Production device special for manganese slag light tile additive, working method and manufacturing method of key parts of production device
A technology for production devices and additives, applied in chemical instruments and methods, mixers with rotary stirring devices, transportation and packaging, etc., can solve the problems of inaccurate monitoring of the production process, high labor intensity of workers, low production efficiency, etc. The effect of saving production time, high liquid mixing uniformity, and improving unit output
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Embodiment 1
[0055]Manufacture condensation plate 6-2 of the present invention according to the following steps, and by weight fraction:
[0056] Step 1: Add 267 parts of ultrapure water with a conductivity of 2.1μS / cm into the reactor, start the stirrer in the reactor at a speed of 185rpm, start the heating pump, and raise the temperature in the reactor to 42°C; add in sequence 60 parts of polymer of 1,2-propanediol and isononylphenyl ether, 38 parts of dimethyl-diacetoxysilane, 2-ethyl-2-(octanoyloxymethyl)-1,3-propanediol 75 parts of dicaprylic acid ester, stir until completely dissolved, adjust the pH value to 4.1, adjust the speed of the agitator to 201rpm, the temperature is 82°C, and the esterification reaction is 21 hours;
[0057] Step 2: Take 80 parts of ethyl-2-oxocyclopentane carboxylate and 95 parts of S-(α, α-dimethylbenzyl)piperidine-1-thiocarbamate and grind them into powder The diameter is 102 mesh; add 30 parts of cyclopentyltrimethoxysilane and mix evenly, spread it on ...
Embodiment 2
[0062] Manufacture condensation plate 6-2 of the present invention according to the following steps, and by weight fraction:
[0063] Step 1: Add 528 parts of ultrapure water with a conductivity of 2.8μS / cm into the reactor, start the stirrer in the reactor at a speed of 253rpm, start the heating pump, and raise the temperature in the reactor to 56°C; add in sequence 105 parts of polymer of 1,2-propanediol and isononylphenyl ether, 59 parts of dimethyl-diacetoxysilane, 2-ethyl-2-(octanoyloxymethyl)-1,3-propanediol 102 parts of dicaprylic acid ester, stir until completely dissolved, adjust the pH value to 6.2, adjust the speed of the agitator to 236rpm, the temperature is 157°C, and the esterification reaction is 30 hours;
[0064] Step 2: Take 116 parts of ethyl-2-oxocyclopentane carboxylate and 146 parts of S-(α, α-dimethylbenzyl)piperidine-1-thioformate and grind them into powder particles The diameter is 147 mesh; add 76 parts of cyclopentyltrimethoxysilane and mix evenly,...
Embodiment 3
[0069] Manufacture condensation plate 6-2 of the present invention according to the following steps, and by weight fraction:
[0070] Step 1: Add 759 parts of ultrapure water with a conductivity of 3.2μS / cm into the reactor, start the stirrer in the reactor at a speed of 324rpm, start the heating pump, and raise the temperature in the reactor to 63°C; add in sequence 150 parts of polymer of 1,2-propanediol and isononylphenyl ether, 85 parts of dimethyl-diacetoxysilane, 2-ethyl-2-(octanoyloxymethyl)-1,3-propanediol 128 parts of dicaprylic acid ester, stir until completely dissolved, adjust the pH value to 7.9, adjust the speed of the agitator to 268rpm, the temperature is 163°C, and the esterification reaction is 36 hours;
[0071] Step 2: Take 150 parts of ethyl-2-oxocyclopentane carboxylate and 198 parts of S-(α, α-dimethylbenzyl)piperidine-1-thioformate and grind them into powder particles The diameter is 196 mesh; add 112 parts of cyclopentyltrimethoxysilane and mix evenly...
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