A kind of low-sulfur diesel oil additive and its preparation process

A low-sulfur diesel and additive technology, which is applied in fuel additives, petroleum industry, liquid carbon-containing fuels, etc., can solve the problem that the miscibility of biodiesel and low-sulfur diesel is not good enough, and cannot effectively improve the combustion rate of low-sulfur diesel, low-sulfur The lubricity of diesel oil has not been greatly improved, and the effects of reducing oxidation sediment, reducing emissions, and strong adsorption and capture capabilities have been achieved

Active Publication Date: 2017-04-05
丁以钿
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, because the miscibility of biodiesel and low-sulfur diesel is not good enough, if 50% of the amount of low-sulfur diesel is added to low-sulfur diesel, it needs constant vigorous mechanical stirring to make the two completely miscible. Therefore, If you want to directly use biodiesel to improve the lubricity of low-sulfur diesel, on the one hand, it is inconvenient to use; Sulfur Diesel Combustion Rate

Method used

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  • A kind of low-sulfur diesel oil additive and its preparation process
  • A kind of low-sulfur diesel oil additive and its preparation process
  • A kind of low-sulfur diesel oil additive and its preparation process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Embodiment one: the preparation method of low-sulfur diesel oil additive, it comprises the following steps: by weight ratio,

[0021] First add 40 parts of biodiesel and 20 parts of solubilizer in reaction vessel, wherein, contain in every hundred parts of solubilizer, 40 parts of sorbitan stearate, 45 parts of polyethylene oxide sorbitol monostearate Esters, 15 parts of sorbitan monooleate, slowly heated while stirring to raise the temperature to 90°C, then stirred at 90°C for 0.5h, then lowered the temperature to 55°C and kept it within the range of 55°C;

[0022] Then add 8 parts of glyceryl stearate, 2 parts of ethyl stearate and 15 parts of oleic acid amide, and stir for 1 hour to fully dissolve the raw materials; then add 10 parts of detergent and stir for 25 minutes, wherein, every hundred parts of detergent contains , 15 parts of imidazoline, 85 parts of T151A polyisobutenyl succinimide;

[0023] Add 5 parts of antioxidants at last, wherein, contain in every hu...

Embodiment 2

[0024] Embodiment two: the preparation method of low-sulfur diesel oil additive, it comprises the following steps: by weight ratio,

[0025] First add 43 parts of biodiesel and 22 parts of solubilizer in reaction vessel, wherein, contain in every hundred parts of solubilizer, 42 parts of sorbitan stearate, 40 parts of polyethylene oxide sorbitol monostearate Esters, 18 parts of sorbitan monooleate, slowly heated while stirring to raise the temperature to 92°C, then stirred at 92°C for 0.8h, then lowered the temperature to 60°C and kept it within the range of 60°C;

[0026] Then add 5 parts of glyceryl stearate, 4 parts of ethyl stearate and 12 parts of oleic acid amide, and stir for 1.2 hours to fully dissolve the raw materials; then add 7 parts of detergent and stir for 30 minutes, wherein, every hundred parts of detergent contains , 20 parts of imidazoline, 80 parts of T151A polyisobutenyl succinimide;

[0027] Add 7 parts of antioxidants at last, wherein, contain in every ...

Embodiment 3

[0028] Embodiment three: the preparation method of low-sulfur diesel oil additive, it comprises the following steps: by weight ratio,

[0029] First add 42 parts of biodiesel and 23 parts of solubilizer in reaction vessel, wherein, contain in every hundred parts of solubilizer, 43 parts of sorbitan stearate, 38 parts of polyethylene oxide sorbitol monostearate Esters, 19 parts of sorbitan monooleate, slowly heated while stirring to raise the temperature to 92°C, then stirred at 92°C for 0.8h, then lowered the temperature to 60°C and kept it within the range of 60°C;

[0030] Then add 6 parts of glyceryl stearate, 3 parts of ethyl stearate and 12 parts of oleic acid amide, and stir for 1.2 hours to make the raw materials fully dissolve; then add 8 parts of detergent and stir for 30 minutes, wherein, every hundred parts of detergent contains , 18 parts of imidazoline, 82 parts of T151A polyisobutenyl succinimide;

[0031] Finally, add 6 parts of antioxidants, wherein every one ...

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Abstract

The invention relates to a low-sulfur diesel additive and a preparation technology thereof. The low-sulfur diesel additive comprises the following components in parts by weight: 40-45 parts of biodiesel, 3-8 parts of glyceryl stearate, 2-5 parts of ethyl stearate, 9-15 parts of oleamide, 20-24 parts of solubilizer, 6-10 parts of detergent and 5-8 parts of antioxidant. A preparation method of the low-sulfur diesel additive comprises the following steps: adding the biodiesel and solubilizer into a reaction container; heating and stirring and adding the glyceryl stearate, ethyl stearate and oleamide; adding the detergent and the antioxidant and stirring and mixing; and after that, filtering to obtain the low-sulfur diesel additive. The advantages of the invention are as follows: the low-sulfur diesel additive can be dissolved well with diesel, and the lubricating property of the diesel can be obviously improved; and the low-sulfur diesel additive also has oxidation resistance as well as detergency and dispersibility.

Description

technical field [0001] The invention relates to the field of additives, in particular to a low-sulfur diesel additive and a manufacturing process thereof. Background technique [0002] Diesel is a product of petroleum refining, which occupies a relatively high share in the fuel structure of all countries in the world and has become an important power fuel. With the acceleration of dieselization of vehicles worldwide, the demand for diesel will increase in the future, but the exhaust gas emitted after diesel combustion is also increasingly harmful to the environment. For example, sulfur dioxide and nitrogen oxides in the exhaust gas not only form acid rain in cities and surrounding areas, but also seriously damage the earth's ozone layer. Particulate matter (PM) contains a variety of substances that are listed as possible carcinogens by international research institutions. At the same time, particulate matter is the cause of fog. The culprit of smog. Studies have shown that...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C10L1/196C10L1/19C10L1/224C10L1/198C10L1/233C10L1/236C10L1/223C10L1/183C10L10/18C10L10/08C10L10/02C10L10/04
CPCC10L1/143C10L1/1832C10L1/1905C10L1/1915C10L1/196C10L1/1983C10L1/223C10L1/224C10L1/233C10L1/2364C10L10/02C10L10/04C10L10/08C10L10/18C10L2300/20
Inventor 丁以钿刘五连游子扬丁宏
Owner 丁以钿
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