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3results about How to "Avoid flying temperature" patented technology

A fully autonomous self-adaptive heat pipe heat transfer performance testing method

This invention belongs to the field of high-temperature heat pipe performance testing technology, specifically relating to a fully autonomous adaptive heat pipe heat transfer performance testing method. It includes the following steps: Step S1: Generating a heat flux density benchmark based on geometric features; Step S2: Using P... base Based on this, differentiated power loading is performed using a stage-dependent loading coefficient β. During step S2, steps S3 to S5 are executed in parallel: Step S3: Parallel execution of adaptive physical stage switching based on a dual criterion of "temperature-anomaly"; Step S4: Parallel execution of autonomous steady-state determination for each power loading at key temperature points in the linear heat transfer stage and during each power loading in the limit approximation stage; Step S5: Parallel execution of full-cycle automated safety protection based on monitoring the second derivative of the evaporation section temperature. The beneficial effects are: improved adaptability of the testing method, compatible with heat pipes of different geometric dimensions; and effective improvement of testing efficiency through the implementation of a staged control strategy.
Owner:NUCLEAR POWER INSTITUTE OF CHINA

A process for the preparation of ethyl acetoacetate by crude ester recycle cooling

ActiveCN116037028BTimely and effective dilutionSolve the problem of rapid temperature riseOrganic compound preparationTransportation and packagingChemical industryAcetic acid
The application discloses a process method for preparing ethyl acetoacetate by crude ester circulation cooling, and belongs to the technical field of chemical industry. The method can dilute the heat generated in the reaction in time and effectively by performing crude ester circulation in the continuous reaction process, better solves the problem of heat accumulation in the reactor, and cannot dissipate heat in time, thereby causing the problem of rapid temperature rise, and avoids the "flying temperature" in the reaction process; the temperature in the reactor is stable without other complex and strict operation control, the operation is simple and feasible; the content of the crude product, the product quality and the yield are improved; the content of the crude methyl acetoacetate obtained by the method is 97.8-98.1%, the content of the finished product after rectification is 99.5-99.7%, and the product yield is 97.8-98.2%; the high-temperature resistance requirement of the pipeline equipment is reduced, and the safety hidden danger is reduced.
Owner:NANTONG ACETIC ACID CHEM

A calcium carbide furnace tail gas deep purification process

The application discloses a calcium carbide furnace tail gas deep purification process. The calcium carbide furnace tail gas is firstly subjected to wet desulfurization and dehydrocyanation and TSA treatment, and then sequentially enters a de-fluorine and de-hydrocyanation reactor, a hydrolysis desulfurization reactor, a fine desulfurization reactor, a de-phosphorus and de-arsenic reactor, a de-oxygen reactor and a de-hydrocarbon reactor. After the treatment process, the HCl content in the gas is less than 0.1 ppm, the HF content is less than 0.1 ppm, the HCN content is less than 0.1 ppm, the total sulfur content is less than 0.1 ppm, the AsH3 content is less than 5 ppb, the PH3 content is less than 5 ppb, the oxygen content is less than 10 ppm, and the unsaturated hydrocarbon content is less than 0.1 ppm, thereby meeting the separation and purification requirements of subsequent processes, and the pressure drop of the whole process is not more than 100 kPa. The process can remove oxygen and unsaturated hydrocarbons in the gas under low-temperature conditions, thereby reducing the occurrence of side reactions, and has the characteristics of reasonable process design, high purification precision, low energy consumption and low operation cost.
Owner:WUHAN KELIN FINE CHEM