Evaluation method of self-repairing effect of self-repairing cement-based material
A technology of cement-based materials and evaluation methods, applied in the direction of applying stable tension/pressure to test the strength of materials, preparation of test samples, etc., can solve the lack of direct improvement of material stiffness, toughness, impermeability, and erosion resistance durability Problems such as effective evaluation methods and single repair efficiency evaluation methods
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Embodiment 1 and 2
[0096] Both Examples 1 and 2 use microcapsule self-healing cement-based materials.
[0097] Firstly, microcapsules with self-healing properties were prepared. The ratio of the mass of the microcapsule particles to the total mass of the finished microcapsule (ie, the microcapsule emulsion system) is the solid content of the microcapsule. The solid content of the microcapsules in Examples 1 and 2 is 40%. The ratio of raw materials is as shown in Table 1:
[0098] Table 1:
[0099] raw material
[0100] potassium persulfate
[0101] The preparation process is as follows:
[0102] (1) take each component material by proportioning;
[0103] (2) Add the epoxy resin diluted with benzyl alcohol as a diluent into a bucket container, stir and dilute;
[0104] (3) Sodium dodecylbenzene sulfonate is used as emulsifier, and octylphenylpolyethylene oxide is used as surfactant, both are mixed with deionized water, after stirring and dispersing for 8 minutes, join in ...
test approach 1
[0113] The test method of embodiment 1 and 2 is consistent, and concrete steps are as follows:
[0114] (1) prepare sample according to sample preparation scheme described in the present invention, each test group prepares 9 specimens, wherein 3 specimens are used for testing reference strength, and other 6 specimens are used for setting different degrees of pre-destruction;
[0115] (2) After the test piece reaches its age, cut a crack with a length of 40mm, a width of 0.5mm, and a depth of 10mm on the side;
[0116] (3) Carry out three-point flexural tests on 3 test pieces of each test group, measure the flexural strength of the samples under different curing conditions with different dosages, and take the average value of the three test data for the final data;
[0117] (4) Carry out different degrees of pre-destruction to the other 6 specimens of each test group according to the method provided in the technical scheme, that is, the aforementioned summary of the invention, ...
Embodiment 3 and 4
[0133] Examples 3 and 4 both use mineral self-healing cement-based materials.
[0134] Both Examples 3 and 4 use a 40mm×40mm×160mm concrete test block to characterize the change of the internal damage degree of the material after mineral self-repair.
[0135] Firstly, concrete materials with mineral self-healing properties are prepared. In Examples 3 and 4, the cementitious material is P O4 2.5 ordinary portland cement; the fine aggregate is river sand, and the fineness modulus is 2.2; the coarse aggregate is continuously graded from 5mm to 25mm; the expansion agent is UEA expansion agent; water reducer using polycarboxylate water reducer. The ratio of raw materials is as shown in Table 5:
[0136] table 5:
[0137]
[0138] After the test pieces were formed, Example 3 was placed in a concrete standard curing room for 28 days, and Example 4 was placed in an aqueous calcium hydroxide solution for 28 days.
[0139] The test method of embodiment 3 and 4 is consistent, and ...
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