Highly efficient composite concrete anti-freezing agent and preparation method thereof

A concrete and composite technology, which is applied in the field of concrete antifreeze, can solve the problems that the real air content of concrete is difficult to design or control, it is difficult to achieve frost resistance, and the strength of concrete is reduced, so as to achieve good antifreeze effect, low production cost, and high The effect of early strength

Inactive Publication Date: 2017-02-15
四会市恒星智能科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the above-mentioned air-entraining antifreeze agents can effectively improve the frost resistance of concrete, the tiny air bubbles introduced by them will inevitably be lost during the process of mixing, transportation and pouring, which is the so-called air content damage problem.
The loss of air content makes it difficult to design or control the real air content of hardened concrete. If the real air content of concrete is too high, the strength of concrete will be reduced; if the air content is too low, it will be difficult to achieve the expected frost resistance.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A preparation method of an efficient composite concrete antifreeze agent, comprising the following steps:

[0019] (1) Warm up 60 parts of water to 60°C, stir evenly, add 6 parts of β-naphthalenesulfonate formaldehyde condensate, 5 parts of glucose laurate, 3 parts of sodium N-lauroyl sarcosinate, and continue stirring for 15 ~30min to get the mixed system A;

[0020] (2) Reduce the temperature of the mixed system A to 40°C, and add 30 parts of lignosulfonate, 20 parts of sodium sulfate, 20 parts of silicate, 8 parts of ammonium chloride, and 8 parts of triethanolamine under stirring conditions, After mixing evenly, put it in an oven and bake at 80°C for 30 minutes to obtain the mixed system B;

[0021] (3) Add 10 parts of propanol and 15 parts of isopropanol to the mixing system B, grind for 20-30 minutes, then add 0.1 part of sodium carbonate and 0.1 part of caustic soda to adjust the pH to 12-13.

Embodiment 2

[0023] A preparation method of an efficient composite concrete antifreeze agent, comprising the following steps:

[0024] (1) Warm up 80 parts of water to 80°C, stir evenly, add 8 parts of β-naphthalenesulfonate formaldehyde condensate, 3 parts of glucose laurate, 3 parts of sodium N-lauroyl sarcosinate, and continue stirring for 15 ~30min to get the mixed system A;

[0025] (2) Reduce the temperature of the mixed system A to 40°C, and add 32 parts of lignosulfonate, 25 parts of sodium sulfate, 18 parts of silicate, 6 parts of ammonium chloride, and 10 parts of triethanolamine under stirring conditions, After mixing evenly, put it in an oven and bake at 80°C for 35 minutes to obtain the mixed system B;

[0026] (3) Add 15 parts of ethylene glycol and 5 parts of ethanol to the mixing system B, grind for 20-30 minutes, then add 0.2 part of lime and 0.1 part of sodium carbonate to adjust the pH to 12-13.

Embodiment 3

[0028] A preparation method of an efficient composite concrete antifreeze agent, comprising the following steps:

[0029] (1) Warm up 50 parts of water to 60°C, stir evenly, add 10 parts of β-naphthalenesulfonate formaldehyde condensate, 3 parts of glucose laurate, 1 part of sodium N-lauroyl sarcosinate, and continue stirring for 15 ~30min to get the mixed system A;

[0030] (2) Reduce the temperature of the mixed system A to 50°C, and add 40 parts of lignosulfonate, 30 parts of sodium sulfate, 15 parts of silicate, 15 parts of ammonium chloride, and 5 parts of triethanolamine under stirring conditions, After mixing evenly, put it in an oven and bake at 70°C for 30 minutes to obtain the mixed system B;

[0031] (3) Add 10 parts of glycerol and 5 parts of methanol to the mixing system B, grind for 20-30 minutes, and then add 0.1 part of caustic soda to adjust the pH to 12-13.

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PUM

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Abstract

The invention discloses a highly efficient composite concrete anti-freezing agent and a preparation method thereof which relates to the technical field of concrete anti-freezing agent. The concrete anti-freezing agent comprises lignin sulfonate, sodium sulfate, silicate, triethanolamine, ammonium chloride, beta naphthalene sulfonate formaldehyde condensate, glucose laurate, N sodium laurate, pH regulator, low molecular weight alcohol and water. The agent has the advantages of proper water reducing rate, minimum losses through concrete, short condensation time, good compatibility with water and observable improvement of the early strength of concrete. The anti-freezing agent can make sure of the normal and stable production of concrete, grant the concrete great anti-freezing effects. Moreover the manufacturing process of the anti-freezing agent is simple and not costly.

Description

technical field [0001] The invention relates to the technical field of concrete antifreeze, in particular to a high-efficiency composite concrete antifreeze and a preparation method thereof. Background technique [0002] Since the advent of Portland cement in the 1920s, concrete materials and their application techniques have been continuously developed. Concrete has become the most widely used building material in modern civil engineering. If the concrete can be designed correctly according to the use environment, and at the same time be constructed and maintained according to the requirements, concrete will be a very durable structural material, and its service life can reach a hundred years or even longer. However, freeze-thaw cycles are one of the main causes of concrete damage in cold regions of the world, especially in severe cold regions, and most of them occur in buildings in contact with water such as dams, roads, pools, and cooling towers of power stations. In th...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B24/22C04B103/60
CPCC04B40/0039C04B2103/601
Inventor 丘焕山
Owner 四会市恒星智能科技有限公司
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