Preparation method of olive microcapsule

A technology of olive microcapsules and olives, which is applied in the field of microcapsules, can solve the problems of loss of activity, rapid oxidation and deterioration, insoluble in water, etc., and achieve the effects of strong antioxidant capacity, high yield and low cost

Inactive Publication Date: 2016-10-26
仇颖莹
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The main technical problem to be solved by the present invention is to provide a preparation method of olive microcapsules in view of the fact that various active components of olives will be rapidly oxidized and deteriorated in the air, and then lose their activity, and that various active components of olives are insoluble in water. In the present invention, the olive fruit is firstly boiled, mashed and homogenized, and then cellulase and pectinase are added to the olive pulp for enzymolysis to obtain the enzymolysis solution, which is sterilized, purified and spray-dried to obtain olive powder, which is mixed with ethyl acetate Mix and set aside, then extract monoglyceride from olive oil as an emulsifier, use maltodextrin and gum arabic as wall materials, and prepare a microcapsule emulsion from the spare olive mixture as a core material, and finally solidify to obtain microcapsules. The operation steps of the invention are simple and will not destroy the active ingredients of the olive extract, and the prepared microcapsules have high embedding yield, high stability, strong anti-oxidation ability and good solubility, and the preparation raw materials are safe, non-toxic and low in cost

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0019] First, select 200g of olive fruit, remove the core and put it into clear water to boil for 5 minutes, put the boiled olives into a stone mortar and manually grind and mash them for 20 minutes, then stir and homogenize them with a homogenizer for 10 minutes to obtain olive pulp, and add to the olive pulp The total mass of 1% compound enzyme was enzymatically hydrolyzed at 40°C for 8 hours. After the enzymolysis was completed, the enzyme was inactivated at a power of 500W for 5s. Evaporate and concentrate under MPa for 30min to obtain a concentrated solution; the compound enzyme is a mixture of cellulase and pectinase in a mass ratio of 2:1; the above-mentioned concentrated solution is adsorbed by a macroporous resin, and the mass fraction is 55% after adsorption. Desorb with ethanol solution, collect the desorption solution, evaporate and concentrate the desorption solution at 70°C for 1 hour to obtain a concentrated solution, spray dry to obtain olive powder, stir and mi...

example 2

[0022]First, select 225g of olive fruit, remove the core and put it into clean water to boil for 6 minutes. Put the boiled olives into a stone mortar and grind them manually for 23 minutes. Stir and homogenize them with a homogenizer for 15 minutes to obtain olive pulp. Add to the olive pulp The total mass of 2% compound enzyme was enzymolyzed at 45°C for 9 hours. After the end of enzymolysis, the enzyme was deactivated at a power of 550W for 10s. Evaporate and concentrate under MPa for 35 minutes to obtain a concentrated solution; the compound enzyme is a mixture of cellulase and pectinase in a mass ratio of 2:1; the above-mentioned concentrated solution is adsorbed by a macroporous resin, and the mass fraction is 55% after adsorption. Desorb with ethanol solution, collect the desorption solution, evaporate and concentrate the desorption solution at 80°C for 1.5h to obtain a concentrated solution, spray dry to obtain olive powder, stir and mix the olive powder with ethyl aceta...

example 3

[0025] First, select 250g of olive fruit, remove the core and put it into clean water to boil for 8 minutes, put the boiled olives into a stone mortar and manually grind and mash them for 25 minutes, then stir and homogenize them with a homogenizer for 20 minutes to obtain olive pulp, and add them to the olive pulp The total mass of 3% compound enzyme was enzymatically hydrolyzed at 50°C for 10 hours. After the enzymolysis was completed, the enzyme was deactivated at a power of 600W for 15s. Evaporate and concentrate under MPa for 40min to obtain a concentrated solution; the compound enzyme is a mixture of cellulase and pectinase in a mass ratio of 2:1; the above-mentioned concentrated solution is adsorbed by a macroporous resin, and the mass fraction is 55% after adsorption. Desorb with ethanol solution, collect the desorption solution, evaporate and concentrate the desorption solution at 90°C for 2 hours to obtain a concentrated solution, spray dry to obtain olive powder, sti...

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Abstract

The invention discloses a preparation method of olive microcapsules, belonging to the field of microcapsules. In the present invention, the olive fruit is firstly boiled, mashed and homogenized, and then cellulase and pectinase are added to the olive pulp for enzymolysis to obtain the enzymolysis solution, which is sterilized, purified and spray-dried to obtain olive powder, which is mixed with ethyl acetate Mix and set aside, then extract monoglyceride from olive oil as an emulsifier, use maltodextrin and gum arabic as wall materials, and prepare a microcapsule emulsion from the spare olive mixture as a core material, and finally solidify to obtain microcapsules. The invention has simple operation steps, does not destroy the active ingredients of the olive extract, and the prepared microcapsules have a high embedding yield of more than 95%, high stability and strong anti-oxidation ability, and the preparation raw materials are safe, non-toxic and low in cost.

Description

technical field [0001] The invention discloses a preparation method of olive microcapsules, belonging to the field of microcapsules. Background technique [0002] Olive fruit is a drupe with high edible and medicinal value. The development and utilization of olive resources in my country is mainly concentrated on the fruit and branches and leaves, especially the processing and utilization of the fruit. At present, olives are generally processed into various products such as candied fruit, candied fruit and juice drinks. Olive contains a variety of active ingredients, which can effectively reduce "bad" cholesterol and increase "good" cholesterol. However, olive oil is insoluble in water, and it is not easy to mix evenly with food materials. It is extremely inconvenient for industrial use. Its active ingredients are unstable and easy to oxidize. [0003] The functions of microencapsulation mainly include: (1) to improve the physical properties of substances, liquid substance...

Claims

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Application Information

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IPC IPC(8): A23L19/00A23L33/00A23P10/30
CPCA23V2002/00
Inventor 仇颖莹王统军
Owner 仇颖莹
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