Flexible electromagnetic-wave shielding material and preparation method thereof
A shielding material and electromagnetic wave technology, which is applied in the field of electromagnetic wave shielding material preparation, can solve the problems of equipment without information security, endangering national information security, information leakage, etc., and achieve good electromagnetic wave shielding effect, soft mechanical properties, and easy promotion.
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Embodiment 1
[0017] (1) Add 6 parts of silver methanesulfonate, 3 parts of titanium silicide, 5 parts of nano-silicon carbide and 4 parts of nano-alumina into the mixture of 15 parts of ethambutol and 10 parts of propylene glycol, and stir well;
[0018] (2) Then add 30 parts of polyperfluoroethylene propylene resin, 25 parts of epoxy resin and 6 parts of methylprednisolone acetate, and stir for 10 minutes at a speed of 300 r / min at a temperature of 100 ° C;
[0019] (3) Then add 8 parts of 2-aminophenol-4-sulfonanilide and 10 parts of polymethyl methacrylate to it, and react at a temperature of 80°C for 15 minutes;
[0020] (4) After that, 7 parts of 4-phenyl-2-pyrrolidone was added dropwise, reacted at a temperature of 120° C. for 20 minutes, and then cooled to obtain the flexible electromagnetic wave shielding material.
Embodiment 2
[0026] (1) Add 9 parts of silver methanesulfonate, 5 parts of titanium silicide, 8 parts of nano-silicon carbide and 9 parts of nano-alumina into the mixture of 20 parts of ethambutol and 15 parts of propylene glycol, and stir well;
[0027] (2) Then add 40 parts of polyperfluoroethylene propylene resin, 35 parts of epoxy resin and 10 parts of methylprednisolone acetate, and stir for 20 minutes at a speed of 500 r / min at a temperature of 120 ° C;
[0028] (3) Then add 12 parts of 2-aminophenol-4-sulfonanilide and 15 parts of polymethyl methacrylate to it, and react at a temperature of 100°C for 20 minutes;
[0029] (4) Afterwards, 13 parts of 4-phenyl-2-pyrrolidone was added dropwise, reacted at a temperature of 130° C. for 40 minutes, and then cooled to obtain the flexible electromagnetic wave shielding material.
Embodiment 3
[0035] (1) Add 7 parts of silver methanesulfonate, 4 parts of titanium silicide, 6 parts of nano-silicon carbide and 5 parts of nano-alumina into the mixture of 16 parts of ethambutol and 11 parts of propylene glycol, and stir well;
[0036] (2) Then add 32 parts of polyperfluoroethylene propylene resin, 28 parts of epoxy resin and 7 parts of methylprednisolone acetate, and stir for 10 minutes at a speed of 300 r / min at a temperature of 100 ° C;
[0037] (3) Then add 9 parts of 2-aminophenol-4-sulfonanilide and 11 parts of polymethylmethacrylate to it, and react at a temperature of 80°C for 15 minutes;
[0038] (4) Afterwards, 8 parts of 4-phenyl-2-pyrrolidone were added dropwise, reacted at a temperature of 130° C. for 40 minutes, and then cooled to obtain the flexible electromagnetic wave shielding material.
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