Liquid compositions and antibacterial articles
A technology of antibacterial active substances and compositions, applied in the field of antibacterial articles with ultraviolet absorbing ability, can solve the problems of unknown glass and the like
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[0240] Hereinafter, the present invention will be specifically described by examples, but the present invention is not limited by these examples. In addition, Examples 1 to 3, 5 to 12, 14 to 19 are examples, Examples 4, 13 are comparative examples.
[0241] Compounds used in the preparation of each membrane formation composition in each membrane formation, etc. are exemplified below.
[0242]
[0243] · Sili-based ultraviolet absorber solution: Add 2, 2 ', 4,4'-tetrahydroxybenzophenone (BASF system) 49.2 g, 3-cyclopproxpropyl trimethoxysilane (believe in Chemical company system) 123.2g, benzyl tetraethyl (pure chemical company) 0.8g, butyl acetate (pure chemical company system) 100g, while stirring while temperatureing to 60 ° C to dissolve, heating to 120 The reaction was reacted for 4 hours, thereby obtaining 4- [2-hydroxy-3- [3- (trimethoxysilyl) propoxy] propoxy] -2, 2 'of the ultraviolet absorber. 4'-trihydroxybenzophenone solid component concentration of 63% by mass of meth...
example 1
[0273] Add a silylating ultraviolet absorber 12.8 g, tetraethoxysilane 15.3g, SiO 2 Particle dispersion 0.7 g, Solmix AP-1 50.6 g, pure water 19.5 g, SR-SEP 1.1G, maleic acid 0.116g, Nonpol PMA-50W0.081G, BYK307 0.060 g, stirred at 50 ° C for 2 hours, added 1% by mass concentration of nitrite solution 0.1 g, resulting in an antibacterial membrane forming coating liquid having ultraviolet absorption capability (0.01% by mass of the silver content in the solid component of the coating liquid 1).
[0274] Then, a high-thermal radiation absorbing green glass (Asahi-branch system, generally known as UVFL) is applied to the gas, in the atmosphere, in the atmosphere It was dried at 200 ° C for 30 minutes to obtain a glass plate 1 with an antibacterial membrane having ultraviolet absorption capacity.
example 2
[0276] The 1% by mass concentration of nitrogen solution was 0.7 g, and the pure water was 19.0 g, except that the same operation as described in Example 1 was obtained, and the coating liquid having ultraviolet absorbent capacity was obtained. 2 (the coating liquid) The silver content in the solid component of 2 is 0.05% by mass). Further, the antibacterial membrane forming coating liquid 1 is formed of an antibacterial film to form a coating liquid 2, except that the same operation as in Example 1 is obtained, and a glass plate 2 having ultraviolet absorbing ability is obtained.
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