Polymer solar cell and preparation method thereof
A technology of solar cells and polymers, applied in circuits, photovoltaic power generation, electrical components, etc., can solve the problems of high cost, complicated manufacturing process, and unsuitable for large-area applications, and achieve the effect of improving conversion efficiency and filling factor
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[0037] a. The mixed material (PTB7: PC 71 BM=1:1.5wt / wt) into a small brown bottle and put into a glove box.
[0038] b. Preparation of mixed solvents:
[0039] Scheme A): Add 1-bromo-4-butylbenzene to chlorobenzene (3% DIO vol%), the ratio of chlorobenzene (3% DIO vol%) to 1-bromo-4-butylbenzene is 97:3 (vol%);
[0040] Or, according to scheme B): Add 1-bromo-4-hexylbenzene to chlorobenzene (3% DIO vol%), the ratio of chlorobenzene (3% DIO vol %) to 1-bromo-4-hexylbenzene is 97:3 (vol%).
[0041] The order of addition is: CB, DIO, solvent additive (the ratio is 94:3:3vol%).
[0042] In the mixed solution composed of mixed material and mixed solvent, the concentration of PTB7 is 10mg / ml.
[0043] The adjustable ratio range of CB, DIO and solvent additive is: 95:3:2--93:3:4.
[0044] c. Stir and heat the mixed solution for at least 12 hours at a temperature of 60°C.
[0045] d. Spin-coat the mixed solution on the hole transport layer.
[0046] Based on PTB7: PC 71 The ...
Embodiment 1
[0054] The preparation process of this embodiment is:
[0055] 1. Configure the active layer material mixed solution one day in advance. The configuration process is as follows:
[0056] a. Weigh a certain amount of PTB7 and PC 71 BM (PTB7:PC 71 BM=1:1.5wt / wt) into a special reagent bottle.
[0057] b. The weighed mixed material (PTB7 and PC 71 BM) into the glove box, first add the calculated chlorobenzene solvent, then add DIO, and finally add the solvent additive Brbb, the volume ratio is CB:DIO:Brbb=94:3:3, to obtain a mixed solution. In the mixed solution, the concentration of PTB7 was 10mg / ml.
[0058] c. Place the prepared mixed solution on a heating platform and stir for at least 12 hours at a temperature of 60°C.
[0059] 2. The anode is indium tin oxide (ITO), and its square resistance is 15Ω / cm 2 . Wipe the ITO with acetone and perform ultrasonication. The order of ultrasonic solution use: ethanol, detergent water, deionized water, acetone, ethanol. After the...
Embodiment 2
[0069] The preparation process of this embodiment is:
[0070] 1. Configure the active layer material mixed solution one day in advance. The configuration process is as follows:
[0071] a. Weigh a certain amount of PTB7 and PC 71 BM (PTB7:PC 71 BM=1:1.5wt / wt) into a special reagent bottle.
[0072] b. Put the weighed mixed material into the glove box, first add the calculated chlorobenzene solvent, then add DIO, and finally add the solvent additive Brph, according to the volume ratio, CB:DIO:Brph=94:3:3 . In the mixed solution, the concentration of PTB7 was 10mg / ml.
[0073] c. Place the prepared mixed solution on a heating platform and stir for at least 12 hours at a temperature of 60°C.
[0074] 2. The anode is indium tin oxide (ITO), and its square resistance is 15Ω / cm 2 . Wipe the ITO with acetone and perform ultrasonication. The order of ultrasonic solution use: ethanol, detergent water, deionized water, acetone, ethanol. After the ultrasound is completed, it is ...
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