Method for preparing porous ceramic heat-insulating material
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A thermal insulation material and porous ceramic technology, applied in the field of preparation of porous ceramic thermal insulation materials, can solve the problems of high density, great harm to human body, high thermal conductivity, etc., and achieve simple preparation process, low raw material cost and low thermal conductivity Effect
Inactive Publication Date: 2016-08-24
许智静
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The former itself consumes a lot of energy in the preparation process. Although the market price is relatively low, it has high density, high thermal conductivity, and general heat insulation effect; the latter has low density and low thermal conductivity, but has low strength and is easy to powder. Chemical, not resistant to erosion, greater harm to human body and other disadvantages
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[0011] The present invention will be described in detail below with specific examples.
[0012] A method for preparing a porous ceramic heat insulating material, comprising the steps of:
[0013] 1) Al 2 o 3 Calcined to Al 2 o 3 It is 99wt% powder, the powder particle diameter is 1.4μm, take 100gAl 2 o 3 powder, 80g chemically pure ammonium citrate, 100ml deionized water and Al 2 o 3 Put the balls together in a stirring mill and mill for 1 h, and the Al 2 o 3 Grinding balls filter out to obtain Al with a mass fraction of 75% 2 o 3 slurry;
[0014] 2) in Al 2 o 3 Add 30g of analytically pure acrylamide, 50g of chemically pure N,N'-methylenebisacrylamide, 50g of analytically pure ammonium persulfate into the slurry, and stir mechanically for 3-5min to dissolve it;
[0015] 3) Add 20 g of industrially pure triethanolamine dodecylsulfate to the solution, stir and foam vigorously, wait for volume expansion, then add 40 g of N, N, N', N'-tetramethylethylenediamine with...
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Abstract
The invention discloses a method for preparing a porous ceramic heat-insulating material and belongs to the technical field of heat insulating materials. The method comprises the steps: calcining Al2O3 so as to obtain powder, in which the content of Al2O3 is 99wt%, putting 100g of Al2O3 powder, 80g of ammonium citrate, 100ml of deionized water and Al2O3 milling balls into a stirring mill together, carrying out ball milling for 1 hour, and filtering out the Al2O3 milling balls, so as to obtain Al2O3 slurry with the mass percent of 75%; adding 30g of acrylamide, 50g of N,N'-methylene-bisacrylamide and 50g of ammonium persulfate into the Al2O3 slurry, and carrying out mechanical stirring so as to dissolve the acrylamide, the N,N'-methylene-bisacrylamide and the ammonium persulfate; adding 20g of triethanolamine lauryl sulfate into the solution, carrying out vigorous stirring foaming, adding N,N,N',N'-tetramethylethylenediamine into the solution until volume expansion is achieved, carrying out stirring for 30 seconds, injecting the mixture into a mold rapidly, and carrying out demolding after a blank is cured; and transferring the blank to a thermo-hygrostat and an air-blast drying oven for curing and drying, and carrying out sintering on the dried blank in a sintering furnace at the temperature of 1,700 DEG C while carrying out heat preservation for 3 hours. The porous ceramic heat-insulating material prepared by the method has the advantages of high strength, low density and low thermal conductivity.
Description
technical field [0001] The invention belongs to the technical field of heat insulating materials, and in particular relates to a preparation method of a porous ceramic heat insulating material. Background technique [0002] In the prior art, the heat insulation material used in high temperature industry is mainly Al 2 o 3 Hollow sphere products and Al 2 o 3 fiber products. The former itself consumes a lot of energy in the preparation process. Although the market price is relatively low, it has high density, high thermal conductivity, and general heat insulation effect; the latter has low density and low thermal conductivity, but has low strength and is easy to powder. Chemical, not resistant to erosion, greater harm to the human body and other shortcomings. Therefore, in response to the energy-saving and consumption-reducing requirements of high-temperature industrial development, there is an urgent need for a new type of thermal insulation material with high strength, ...
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