ethyl acetate, stir at room temperature for 3 minutes, then add 0.2 part by weight of acetylacetone and oxidize 0.1 parts by weight of boron mixed solution, continue to stir at room temperature for 20 minutes, add 0.2 parts by weight of n-butylamine, continue to stir for 3 hours, then stop stirring and let stand for 12 hours, then add 5 parts by weight of hydrochloric acid with a concentration of 0.4mol / L, and control the temperature...
Embodiment 3
[0042] This program utilizes curcumin derivatives to process the method for titanium dioxide nanotubes, comprising the following steps:
[0043] 1) Dissolve 5 parts by weight of p-hydroxybenzaldehyde in 10 parts by weight of ethyl acetate, add 3 parts by weight of 4-nitrobenzyl chloride, control 80 ° C, stir for 3 hours, and obtain a compound with formula (1), namely p-(4-nitrobenzyloxy)benzaldehyde;
[0044]
[0045] 2) Dissolve 4 parts by weight of p-(4-nitrobenzyloxy)benzaldehyde and 4 parts by weight of tributyl borate in 8 parts by weight of ethyl acetate, stir at room temperature for 7 minutes, add 1 part by weight of acetylacetone and oxidize For the mixed solution of 0.8 parts by weight of boron, continue to stir at room temperature for 30 minutes, then add 1 part by weight of n-butylamine, continue to stir for 5 hours, then stop stirring and let it stand for 18 hours, then add 10 parts by weight of hydrochloric acid with a concentration of 0.4mol / L, and control the...
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