Preparation method of environment-friendly emulsified releasing agent

A release agent and emulsifying technology, which is applied in the field of preparation of environmentally friendly emulsifying release agents, can solve problems such as high cost, shortage, and health hazards for operators, and achieve no pollution to the environment, no corrosion of molds, and good cleaning performance Effect

Inactive Publication Date: 2016-04-13
刘方旭
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, most of the domestic release agents are oil release agents. The raw materials of oil release agents are in short supply, the cost

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0013] A preparation method of an environmentally friendly emulsifying release agent comprises the following raw materials in parts by mass: 15 kg of simethicone oil, 4 kg of PVA-1788 polyvinyl alcohol, 4 kg of PVA-1799 polyvinyl alcohol, 6 kg of ricinoleic acid, Poly fatty acid 3 kg, dodecyl diphenyl ether sulfonate 1 kg, sorbitan palmitate 4 kg, diglycolamine 2 kg, triisopropanolamine 4.7 kg, dodecyl dibasic acid 1.0 kg, 0.05 kg of fungicide, and 45 kg of deionized water.

[0014] The preparation method is: 4 kg of PVA-1788 polyvinyl alcohol and 4 kg of PVA-1799 polyvinyl alcohol are dissolved in 20 kg of deionized water at 85°C to make a polyvinyl alcohol solution for use; In the container of the thermometer, add 2 kg of diglycolamine, 4.7 kg of triisopropanolamine and 1 kg of deionized water, mix well, then add 6 kg of ricinoleic acid, 3 kg of dimer fatty acid and dodecyl 1.0 kg of dibasic acid, after stirring and reacting for 2 hours at 60-70°C, add 15 kg of dimethyl sil...

Embodiment 2

[0016] A preparation method of an environmentally friendly emulsifying release agent comprises the following raw materials in parts by mass: 20 kg of simethicone oil, 6.5 kg of PVA-1788 polyvinyl alcohol, 7.5 kg of ricinoleic acid, 4.5 kg of dimer fatty acid, sulfonate di Polysurfactant 1.5 kg, sorbitan oleate 4.5 kg, monoisopropanolamine 1.5 kg, triisopropanolamine 1.5 kg, triethanolamine 3.2 kg, undecane dibasic acid 0.6 kg, fungicide 0.08 kg, 52 kg of deionized water.

[0017] Its preparation method is: 6.5 kg of PVA-1788 polyvinyl alcohol is dissolved in 17 kg of deionized water at 80 ° C to make a polyvinyl alcohol solution for use; in a container with a stirrer and a thermometer, add diglycol 2 kg of alkanolamine, 4.7 kg of triisopropanolamine and 1.5 kg of deionized water, after mixing evenly, add 6 kg of ricinoleic acid, 3 kg of dimer fatty acid and 1.0 kg of dodecane dibasic acid. After stirring and reacting at 70°C for 3 hours, add 15 kg of simethicone oil, 1.5 kg o...

Embodiment 3

[0019] A preparation method of an environmentally friendly emulsifying release agent comprises the following raw materials in parts by mass: 25 kg of dimethyl silicone oil, 5 kg of PVA-1792 polyvinyl alcohol, 9 kg of ricinoleic acid, 6 kg of dimer fatty acid, and 5 kg of co-emulsifier kg, 1.6 kg of monoethanolamine, 5.5 kg of triethanolamine, 0.4 kg of dodecane dibasic acid, 0.4 kg of undecane dibasic acid, 0.1 kg of fungicide, and 60 kg of deionized water.

[0020] Its preparation method is: 5 kg of PVA-1792 polyvinyl alcohol is dissolved in 15 kg of deionized water at 90 ° C to make a polyvinyl alcohol solution for use; in a container with a stirrer and a thermometer, add diethylene glycol 2 kg of amine, 4.7 kg of triisopropanolamine and 2 kg of deionized water, after mixing evenly, add 6 kg of ricinoleic acid, 3 kg of dimer fatty acid and 1.0 kg of dodecane dibasic acid. After stirring and reacting at ℃ for 3 hours, add 15 kg of simethicone, 2 kg of fatty alcohol polyoxyeth...

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PUM

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Abstract

The invention discloses a preparation method of an environment-friendly emulsified releasing agent. The environment-friendly emulsified releasing agent comprises the following raw materials by mass, 15-25 parts of simethicone, 5-8 parts of polyvinyl alcohol, 6-9 parts of ricinoleic acid, 3-6 parts of dimer fatty acid, 5-7 parts of assistant emulsifiers, 6-10 parts of hydroxyalkyl ammonium, 0.6-1.0 part of organic dicarboxylic acid, 0.05-0.1 part of bactericide and 45-60 parts of deionized water. By adopting the film forming mode that a primary emulsifier and an antirust agent are synthesized by organic acid and hydroxyalkyl ammonium, in company with the assistant emulsifiers, simethicone is emulsified in the deionized water and polyvinyl alcohol, the external-use emulsified releasing agent is mainly used for epoxy resin and unsaturated polyester material forming dies, and is sprayed to the surfaces of the dies for use, so that the effects that epoxy resin and unsaturated polyester products are easy to form, do not corrode the dies, and are not bonded with the dies are reached; and the environment-friendly emulsified releasing agent has the characteristics that no decomposition residues exist, the colors and performances and the products are not affected, the cleaning property is good and no pollution to environment is caused.

Description

technical field [0001] The invention relates to the technical field of release agents, in particular to a preparation method of an environmentally friendly emulsifying release agent. Background technique [0002] The release agent is a functional substance between the mold and the finished product. The release agent is an interface coating used on the surface of two objects that are easy to adhere to each other. It can make the surface of the object easy to release, smooth and clean. It is an indispensable additive to prevent the formed composite product from sticking to the mold, improve production efficiency, prolong the service life of the mold, and at the same time make the surface of the product smooth, the size is qualified, and reduce defective products. In industrial production, during the molding process of some molding materials such as epoxy resin and unsaturated polyester, it is required to have a certain thermal stability when demolding, not to corrode the mold...

Claims

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Application Information

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IPC IPC(8): B29C33/64
CPCB29C33/64
Inventor 刘方旭
Owner 刘方旭
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