Liquid gum and preparing method thereof
A technology of chewing gum and liquid, which is applied in the field of liquid chewing gum and its preparation, which can solve problems such as not easy to decompose, pollute the environment, and cannot be absorbed by the human body, and achieve the effect of promoting health and simple process
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preparation Embodiment 1
[0026] Preparation Example 1: Pure Natural Essential Oil Liquid Chewing Gum
[0027] Step 1, the preparation of low molecular weight chitosan solution
[0028] Chitosan with a degree of deacetylation of 80% and a molecular weight of 80kDa is mixed with purified water and acetic acid in a mass ratio of 1:100:1, stirred and dissolved at 50°C until all dissolve evenly (determine the reaction time depending on the amount of material, from Between 1h and 24h) add hydrogen peroxide solution (30% mass concentration) accounting for 2% of the total reactant mass, stir and react for 2h, and vacuum-concentrate the whole at 60°C to a paste (water content 20wt.%).
[0029] Step 2, the preparation of high-purity (95wt.%) fatty acid:
[0030] Reagent-grade mixed fatty acids (provided by Guangzhou Chemical Reagent Factory) (a mixture of myristic acid, palmitic acid, stearic acid, oleic acid, linoleic acid, and linolenic acid): methanol: polyglycerol ester (provided by Zhengzhou Dahe Food Tec...
preparation Embodiment 2
[0037] Preparation Example 2: Pure Natural Essential Oil Liquid Chewing Gum
[0038] Step 1, the preparation of low molecular weight chitosan solution
[0039] Chitosan with deacetylation degree 85%, molecular weight 140kDa and pure water and acetic acid are carried out stirring and dissolving at 60 ℃ by the mass ratio of 2: 150: 1, after all dissolving evenly (depending on how many materials determine the reaction time, from Between 1h and 24h) add 6% hydrogen peroxide solution (30% mass concentration) accounting for 6% of the total reactant mass, stir and react for 6h, and concentrate the whole in vacuum at 70°C to a paste (water content 40%).
[0040] Step 2, the preparation of high-purity (90wt.%) monounsaturated fatty acid
[0041]Reagent-grade mixed fatty acids (provided by Guangzhou Chemical Reagent Factory) (a mixture of myristic acid, palmitic acid, stearic acid, oleic acid, linoleic acid, and linolenic acid): methanol: polyglycerol ester (provided by Zhengzhou Dahe ...
preparation Embodiment 3
[0048] Preparation Example 3: Pure Natural Essential Oil Liquid Chewing Gum
[0049] Step 1, the preparation of low molecular weight chitosan solution
[0050] With deacetylation degree 90%, the chitosan of molecular weight 200kDa and purified water and acetic acid are carried out stirring and dissolving at 70 ℃ by the mass ratio of 3: 200: 2, after all dissolving evenly (determining the reaction time with how many materials, from Between 1h and 24h) add 10% of the total reaction mass of hydrogen peroxide solution (mass concentration: 30%), stir and react for 10h, and concentrate the whole in vacuum at 80°C to a paste (water content: 60wt.%).
[0051] Step 2, the preparation of fatty acid:
[0052] Monounsaturated fatty acid (reagent grade oleic acid or palmitoleic acid) with a purity of 60% (mass) was selected as the material.
[0053] Step 3, the preparation of chitosan emulsion
[0054] Taking the weight of the above-mentioned low-molecular-weight chitosan solution as a ...
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