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High-carbon spent catalyst continuous regeneration method

A catalyst to be produced, catalyst technology, applied in catalyst regeneration/reactivation, chemical instruments and methods, physical/chemical process catalysts, etc. Excessive pressure drop and other problems, to achieve the effect of preventing flying temperature, reducing frequency and low water content

Inactive Publication Date: 2016-05-11
SINOPEC GUANGZHOU ENG +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Such as local overheating of the catalyst bed, excessive bed pressure drop, intolerance to dust clogging, difficult switching operation and high cost of catalyst recovery, etc.
Although the fluidized bed is more conducive to the reaction in terms of transfer, the inevitable catalyst wear and separation problems have always been troublesome engineering problems
In this method, one section of the regenerator is burnt, there is no drying zone, there is no effective means to control the temperature of the burnt bed of the regenerator, and there is no catalyst roasting and drying process

Method used

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  • High-carbon spent catalyst continuous regeneration method

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Embodiment Construction

[0031] The unborn catalyst from the reaction part enters the reactor lower hopper 3 at the bottom of the last reactor 2, and first replaces the carried hydrocarbons with nitrogen, and then enters the reactor riser 4, which uses self-circulating nitrogen The nitrogen from the compressor 5 lifts the raw catalyst to the separation hopper 6 at the top of the regenerator 8, where the raw catalyst enters the lock hopper 7 in a nitrogen environment after the dust is blown off by the elutriation gas, and then enters the regenerator 8. The control system of the lock hopper 7 controls the five steps of waiting, pressurization, discharge, depressurization and charging of the lock hopper 7 through pressure balance, and sends the catalyst from the separation hopper 6 to the regenerator 8 and controls the catalyst flow rate. The coke regeneration process is completed in the regenerator 8, and the regenerated catalyst enters the regenerator lower hopper 16 and is replaced with nitrogen, then ...

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Abstract

The present invention discloses a high-carbon spent catalyst continuous regeneration method. The main technical program is as follows: a regenerator comprises, from top to bottom, a buffer zone, a scorching zone and a drying zone, the scorching zone comprises an upper scorching section and a lower scorching section, a regeneration gas from the regenerator is led out from the upper part of the regenerator, and divided into three ways after heat change, cooling, drying and compression, a first way is supplemented with air, then enters the upper scorching section of the regenerator after increasing of temperature by heating, a second way is supplemented with the air, then enters the lower scorching section of the regenerator after increasing of temperature by heating, a third way as a drying gas enters the drying zone, the regeneration gas and a spent catalyst are in crossflow contact in the scorching zone, the catalyst scorched in the scorching zone downward enters the drying zone to complete the entire scorching regeneration process, the catalyst after the regeneration is recycled, and the regeneration gas completing the scorching in the scorching zone and the drying gas from the drying zone of the regenerator are led out from the upper part of the regenerator for recycling. The method can effectively control scorching bed layer temperature of the regenerator and extends the service life of the catalyst.

Description

technical field [0001] The invention belongs to the field of catalyst regeneration in coal chemical industry or natural gas chemical industry, and in particular relates to a method for continuous regeneration of a high-carbon standby catalyst in methanol conversion to hydrocarbon production reaction using moving bed technology. Background technique [0002] At present, in the field of coal chemical industry or natural gas chemical industry, technologies such as methanol to propylene (MTP), methanol to gasoline (MTG) and methanol to aromatics (MTA) are research hotspots at home and abroad. On the one hand, these technologies can make efficient chemical utilization of coal resources, and on the other hand, they can solve the situation of high dependence on imports of related products caused by the shortage of oil resources. Therefore, the partial substitution of petroleum supply by synthesizing hydrocarbons from methanol has received great attention. [0003] In the conversio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J38/22B01J38/14B01J38/20
Inventor 徐又春郭劲鹤孙秋荣李爱国杨旭东寇肖董海芳王发辉孙晓娟张钟岩罗妍杨红斌李健田纪伟曾菁冯好喆
Owner SINOPEC GUANGZHOU ENG
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