Highly efficient composite concrete anti-freezing agent and preparation method thereof
A concrete and composite technology, which is applied in the field of concrete antifreeze, can solve the problems that the real air content of concrete is difficult to design or control, it is difficult to achieve frost resistance, and the strength of concrete is reduced, so as to achieve good antifreeze effect, low production cost, and high The effect of early strength
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Embodiment 1
[0018] A preparation method of an efficient composite concrete antifreeze agent, comprising the following steps:
[0019] (1) Warm up 60 parts of water to 60°C, stir evenly, add 6 parts of β-naphthalenesulfonate formaldehyde condensate, 5 parts of glucose laurate, 3 parts of sodium N-lauroyl sarcosinate, and continue stirring for 15 ~30min to get the mixed system A;
[0020] (2) Reduce the temperature of the mixed system A to 40°C, and add 30 parts of lignosulfonate, 20 parts of sodium sulfate, 20 parts of silicate, 8 parts of ammonium chloride, and 8 parts of triethanolamine under stirring conditions, After mixing evenly, put it in an oven and bake at 80°C for 30 minutes to obtain the mixed system B;
[0021] (3) Add 10 parts of propanol and 15 parts of isopropanol to the mixing system B, grind for 20-30 minutes, then add 0.1 part of sodium carbonate and 0.1 part of caustic soda to adjust the pH to 12-13.
Embodiment 2
[0023] A preparation method of an efficient composite concrete antifreeze agent, comprising the following steps:
[0024] (1) Warm up 80 parts of water to 80°C, stir evenly, add 8 parts of β-naphthalenesulfonate formaldehyde condensate, 3 parts of glucose laurate, 3 parts of sodium N-lauroyl sarcosinate, and continue stirring for 15 ~30min to get the mixed system A;
[0025] (2) Reduce the temperature of the mixed system A to 40°C, and add 32 parts of lignosulfonate, 25 parts of sodium sulfate, 18 parts of silicate, 6 parts of ammonium chloride, and 10 parts of triethanolamine under stirring conditions, After mixing evenly, put it in an oven and bake at 80°C for 35 minutes to obtain the mixed system B;
[0026] (3) Add 15 parts of ethylene glycol and 5 parts of ethanol to the mixing system B, grind for 20-30 minutes, then add 0.2 part of lime and 0.1 part of sodium carbonate to adjust the pH to 12-13.
Embodiment 3
[0028] A preparation method of an efficient composite concrete antifreeze agent, comprising the following steps:
[0029] (1) Warm up 50 parts of water to 60°C, stir evenly, add 10 parts of β-naphthalenesulfonate formaldehyde condensate, 3 parts of glucose laurate, 1 part of sodium N-lauroyl sarcosinate, and continue stirring for 15 ~30min to get the mixed system A;
[0030] (2) Reduce the temperature of the mixed system A to 50°C, and add 40 parts of lignosulfonate, 30 parts of sodium sulfate, 15 parts of silicate, 15 parts of ammonium chloride, and 5 parts of triethanolamine under stirring conditions, After mixing evenly, put it in an oven and bake at 70°C for 30 minutes to obtain the mixed system B;
[0031] (3) Add 10 parts of glycerol and 5 parts of methanol to the mixing system B, grind for 20-30 minutes, and then add 0.1 part of caustic soda to adjust the pH to 12-13.
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