Method and equipment for preparing ultralow-loss optical fiber perform with fluorine-doped pure silicon core cladding

An optical fiber preform and core wrap technology, applied in glass manufacturing equipment, manufacturing tools, glass deposition furnaces, etc., can solve the problems of unfavorable refractive index profile, unfavorable dehydration of loose bodies, and high optical fiber water peaks

Active Publication Date: 2016-10-12
ZHONGTIAN TECH ADVANCED MATERIALS CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in actual production, due to the structure of the dense layer, if the density is high, it is not conducive to the dehydration of the loose body, resulting in a high water peak in the optical fiber; if the density is low, the doped fluorine element still penetrates into the core layer, which is not conducive to the formation of stages refractive index profile
If the pure silicon core rod and the F-doped cladding sleeve are separately produced and re-melted in the manufacturing process, the complexity of the process will also be greatly increased.

Method used

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  • Method and equipment for preparing ultralow-loss optical fiber perform with fluorine-doped pure silicon core cladding
  • Method and equipment for preparing ultralow-loss optical fiber perform with fluorine-doped pure silicon core cladding
  • Method and equipment for preparing ultralow-loss optical fiber perform with fluorine-doped pure silicon core cladding

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0062] Example 1: Manufacturing Φ200mm×1600mm pure silicon core cladding fluorine-doped ultra-low loss optical fiber preform

[0063] (1) The material made of quartz glass is selected as the deposition target rod. Pickle the selected target rods, soak them in 10% hydrochloric acid for 1 hour to remove impurities attached to the surface of the target rods, then rinse them repeatedly with deionized water, and finally dry them.

[0064] (2) Clamp the pretreated target rod on the boom hook of the VAD equipment. The mixture of silicon tetrachloride, oxygen, carbon monoxide, helium and nitrogen is used as raw material gas, and the flow rates of various raw material gases are 5g / min, 7.5L / min, 5L / min, 5L / min, 1.5L / min After the core layer of quartz material is injected into the blowtorch, the silicon dioxide particles generated by the high-temperature reaction of the raw materials in the flame are deposited on the surface of the target rod perpendicular to the blowtorch. Above the ...

Embodiment 2

[0067] Example 2: Manufacturing Φ200mm×1600mm pure silicon core cladding fluorine-doped ultra-low loss optical fiber preform

[0068] (1) The material made of quartz glass is selected as the deposition target rod. Pickle the selected target rods, soak them in 10% hydrochloric acid for 1.5 hours to remove impurities attached to the surface of the target rods, then rinse them repeatedly with deionized water, and finally dry them.

[0069] (2) Clamp the pretreated target rod on the boom hook of the VAD equipment. The mixture of silicon tetrachloride, oxygen, carbon monoxide, helium and nitrogen is used as the raw material gas. After the core layer of quartz material is torched, the silicon dioxide particles generated by the high-temperature reaction of the raw materials in the flame are deposited on the surface of the target rod perpendicular to the torch. Above the core layer, configure 3 auxiliary blowtorches with a Ɵ of 120°. Carbon monoxide and oxygen are injected into each...

Embodiment 3

[0072] Example 3: Manufacturing Φ200mm×1600mm pure silicon core cladding fluorine-doped ultra-low loss optical fiber preform

[0073] (1) The material made of quartz glass is selected as the deposition target rod. Pickle the selected target rods, soak them in 10% hydrochloric acid for 2 hours to remove impurities attached to the surface of the target rods, then rinse them repeatedly with deionized water, and finally dry them.

[0074](2) Clamp the pretreated target rod on the boom hook of the VAD equipment. The mixture of silicon tetrachloride, oxygen, carbon monoxide, helium and nitrogen is used as the raw material gas, the flow rates of various raw material gases are 5g / min, 15L / min, 15L / min, 5L / min, 2.5L / min After the core layer of quartz material is torched, the silicon dioxide particles generated by the high-temperature reaction of the raw materials in the flame are deposited on the surface of the target rod perpendicular to the torch. On the top of the core layer, 5 au...

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Abstract

The invention discloses a method and equipment for preparing an ultralow-loss optical fiber perform with a fluorine-doped pure silicon core cladding, and relates to a method for preparing the ultralow-loss optical fiber perform with the fluorine-doped pure silicon core cladding by doping fluorine in the cladding through powder obtained according to a vapor deposition method. The equipment comprises a target bar, a deposition chamber, an outer-cladding blow lamp, a middle-cladding blow lamp, an auxiliary blow lamp, a core layer blow lamp, a suspension rod, an exhaust pipe, an upper deposition cavity and a graphite heating resistance furnace. The upper deposition cavity is formed in the upper portion of the deposition chamber. The suspension rod is mounted in the upper deposition cavity, is provided with a hook and is connected with a lifting mechanism. The target bar is hung on the hook of the suspension rod connected with the lifting mechanism. The outer-cladding blow lamp, the middle-cladding blow lamp, the auxiliary blow lamp and the core layer blow lamp are mounted on one side of the lower portion of the disposition chamber sequentially. A graphite sintering furnace comprises a quartz suspension rod, a sealing component, a cover plate, a quartz furnace core tube, a graphite furnace core tube, a gas pipeline, a target bar, a powder body, a graphite heating body and a gas quality and flow controller.

Description

technical field [0001] The invention relates to a method and equipment for preparing a pure silicon core cladding fluorine-doped ultra-low loss optical fiber preform, which relates to a powder body obtained by vapor deposition method, and the cladding is doped with fluorine to prepare a pure silicon core A method for cladding a fluorine-doped ultra-low loss optical fiber preform. Background technique [0002] An optical fiber preform is the raw material for optical fiber manufacturing, and it usually consists of a core layer and a cladding layer made of materials with different refractive indices. Silica is the main matrix material for manufacturing optical fiber preforms, and the refractive index of the core layer is increased by doping germanium in the core layer n core , so that the core refractive index is greater than the pure silicon cladding refractive index n siO2 , so as to meet the total reflection condition of optical fiber transmission, that is, to achieve a ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03B37/014
CPCC03B37/01453C03B2207/28C03B2207/38C03B2207/50
Inventor 吴椿烽沈一春钱宜刚
Owner ZHONGTIAN TECH ADVANCED MATERIALS CO LTD
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