Para-aramid nano fiber/polyphenylene sulfide non-woven fabric composite filter material and preparation method for same
A nanofiber, para-aramid fiber technology is applied in the field of composite filter material and its preparation, which can solve the problems of high cost, complicated preparation process, and no improvement in the filtration efficiency of tiny particles, and achieves long service life, simple preparation process, and preparation method. Simple and energy-saving effect
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[0034] The preparation method refers to compounding para-aramid nanofibers and polyphenylene sulfide non-woven fabrics to obtain a composite filter material. The preparation method follows the steps below:
[0035] ① Suspension and dispersion of para-aramid nanofibers
[0036] Adding N-methylpyrrolidone to the aramid resin jelly body formed by the para-aramid polymerization reaction to swell the jelly body, and then stirring at a high speed to break the swollen aramid resin jelly body into granular colloidal particles. Adding a dispersant to the swollen aramid resin jelly body and stirring at a high speed for dispersion to obtain a uniform and stable para-aramid nanofiber suspension dispersion.
[0037] Wherein, the resin content of the aramid resin jelly is 15%~28%; the mass ratio of the aramid resin jelly to N-methylpyrrolidone is 1:0.2~3; the swelling aramid resin jelly and The mass ratio of the dispersant is 1:1~6; the diameter of the para-aramid nanofiber contained in th...
Embodiment 1
[0049] ① Suspension and dispersion of para-aramid nanofibers
[0050] Adding N-methylpyrrolidone to the aramid resin jelly body formed by the para-aramid polymerization reaction to swell the jelly body, and then stirring at a high speed to break the swollen aramid resin jelly body into granular colloidal particles. Adding water to the swollen aramid resin jelly body, stirring and dispersing at a high speed, obtains a uniform and stable para-aramid fiber nanofiber suspension dispersion.
[0051] Wherein, the resin content of the aramid resin jelly is 15%; the mass ratio of the aramid resin jelly to N-methylpyrrolidone is 1:0.2; the mass ratio of the aramid resin jelly to the dispersant The ratio is 1:1; the diameter of the para-aramid nanofiber contained in the suspension dispersion is 40nm, the fiber length is 10um, and the fiber mass percentage is 6%.
[0052] ② Composite treatment of para-aramid nanofibers and polyphenylene sulfide non-woven fabrics
[0053] Spray the para...
Embodiment 2
[0061] ① Suspension and dispersion of para-aramid nanofibers
[0062] Adding N-methylpyrrolidone to the aramid resin jelly body formed by the para-aramid polymerization reaction to swell the jelly body, and then stirring at a high speed to break the swollen aramid resin jelly body into granular colloidal particles. Adding water to the swollen aramid resin jelly body, stirring and dispersing at a high speed, obtains a uniform and stable para-aramid fiber nanofiber suspension dispersion.
[0063] Wherein, the resin content of the aramid resin jelly is 18%; the mass ratio of the aramid resin jelly to N-methylpyrrolidone is 1:1; the mass ratio of the aramid resin jelly to the dispersant The ratio is 1:2; the diameter of the para-aramid nanofiber contained in the suspension dispersion is 50nm, the fiber length is 20um, and the fiber mass percentage is 6%;
[0064] ② Composite treatment of para-aramid nanofibers and polyphenylene sulfide non-woven fabrics
[0065] Immerse the poly...
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