Preparation method of soldering paste for laser reflow soldering
A reflow soldering and solder paste technology, applied in welding equipment, welding media, manufacturing tools, etc., can solve problems such as vulnerability, product quality, splashing, affecting work efficiency, etc., to avoid local high temperature, concise process steps, The effect of improving thermal conductivity
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Embodiment 1
[0023] A) To prepare the intermediate, first put 2% triethylene glycol butyl ether and 2% 2-ethyl-2,6-pentanediol into a container equipped with a heater and a stirring device, Then the mass % ratio is 4.5% film forming agent KE604 and the mass % ratio is 2% succinic acid, 2% adipic acid and 0.1% glutaric acid are dropped into the container and heated and stirred, so that the KE604, succinic acid, adipic acid and glutaric acid are fully dissolved in triethylene glycol butyl ether and 2-ethyl-2,6-pentanediol, and the heating temperature of the heater is 170°C to obtain intermediate body;
[0024] B) To prepare the mixture, add flaky silver powder with a mass % ratio of 3% and a particle size of 1-10 μm, hydrogenated castor oil (HCO) with a mass % ratio of 0.5% and ethylene bis-stearin of 0.5% The acid amide (EBS) is slowly added to the intermediate obtained in step A) and placed in a constant temperature magnetic dispersion stirrer in a water bath for dispersion and stirring. ...
Embodiment 2
[0027] A) To prepare the intermediate, first put 2% triethylene glycol butyl ether, 1% 2-ethyl-2,6-pentanediol and 1% tetrahydrofurfuryl alcohol into the heater equipped with And in the container of the stirring device, the film-forming agent KE604 and the mass % ratio of 0.25% succinic acid, 0.25% adipic acid, 0.25% glutaric acid and 0.25% Cyclohexylamine hydrobromide is put into the container and heated and stirred, and described KE604, succinic acid, adipic acid, glutaric acid and cyclohexylamine hydrobromide are fully dissolved in triethylene glycol butyl ether, 2 - In ethyl-2,6-pentanediol and tetrahydrofurfuryl alcohol, the heating temperature of the heater is 190°C to obtain the intermediate;
[0028] B) To prepare the mixture, the flake silver powder with a mass % ratio of 2% and a particle size of 1-10 μm, hydrogenated castor oil (HCO) with a mass % ratio of 0.25%, and 0.25% ethylene bis-stearin The acid amide (EBS) is slowly added to the constant temperature magneti...
Embodiment 3
[0031] A) To prepare the intermediate, first put 2% triethylene glycol butyl ether and 2% tetrahydrofurfuryl alcohol into a container equipped with a heater and a stirring device, and then put 3% The film-forming agent KE604 and mass % ratio are 0.1% succinic acid, 0.1% adipic acid and 0.3% glutaric acid and put them into the container for heating and stirring, so that the KE604, succinic acid, adipic acid And glutaric acid is fully dissolved in triethylene glycol butyl ether and tetrahydrofurfuryl alcohol, and the heating temperature of the heater is 180°C to obtain the intermediate;
[0032] B) To prepare the mixture, add flaky silver powder with a mass % ratio of 4% and a particle size of 1-10 μm, hydrogenated castor oil (HCO) with a mass % ratio of 0.4%, and 0.1% ethylene bis-stearic acid Add amide (EBS) slowly to the constant temperature magnetic dispersing stirrer containing the intermediate obtained in step A) and place it in a water bath for dispersing and stirring. Th...
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