376results about "Crystallization plant arrangements" patented technology

The invention provides an evaporative crystallization device and process for fluorine-containing high-salinity wastewater, and relates to the technical field of high-salinity wastewater treatment.The evaporative crystallization device for the fluorine-containing high-salinity wastewater comprises a support and an evaporation tank, and a first material opening used for communicating a stacking ring cavity with a material storage cavity is formed in an inner cylinder; a second material opening for communicating the material storage cavity with the material discharge cavity is formed in the first baffle plate; the heating assembly is in contact with and heats the wastewater to evaporate and discharge a wastewater solvent, a wastewater solute is gradually separated out to form crystals and moves towards the material stacking ring cavity, the first material opening is controlled to be opened, the second material opening is controlled to be closed, the crystals in the material stacking ring cavity enter the material storage cavity through the first material opening, and then the first material opening is controlled to be closed and the second material opening is controlled to be opened; the crystals in the material storage cavity enter the material discharging cavity through the second material opening, the crystals in the material discharging cavity are discharged through the first auger, the separated crystals can be continuously discharged without shutdown, meanwhile, the negative pressure environment in the evaporation tank is prevented from being damaged, and the working efficiency is improved.

The invention provides an ultrasonic-assisted gamma-aminobutyric acid crystallization particle size regulation and control method, which comprises the following steps: removing impurities and decolorizing gamma-aminobutyric acid-containing feed liquid, heating, stirring and concentrating to a nearly saturated state, then carrying out ultrasonic-assisted crystallization, cooling, aging and suction filtration to obtain coarse crystals, and finally washing and drying to obtain target crystals. According to the method, a synergistic process of raw material liquid pretreatment, evaporation concentration-ultrasonic-cooling coupling crystallization, aging and post-treatment is adopted, an ultrasonic cavitation effect is utilized to reduce a nucleation barrier, and a supersaturation degree precise control and gradient cooling strategy is combined, so that grain size refinement, obvious narrowing of distribution and effective inhibition of agglomeration of crystals are realized; the median particle size of the crystal can be controlled to be smaller than or equal to 200 microns, the particle size distribution span is smaller than or equal to 1.5, the agglomeration phenomenon is remarkably inhibited, the crystal form is kept stable, the crystal habit is complete and smooth, the crystal product quality and the process efficiency are remarkably improved, and the method has important industrial application value.

The invention relates to the technical field of acetaminophen crystallization, in particular to a multi-stage continuous cooling crystallization device and method for acetaminophen. The invention provides a multi-stage continuous cooling crystallization method for acetaminophen, which comprises the following steps: S1, at least five stages of continuous cooling crystallization are adopted, and circulating water with a set temperature is injected into a jacket of a crystallization kettle during each stage of cooling crystallization; wherein during the first several stages of crystallization, the difference between the initial temperature of the material entering the crystallization kettle and the initial temperature of the circulating water is 13-25 DEG C; and during the last crystallization, the initial temperature of the material entering the crystallization kettle is 30-35 DEG C. According to the multi-stage continuous cooling crystallization method, different water temperatures are adopted to carry out gradient cooling on the materials, so that the problems of non-uniform grain size and low purity caused by crystal explosion due to large temperature difference between the materials and a refrigerant and high cooling rate in the early stage of cooling are avoided.

The invention belongs to the technical field of coal chemical industry grey water treatment, and particularly relates to an advanced treatment method and system for coal chemical industry grey water circulating water. The method integrates pretreatment, complexing cracking, fractional crystallization and deep deamination, and is characterized in that a chelating structure of an organic phosphorus dispersing agent and calcium and magnesium ions is thoroughly destroyed through an advanced reduction-advanced oxidation combined process, target ions are released, and the core problems that hardness removal is hindered and phosphorus pollution is caused are solved; then, calcium and magnesium are respectively converted into calcium carbonate and magnesium ammonium phosphate particles for resource recovery by utilizing a secondary crystallization technology, so that the bottlenecks of high alkali liquor consumption and salt accumulation of a traditional high-pH magnesium ion precipitation method are broken through; and finally, the residual ammonia nitrogen is deeply removed by adopting a pollution-resistant PTFE hydrophobic membrane, so that the residual ammonia nitrogen is efficiently and stably removed, and the problem that a traditional polypropylene material membrane system is easy to pollute and block, easy to oxidize and difficult to apply to the field is solved.

The invention provides a process for recovering sodium sulfate, sodium carbonate and glaserite in alkali ash and removing chloride ions. The process specifically comprises the following steps: dissolving the alkali ash; sodium sulfate and sodium carbonate in the alkali ash solution are separated through hot crystallization; cooling, crystallizing and separating glaserite in the alkali ash solution; sulfate ions and carbonate ions in the alkali ash solution are separated from chloride ions; and further separating sodium sulfate, sodium carbonate, glauberite and the like in the alkali ash solution. Meanwhile, the invention provides a system for implementing the process. The system comprises an alkali ash dissolving unit, a main crystallization unit, a glaserite crystallization unit, a nanofiltration unit and other elements. According to the process and the system provided by the invention, on one hand, sodium sulfate and sodium carbonate in the alkali ash solution can be extracted, glaserite can be extracted at the same time, chloride ions in the solution are removed at the same time, and the discharge amount of mother liquor is reduced.

