Preparation method of anticorrosive coating
An anti-corrosion coating and ultrasonic stirring technology, which is applied in anti-corrosion coatings, anti-fouling/underwater coatings, epoxy resin coatings, etc., can solve the problems of single coating function and difficulty in achieving the effect, and achieve good antibacterial effect, improved effect, and excellent Effect of anti-formaldehyde properties
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Embodiment 1
[0029] A kind of preparation method of porous graphene loaded silver / titanium dioxide antibacterial composite material, it comprises the following steps:
[0030] (1) Preparation of graphene quantum dot suspension: weigh 0.5g of C60 powder, measure 100ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, put the beaker in an ice-water bath, and simultaneously Stir at a speed of 500rpm to obtain a mixed solution; weigh 3g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30-40°C, and react for 5 hours; quickly add 200ml of pure Water, filtered, and then dialyzed for 3 days with a dialysis bag with a molecular weight cut-off of 1000 to obtain a suspension of graphene quantum dots; the suspension of graphene quantum dots was stirred at a speed of 100 rpm, while laser irradiation was p...
Embodiment 2
[0037] A kind of preparation method of porous graphene loaded silver / titanium dioxide antibacterial composite material, it comprises the following steps:
[0038] (1) Preparation of graphene quantum dot suspension: weigh 0.6g of C60 powder, measure 50-100ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, put the beaker in an ice-water bath, At the same time, stir at a speed of 500rpm to obtain a mixed solution; weigh 1g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30~40°C, and react for 7 hours; quickly add 200ml of pure water, filtered, and then dialyzed with a dialysis bag with a molecular weight cut-off of 1000 for 3 days to obtain a suspension of graphene quantum dots; stir the suspension of graphene quantum dots at a speed of 100rpm, and irradiate the laser for 45min a...
Embodiment 3
[0045] A kind of preparation method of porous graphene loaded silver / titanium dioxide antibacterial composite material, it comprises the following steps:
[0046] (1) Preparation of graphene quantum dot suspension: Weigh 0.8g of C60 powder, measure 100ml of concentrated sulfuric acid with a mass fraction of 98%, mix C60 powder and concentrated sulfuric acid in a beaker, put the beaker in an ice-water bath, and simultaneously Stir at a speed of 500rpm to obtain a mixed solution; weigh 0.5g of potassium permanganate powder, and slowly add it to the above mixed solution; remove the ice-water bath and replace it with a water bath, keep the temperature of the water bath at 30-40°C, and react for 8 hours; quickly add 100ml Pure water, filtered, and then dialyzed for 3 days with a dialysis bag with a molecular weight cut-off of 1000, to obtain a suspension of graphene quantum dots; the suspension of graphene quantum dots was stirred at a speed of 100 rpm, while laser irradiation was p...
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