A method and equipment for preparing ultra-low loss optical fiber preform rod with pure silicon core cladding doped with fluorine
An optical fiber preform and core-packing technology, which is applied in glass manufacturing equipment, manufacturing tools, glass deposition furnaces, etc., can solve problems such as unfavorable refractive index profile, unfavorable loose body dehydration, and high water peak of optical fiber
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Embodiment 1
[0062] Example 1: Manufacturing Φ200mm×1600mm pure silicon core cladding fluorine-doped ultra-low loss optical fiber preform
[0063] (1) Use quartz glass material as the deposition target. The selected target rod is pickled, soaked in 10% hydrochloric acid for 1 hour to remove impurities attached to the surface of the target rod, then rinsed repeatedly with deionized water, and finally dried.
[0064] (2) Clamp the pre-processed target rod on the hanger of the VAD equipment. Using silicon tetrachloride, oxygen, carbon monoxide, helium and nitrogen mixture as raw material gas, the flow rate of each raw material gas is 5g / min, 7.5L / min, 5L / min, 5L / min, 1.5L / min, After entering the quartz core layer torch, the silicon dioxide particles generated by the high-temperature reaction of the raw material in the flame are deposited on the surface of the target rod perpendicular to the torch. Above the core layer, two auxiliary blowtorches are arranged perpendicular to each other, and carbo...
Embodiment 2
[0067] Example 2: Manufacturing Φ200mm×1600mm pure silicon core cladding fluorine-doped ultra-low loss optical fiber preform
[0068] (1) Use quartz glass material as the deposition target. The selected target rod is pickled and soaked in 10% hydrochloric acid for 1.5 hours to remove impurities attached to the surface of the target rod, then rinsed repeatedly with deionized water, and finally dried.
[0069] (2) Clamp the pre-processed target rod on the hanger of the VAD equipment. Using silicon tetrachloride, oxygen, carbon monoxide, helium and nitrogen mixture as raw materials, the flow rates of each raw material gas are 5g / min, 11.3L / min, 10L / min, 5L / min, 2L / min, and pass in After the quartz core layer torch, the silicon dioxide particles generated by the high-temperature reaction of the raw material in the flame are deposited on the surface of the target rod perpendicular to the torch. Above the core layer, three auxiliary blowtorches are arranged with a value of 120°. Carbon...
Embodiment 3
[0072] Example 3: Manufacturing Φ200mm×1600mm pure silicon core cladding fluorine-doped ultra-low loss optical fiber preform
[0073] (1) Use quartz glass material as the deposition target. The selected target rod is pickled, soaked in 10% hydrochloric acid for 2 hours to remove impurities attached to the surface of the target rod, then rinsed repeatedly with deionized water, and finally dried.
[0074] (2) Clamp the pre-processed target rod on the hanger of the VAD equipment. Using silicon tetrachloride, oxygen, carbon monoxide, helium and nitrogen mixture as raw materials, the flow rates of various raw materials are 5g / min, 15L / min, 15L / min, 5L / min, 2.5L / min, and pass through After the quartz core layer torch, the silicon dioxide particles generated by the high-temperature reaction of the raw material in the flame are deposited on the surface of the target rod perpendicular to the torch. Above the core layer, there are 5 auxiliary blowtorches with a Ɵ of 72°. Each blowtorch is ...
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