Preparation method and application of okra extract for treating kidney deficiency
The technology of extract and okra tender fruit is applied in the field of preparation of okra extract, and achieves the effects of improving immunity, definite and reliable curative effect, and simple production process
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Embodiment 1
[0014] The preparation method of the okra extract for treating kidney deficiency of the present invention comprises cleaning and removing impurities of 30 g of okra tender fruit, chopping and drying, and sequentially using 10 times, 8 times and 6 times of the weight of the material to extract by reflux of ethanol with a mass concentration of 50%. Extract 3 times for 3 hours each time, filter and combine the extracts, and concentrate to obtain 1200 g of total okra extract; disperse with water twice the weight of the total okra extract to obtain a dispersion, and then use 2 times the volume of the dispersion to boil at 60°C Petroleum ether, ethyl acetate, and n-butanol sequentially extract the dispersion, each solvent extracts 3 times, combine the extracts, concentrate and recover the solvent, and obtain 100 g of petroleum ether, 290 g of ethyl acetate, and 290 g of ethyl acetate extracted from the total okra extract respectively. 110g of the n-butanol part, and 670g of the remai...
Embodiment 2
[0016] The preparation method of the okra extract for treating kidney deficiency of the present invention comprises washing and removing 4.7 kg of dried okra fruit pods, chopping them up, and then using 8 times, 7 times, and 6 times the weight of the materials in turn to reflux and extract them with ethanol with a mass concentration of 95%. 3 times, extracting for 2 hours each time, filtering and combining the extracts, and concentrating to obtain the total okra extract; disperse with water that is 1 times the weight of the total okra extract to obtain a dispersion, and then use the same volume of the dispersion as petroleum oil with a boiling range of 90°C Ether, ethyl acetate, n-butanol sequentially extract the dispersion, each solvent is extracted 5 times, the extracts are combined, the solvent is concentrated and recovered, and 42.4g of petroleum ether, 35g of ethyl acetate, and n-butanol extracted from the total okra extract are obtained respectively 51g of the butanol par...
Embodiment 3
[0018] The preparation method of the okra extract for treating kidney deficiency of the present invention comprises washing and removing impurities from the tender okra fruit, chopping and drying, and then using 9 times, 8 times, and 6 times the weight of the material to reflux and extract 3 Each time, extract for 1 hour, filter and combine the extracts, and concentrate to obtain the total okra extract; disperse with 1.5 times the weight of the total okra extract in water to obtain a dispersion, and then use 1.5 times the volume of the dispersion to obtain the oil with a boiling range of 80 ° C. Ether, ethyl acetate, and n-butanol extract the dispersion in sequence, each solvent extracts 4 times, combine the extracts, concentrate and recover the solvent, and obtain the petroleum ether part, ethyl acetate part, and n-butanol part of the okra total extract respectively. , and the remaining water-soluble part after n-butanol extraction; collect the ethyl acetate part and the water...
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