Pharmaceutical composition for treating gastroesophageal reflux diseases and its preparation method and use
A technology of gastroesophageal reflux and composition, which is applied in the field of medicine, can solve the problems of high recurrence rate, long-term medication, high treatment costs, etc., and achieve the effect of low recurrence rate, no toxic and side effects, and significant curative effect
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Embodiment 1
[0015] Example 1 Preparation of Periplaneta americana Extract by Organic Solvent Extraction
[0016] Coarsely crush 100kg of dried Periplaneta americana, add 4 times the amount of 70% ethanol, soak for 1 hour, and extract twice at 70°C for 8 hours for the first time; add 3 times the amount of ethanol for the second time, extract for 6 hours and combine Secondary extract, filter, and concentrate the green leaves to a clear paste with a relative density of 1.09-1.16 (70°C), add water, keep stirring at 70°C for 60 minutes, let stand for 12 hours, discard the upper layer of grease, filter the lower layer of liquid medicine, The ethanol was recovered from the filtrate, concentrated under reduced pressure to a medicinal solution (70°C) with a relative density of 1.16-1.22, and dried to obtain the Periplaneta americana extract.
Embodiment 2
[0017] Example 2 Preparation of Periplaneta americana Extract by Flash Extraction
[0018] Get Periplaneta americana coarse powder 100g, the mass volume ratio of Periplaneta americana coarse powder and water is 25:12, extract 3 times under the condition of voltage 80 volts, each time 3 minutes, the medicinal liquid that extracts is in 4000r / min. Centrifuge under the conditions for 30 minutes, filter, combine the filtrates, pre-freeze for 24 hours, and freeze-dry in a freeze dryer for 48 hours to obtain the Periplaneta americana extract.
Embodiment 3
[0019] Example 3 Preparation of Liquid Dosages
[0020] Weigh 20g of glutamic acid, 30g of arginine, and 50g of the Periplaneta americana extract prepared in Example 1, dissolve in an appropriate amount of water for injection, then add 2g of potassium sorbate and 50ml of glycerin, mix well, and add water for injection to 1000ml , adjust the pH value to 6.5-7.5, filter, pot, sterilize at 115°C for 30 minutes, pack, and get ready.
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