Sustained-release antioxidant food packaging film and method for preparing same
An oxidative food and sustained-release technology, which is used in the field of antioxidant active food packaging materials and the preparation of sustained-release antioxidant films, can solve the problem of reducing the release rate, prolonging the action time of antioxidants, and releasing too fast active substances with sustained-release effects, etc. problems, to achieve the effect of prolonging the action time, prolonging the shelf life, and widening the scope of application
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Embodiment 1
[0018] Present embodiment packaging film preparation steps are as follows:
[0019] (1) Dissolve 4.308g of α-tocopherol in 40mL of ethanol, add 2g of MCM-41 to the solution, stir magnetically at room temperature for 3 hours and then filter it with a sand core funnel, and dry the obtained solid in a vacuum oven at 35°C overnight to obtain Assembly.
[0020] (2) Weigh 2g of the assembly obtained in step 1), mix it evenly with 200g of LDPE masterbatch, add it to the feed hopper of a twin-screw extrusion granulator preheated at 175°C, set the screw speed to 60rpm, and granulate .
[0021] (3) Pour the blended masterbatch prepared in step (2) into the feed hopper of a single-screw extrusion casting machine preheated at 175° C., and set the screw speed at 30 rpm to prepare a film. The prepared films were stored away from light and vacuum-sealed until sampling and testing.
Embodiment 2
[0023] Present embodiment packaging film preparation steps are as follows:
[0024] (1) Dissolve 2.58g of α-tocopherol in 20mL of ethanol, add 2g of MCM-41 to the solution, stir magnetically at room temperature for 3 hours, then filter it with a sand core funnel, and dry the obtained solid in a vacuum oven at 35°C overnight to obtain Assembly.
[0025] (2) Weigh 1g of the assembly obtained in step 1), mix it evenly with 200g of LDPE masterbatch, add it to the feed hopper of a twin-screw extrusion granulator preheated at 175°C, set the screw speed to 60rpm, and granulate .
[0026] (3) Pour the blended masterbatch prepared in step (2) into the feed hopper of a single-screw extrusion casting machine preheated at 175° C., and set the screw speed at 30 rpm to prepare a film. The prepared films were stored away from light and vacuum-sealed until sampling and testing.
Embodiment 3
[0028] Present embodiment packaging film preparation steps are as follows:
[0029] (1) Dissolve 2.58g of α-tocopherol in 20mL of ethanol, add 2g of MCM-41 to the solution, stir magnetically at room temperature for 3 hours, then filter it with a sand core funnel, and dry the obtained solid in a vacuum oven at 35°C overnight to obtain Assembly.
[0030] (2) Weigh 1g of the assembly obtained in step 1), mix it evenly with 200g of polypropylene masterbatch, add it to the feed hopper of a twin-screw extrusion granulator preheated at 230°C, set the screw speed to 60rpm, Granulate.
[0031] (3) Pour the blended masterbatch prepared in step (2) into the feed hopper of a single-screw extrusion casting machine preheated at 230° C. and set the screw speed at 30 rpm to prepare a film. The prepared films were stored away from light and vacuum-sealed until sampling and testing.
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