A kind of segregation bleeding inhibitor for cement concrete and preparation method thereof
A technology of cement concrete and inhibitor, which is applied in the field of cement concrete admixtures in building materials, can solve problems such as poor workability, and achieve the effects of improving work performance and durability, good benefits, and improved workability
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Embodiment 1
[0027] The preparation method of the segregation bleeding inhibitor for cement concrete of the present invention, the steps are:
[0028] (1) In parts by weight (unit: gram), take respectively 0.05 parts of initiator ammonium persulfate, 5 parts of alkali, 18 parts of acrylic acid, and 40 parts of water, and add them together to a tank equipped with a thermometer, a stirrer and a dropping device. In a four-neck flask, stir evenly;
[0029] (2) In parts by weight (unit: gram), take concentration respectively and be 1.4 parts of 5% hydrogen peroxide as oxidant, 1.0 part of reducing agent vitamin C and 0.006 part of chain transfer agent mercaptopropionic acid, add dropwise to step (1) ) in the prepared solution, control the reaction for 1.2 hours to obtain a solution that generates sodium polyacrylate with large molecular weight;
[0030] (3) In parts by weight (unit: gram), respectively weigh 5 parts of acrylic acid, 4 parts of acrylamide, and 23 parts of water, and then add th...
Embodiment 2
[0038] (1) In parts by weight (unit: gram), weigh 0.05 parts of initiator sodium bisulfite, 5 parts of alkali, 18 parts of acrylic acid, and 40 parts of water, and add them together to the In a four-neck flask, stir evenly;
[0039] (2) In parts by weight (unit: gram), take 1.6 parts of potassium permanganate as an oxidizing agent, 1.2 parts of reducing agent vitamin C and 0.008 part of chain transfer agent mercaptopropionic acid, and add them dropwise to step (1) In the prepared solution, the reaction was controlled for 1.5 hours to obtain a solution that generated sodium polyacrylate with large molecular weight;
[0040] (3) In parts by weight (unit: gram), weigh 5 parts of acrylic acid, 5 parts of acrylamide, and 23 parts of water, and then add them together to the solution prepared in step (2), and continue to react for 5 hours. Let stand for 1 hour;
[0041] (4) Add alkali to the solution prepared in step (3), adjust the pH value of the solution to 7.2, and obtain the p...
Embodiment 3
[0043] The preparation method of the segregation bleeding inhibitor for cement concrete of the present invention, the steps are:
[0044] (1) In parts by weight (unit: gram), take respectively 0.05 parts of initiator ammonium persulfate, 5 parts of alkali, 20 parts of acrylic acid, and 40 parts of water, and add them together to a tank equipped with a thermometer, a stirrer and a dropping device. In a four-neck flask, stir evenly;
[0045](2) In parts by weight (unit: gram), take concentration respectively and be 1.5 parts of 5% hydrogen peroxide as oxidizing agent, 1.1 parts of reducing agent vitamin C and 0.005 part of chain transfer agent mercaptopropionic acid, add dropwise to step (1) ) in the prepared solution, control reaction 1 hour, obtain the solution that generates the sodium polyacrylate with large molecular weight;
[0046] (3) In parts by weight (unit: gram), weigh 5 parts of acrylic acid, 3 parts of acrylamide, and 23 parts of water, and add them to the solutio...
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