Preparation method of novel fat substitute
A fat substitute, a new type of technology, applied in food preparation, food science, application, etc., can solve the problem of not being able to provide unsaturated fatty acids and achieve the effect of reducing energy
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Embodiment 1
[0014] 1. Preparation of soybean oil fatty acid methyl ester
[0015] Add 1kg of soybean oil and 400mL of methanol into a 2L three-necked flask, then add 7g of sodium methoxide, reflux at 90°C for 3h, wash with water three times after the reaction, and dry to obtain 900g of soybean oil fatty acid methyl ester.
[0016] 2. Preparation of fat substitute
[0017] Add 50g polyerythritol and 300g soybean oil fatty acid methyl ester into a 500mL three-necked flask, add 3.5g tetrabutylammonium bromide, 3.5g anhydrous potassium carbonate, and react under vacuum at 120°C for 3h. Cool to room temperature, wash the catalyst with water, deodorize, decolorize, and dry to obtain 300 g of yellow oily liquid.
Embodiment 2
[0019] 1. Structural identification
[0020] Infrared identification of fat substitutes was carried out by the solution method using a PEspectrumRX Fourier transform infrared spectrometer. Its infrared spectrum is characterized by: 2925cm -1 , 2854cm -1 is-CH 3 ,-CH 2 One stretching vibration absorption peak, 1744cm -1 It is C=O stretching vibration absorption peak, 1637cm -1 It is C=C stretching vibration absorption peak, 722cm -1 is the CH=CH (cis) out-of-plane bending vibration absorption peak.
[0021] 2. Determination of viscosity and density
[0022] The viscosity and density of the fat substitute and soybean oil were measured using a SVM3000 viscometer and compared with Olean (data from Technical Brochure). The viscosity of the fat substitute was larger than that of soybean oil and slightly smaller than that of Olean at different temperatures. The fat substitute is slightly denser than soybean oil.
[0023] 3. In vitro simulated intestinal fluid degradation ex...
Embodiment 3
[0028] 1. Application of fat substitutes in bread
[0029] Bread was prepared according to the control formula and the formulas comprising fat substitutes 20%, 50%, 100% (percentage refers to the percentage content of substituted butter), as shown in the following table:
[0030]
[0031] As a result, the shape of the bread with 20% fat substitute was the best, and the bread with 100% fat substitute had the best skin texture and taste. influence of things.
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