Viscous physical stripping method for graphene
A physical exfoliation and graphene technology, applied in the direction of graphene, nano-carbon, etc., can solve the problems of reducing the service life of equipment, high acid consumption, sulfur residue in products, etc., to improve shearing effect, improve electrical conductivity, and efficient exfoliation. Effect
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[0022] Example 1
[0023] The present invention is a method for viscous physical exfoliation of graphene. The method includes the following steps:
[0024] S1. Pour the graphite flakes with a purity of 98% or more and a particle size of 30~500μm and the peeling liquid into the ball mill tank. The composition of the peeling liquid is: 100 parts by weight of water, 30 parts by weight of ethanol, and 50 parts by weight of polyacrylate Count, 0.5 parts by weight of lithium fluoride. Among them, the number average molecular weight of polyacrylate is greater than 100,000. The weight ratio of graphite flakes and peeling liquid is 1:2.
[0025] S2. Ball milling for 4 hours, the speed of the ball mill is 6000rpm / min.
[0026] S3. After the reaction is stopped, the suspension is discharged into the storage tank through the discharge port, and the initial product is obtained by standing for more than 24 hours.
[0027] S4. Transport the graphene suspension in the storage tank obtained in step S...
Example Embodiment
[0029] Example 2
[0030] The present invention is a method for viscous physical exfoliation of graphene. The method includes the following steps:
[0031] S1. Inject the graphite flakes with a purity of 98% or more and a particle size of 30~500μm and the stripping liquid into the ball mill tank. The composition of the stripping liquid is: 100 parts by weight of water, 40 parts by weight of ethanol, and 20 parts by weight of n-propanol. Count, 80 parts by weight of polyurethane-modified acrylate and 2 parts by weight of sodium fluoride. Among them, the number average molecular weight of the polyurethane-modified acrylate is greater than 100,000. The weight ratio of graphite flakes and peeling liquid is 1:3.
[0032] S2. Ball mill 8h, the speed of the ball mill is 4000rpm / min.
[0033] S3. After the reaction is stopped, the suspension is discharged into the storage tank through the discharge port, and the initial product is obtained by standing for more than 24 hours.
[0034] S4. Tra...
Example Embodiment
[0036] Example 3
[0037] The present invention is a method for viscous physical exfoliation of graphene. The method includes the following steps:
[0038] S1. Pour the graphite flakes with a purity of 98% or more and a particle size of 30~500μm and the stripping liquid into the ball mill tank. The composition of the stripping liquid is: 100 parts by weight of water, 40 parts by weight of n-butanol, and 40 parts by weight of propylene glycol. Number, 60 parts by weight of urethane-modified acrylate and 4 parts by weight of sodium chloride. Among them, the number average molecular weight of the polyurethane modified acrylate is greater than 100,000. The weight ratio of graphite flakes and peeling liquid is 1:4.
[0039] S2. The ball mill is 24h, the speed of the ball mill is 3000rpm / min.
[0040] S3. After the reaction is stopped, the suspension is discharged into the storage tank through the discharge port, and the initial product is obtained by standing for more than 24 hours.
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