Low pressure superheated steam assisted evaporation crystallization device and crystallization process

A technology of superheated steam and crystallization device, which is applied in the direction of evaporation, separation and crystallization, general layout of crystallization device, crystallization separation, etc. It can solve the problems of inconvenient collection of low-pressure steam, difficult practical operation, unsatisfactory effect, etc., and achieve maximum Utilize, realize energy, design ingenious effects

Active Publication Date: 2018-12-07
JIANGSU WORLD TOP THERMAL TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the drying technology, some scholars have begun to conduct drying experiments on low-pressure superheated steam, and have obtained some physical and chemical advantages of low-pressure superheated steam during drying, but there are great technical difficulties in the specific practical operation process. The generation of steam is not complicated. Due to the inconvenient collection of low-pressure steam in the existing evaporation and crystallization technology, the practical operation is more difficult. Those skilled in the art have been trying various methods, but the effect is not very good. ideal

Method used

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  • Low pressure superheated steam assisted evaporation crystallization device and crystallization process
  • Low pressure superheated steam assisted evaporation crystallization device and crystallization process
  • Low pressure superheated steam assisted evaporation crystallization device and crystallization process

Examples

Experimental program
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Effect test

Embodiment 1

[0018] see Figure 1-Figure 4 , a low-pressure superheated steam assisted evaporation crystallization device, the crystallization device includes a material pump 1, a material preheater 2, a low-pressure steam generator 3, a heat exchanger 4, a falling film evaporator 5, a concentrated liquid delivery pump 6, a preheater Crystallizer 7, crystallizer 8 and condenser 9, the material preheater 2 is arranged between the material pump 1 and the falling film evaporator 5, connected by pipelines, the heat exchanger 4 is arranged in the low-pressure steam generator 3 Between the pre-crystallizer 7 and the pre-crystallizer 7, the pre-crystallizer 7 is connected to the condenser through a pipeline, and the dope delivery pump 6 is arranged between the falling film evaporator 5 and the pre-crystallizer 7, and the pre-crystallizer 7 is connected through a pipeline Connect crystallizer 8. In this technical solution, saturated steam under negative pressure condition is generated by a low-pr...

Embodiment 2

[0020] see figure 1 , figure 2 , as an improvement of the present invention, the pre-crystallizer 7 includes a crystallizer tank 13, a dope distributor 12 and a steam speed-up distributor 14, and the dope distributor 12 and the steam speed-up distributor 14 are set In the pre-crystallizer tank body, the steam speed-increasing distributor includes a steam distribution plate 17, a diffusion speed-increasing pipe 15 and a tee connection end, and the steam distribution plate is connected to the top of the diffusion speed-increasing pipe, and the diffuser The bottom of the speed-increasing pipe is connected with the three-way connecting step end. The thick liquid distributor 12 is larger than the opening of the ordinary material distributor, and the diameter of the opening is φ38. At the same time, the thick liquid distributor 12 is overlapped with the inner wall of the pre-crystallizer tank 13; the steam speed-increasing distributor It is composed of a three-way connection end ...

Embodiment 3

[0022] see figure 1 , figure 2 , as an improvement of the present invention, the crystallization device also includes a vacuum pump 10 and a pool 11, the vacuum pump is used to maintain the vacuum of the entire device, and one end of the condenser is connected through a pipeline. The vacuum degree of the system is mainly maintained by the vacuum pump 10, and the vacuum degree of the low-pressure superheated steam system is adjusted by an external vacuum pump system. In principle, the vacuum degree of the low-pressure superheated steam system is higher than that of the evaporation crystallization system. Other structures and advantages are exactly the same as those in the embodiment.

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Abstract

The invention relates to a low-pressure superheated steam-assisted evaporative crystallization device. A pre-crystallizer is added between an evaporator and a crystallizer. The pre-crystallizer consists of three major parts, i.e., a pre-crystallizer tank body, a concentrated solution distributor and a steam speed-up distributor. A material is concentrated by the evaporator, then, the concentrated material is conveyed into the pre-crystallizer by a concentrated solution conveying pump, a concentrated solution is uniformly distributed in the pre-crystallizer through the concentrated solution distributor, low-pressure saturated steam generated by a low-pressure saturated steam generator is subjected to heat exchange with a heat exchanger and then is changed into low-pressure superheated steam, the low-pressure superheated steam enters the pre-crystallizer through a steam speed increaser and is subjected to contact heat exchange with the concentrated solution from top end to bottom, moisture remaining in the concentrated solution is taken away, thus, the effect of further evaporating heat exchange of the material is achieved, and finally, the material is subjected to separation by crystallization in the crystallizer. The low-pressure saturated steam generator is generated in a water bath, so that preheat of an evaporative crystallization system can be used for heating a water-bath device, and thus, the effect of efficiently utilizing residual heat is achieved.

Description

technical field [0001] The invention relates to a crystallization device, specifically designs a low-pressure superheated steam assisted evaporation crystallization device, and belongs to the technical field of evaporation crystallization equipment. Background technique [0002] In the process of evaporation and crystallization, a considerable amount of low-temperature or low-pressure steam will be produced. Except for preheated materials or non-condensable gases, these steams will basically be condensed and discharged as condensed water. So how to make full use of this part of steam becomes particularly important under the background of energy shortage and energy crisis. Of course, the low-temperature or low-pressure steam generated during the evaporative crystallization process has been applied in the existing technology to a certain extent, and considerable results have been achieved. For example, for the mechanical compression of the secondary steam, the MVR technology ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D9/00
CPCB01D9/0031B01D9/0059
Inventor 宋玉臣
Owner JIANGSU WORLD TOP THERMAL TECH
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