Glass-ceramic for laser protection and preparation method thereof
A technology of laser protection and glass-ceramics, which is applied in glass manufacturing equipment, glass molding, manufacturing tools, etc., to achieve low expansion coefficient, good thermal shock and mechanical shock resistance
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Embodiment 1
[0020] A kind of laser protective glass-ceramic material of the present invention and preparation method thereof are as follows:
[0021] a. The oxidation composition of the basic glass is: SiO 2 (54wt%), Al 2 o 3 (22wt%), Li 2 O (4.3wt%), SrO (5wt%), MgO (5wt%), B 2 o 3 (1.5wt%), Na 2 O (0.4wt%), TiO 2 (3wt%), ZrO 2 (2wt%), Er 2 o 3 (2wt%), Bi 2 o 3 (0.5wt%), Co 2 o 3 (0.2wt%), Sb 2 o 3 (0.1 wt%). Correspondingly, the raw materials used are chemically pure chemical raw materials, corresponding to: silica, alumina powder, lithium carbonate, strontium carbonate, magnesium carbonate, boric acid, soda ash, titanium oxide, zirconia, erbium oxide, oxide Bismuth, cobalt trioxide and antimony trioxide.
[0022] b. Use the above-mentioned chemical raw materials for glass batching, including batching calculation, weighing, mixing and other processes.
[0023] c. Put the glass batch material into a corundum crucible and melt it in a silicon-molybdenum furnace with a te...
Embodiment 2
[0029] a. The oxidation composition of the basic glass is: SiO 2 (59wt%), Al 2 o 3 (20wt%), Li 2 O (4wt%), SrO (3wt%), MgO (3wt%), B 2 o 3 (0.5wt%), Na 2 O (0.5wt%), TiO 2 (2wt%), ZrO 2 (3wt%), Er 2 o 3 (3wt%), Bi 2 o 3 (1.5wt%), Co 2 o 3 (0.3wt%), Sb 2 o 3 (0.2 wt%). Correspondingly, the raw materials used are chemically pure chemical raw materials, corresponding to: silica, alumina powder, lithium carbonate, strontium carbonate, magnesium carbonate, boric acid, soda ash, titanium oxide, zirconia, erbium oxide, oxide Bismuth, cobalt trioxide and antimony trioxide.
[0030] b. Use the above-mentioned chemical raw materials for glass batching, including batching calculation, weighing, mixing and other processes.
[0031] c. Put the glass batch material into a corundum crucible and melt it in a silicon-molybdenum furnace with a temperature range of 1600°C for 5 hours. The molten glass is cast into a plate shape in a hot graphite mold, and then placed in a muffl...
Embodiment 3
[0036] a. The oxidation composition of the basic glass is: SiO 2 (64wt%), Al 2 o 3 (18wt%), Li 2 O (3wt%), SrO (3wt%), MgO (3wt%), B 2 o 3 (1wt%), Na 2 O (0.5wt%), TiO 2 (2.5wt%), ZrO 2 (2wt%), Er 2 o 3 (2wt%), Bi 2 o 3 (0.5wt%), Co 2 o 3 (0.2wt%), Sb 2 o 3 (0.3 wt%). Correspondingly, the raw materials used are chemically pure chemical raw materials, corresponding to: silica, alumina powder, lithium carbonate, strontium carbonate, magnesium carbonate, boric acid, soda ash, titanium oxide, zirconia, erbium oxide, oxide Bismuth, cobalt trioxide and antimony trioxide.
[0037] b. Use the above-mentioned chemical raw materials for glass batching, including batching calculation, weighing, mixing and other processes.
[0038] c. Put the glass batch material into a corundum crucible and melt it in a silicon-molybdenum furnace with a temperature range of 1620°C for 6 hours. The molten glass is cast into a plate shape in a hot graphite mold, and then placed in a muffl...
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