The invention relates to the technical field of wastewater treatment, in particular to a high-salinity wastewater low-temperature crystallization melting desalting device and method.The high-salinity wastewater low-temperature crystallization melting desalting device comprises a crystallization melting desalting device, a ton barrel and an infusion pump arranged on the crystallization melting desalting device, the infusion pump is slidably connected to the side wall of the crystallization melting desalting device, and a bottom frame is arranged beside the crystallization melting desalting device; the bottom frame is slidably connected with a containing frame used for containing a ton barrel, the containing frame is provided with two containing grooves matched with the ton barrel, the liquid inlet end of the infusion pump is fixedly connected with a fixing pipe, the side wall of the fixing pipe is fixedly connected with a side pipe, the side wall of the fixing pipe is provided with a conical sealing ring, and the upper side and the lower side of the outer wall of the side pipe are each provided with a top groove. Through the arrangement of the fixing pipe, the side pipe, the driving mechanism and other structures, rapid connection between the ton barrel and the crystallization melting desalter can be automatically achieved, meanwhile, an exhaust groove of the ton barrel can be automatically opened, connection between the ton barrel and the crystallization melting desalter can be rapidly released after extraction is completed, manual disassembly and assembly by workers are not needed, and the convenient performance of the device is greatly improved.

Black mass from disused lithium batteries is leached for recovery of various metals in a process that includes precipitation, solvent exchange, ion exchange, and salt splitting to create multiple product streams for recovery of pure value products. Most typically, the process is a closed-loop process and allows for production of metallic cobalt and nickel, EMD, and a high purity lithium hydroxide or carbonate product with minimal generation of waste streams.

The cooling crystallization production system comprises a crystallization unit, a product storage tank, a pipeline and a switching unit, the crystallization unit is composed of at least two parallel crystallizers, feeding ports of the crystallizers are connected with a discharging port of a distribution tank, and a discharging port of the distribution tank is connected with a discharging port of the product storage tank. Each crystallizer is a double-pipe heat exchanger, the shell pass of each crystallizer is a material flow path, and the tube pass of each crystallizer is a cold / hot medium flow path; the pipeline and switching unit is configured to selectively enable any crystallizer to be connected into a circulation loop, and in the circulation loop, materials circularly flow in the shell pass of the crystallizer through a circulation pump so as to achieve cooling crystallization. The crystallizer completing crystallization can be selectively switched to a discharging pipeline, and a heating medium is introduced into the tube pass of the crystallizer to melt crystals and then output the crystals into the product storage tank; compared with the prior art, a semi-continuous production mode is constructed, and the production cycle of unit products is shortened.

The invention discloses a crystallization device for sodium sarcosinate production, relates to the technical field of crystallization devices, and aims to solve the problems that when supersaturated liquid drops make contact with the wall surface of a low-temperature gas-liquid separator, water evaporation is intensified, the solubility of solute is further reduced due to temperature reduction, crystal precipitation is accelerated under the dual action, the supersaturated liquid drops are prone to being attached to the wall of a tank in the crystallization process, and the crystallization effect is poor. In order to solve the problems that the heat exchange efficiency is influenced by scaling of a tank wall, wall-adhered crystals cannot be recycled and the yield is reduced in the prior art, an evaporator is mounted on one side of a gas-liquid separator, a cyclone separator is mounted on the other side of the gas-liquid separator, an ultrasonic disperser is mounted on one side of the cyclone separator, a membrane filter is mounted on one side of the ultrasonic disperser, and a water outlet is formed in the other side of the membrane filter. A gas-liquid separator cleaning mechanism is mounted in the gas-liquid separator, a gas-liquid separator scraping frame is mounted at one end of the gas-liquid separator cleaning mechanism, and a membrane filter cleaning mechanism is mounted in the membrane filter.

The invention relates to the technical field of insecticides, and discloses an indoxacarb finished product crystallization device and method.The indoxacarb finished product crystallization device comprises a supporting bracket, a stirring tank is arranged at the top of the supporting bracket, an opening plate is arranged on one side of the stirring tank, a mounting frame is arranged at the top of the stirring tank, a driving source is arranged on the mounting frame, and a rotating shaft is arranged at the output end of the driving source; a fixing frame is arranged at the bottom of the inner wall of the stirring tank, and a homogenizing assembly is arranged on the fixing frame; the fixing frame is further provided with a vibration assembly. The homogenizing assembly is used for uniformly mixing the indoxacarb finished product solution in the stirring tank; the vibration assembly is used for reducing the phenomenon of local supersaturation of liquid in the stirring tank through vibration. Compared with the prior art, crystal agglomeration can be reduced, the particle distribution uniformity can be improved, the wall surface scaling risk can be reduced, the cleaning and maintenance frequency can be reduced, and the production efficiency and the product quality can be improved.

The invention relates to a wastewater treatment method, in particular to a capacitive deionization-oxidation coupling high-salt industrial wastewater treatment process, which comprises the following steps: firstly, carrying out micro-filtration to remove suspended matters and adjust the pH value, then carrying out low-voltage electro-adsorption desalination through a modified capacitive deionization unit, collecting electric energy released in a regeneration stage, converting the electric energy into electric energy of a catalytic oxidation unit through a converter, and carrying out high-salt industrial wastewater treatment. Desalted water enters a non-free radical catalytic oxidation unit, a UV-LED excitation catalyst activates persulfate, singlet oxygen is generated to degrade organic matter, an intelligent control system dynamically adjusts voltage, medicament and energy distribution according to the water inlet condition, finally, capacitive deionization regeneration liquid is subjected to multi-stage membrane concentration and crystallization, salt products are recycled, and waste water treatment and recycling are achieved.

The invention relates to the technical field of ammonium dihydrogen phosphate preparation, and discloses a high-purity ammonium dihydrogen phosphate crystallization device and a method thereof.The high-purity ammonium dihydrogen phosphate crystallization device comprises a first-stage crystallization system, a first-stage centrifugal separation system, a second-stage crystallization system and a second-stage centrifugal separation system which are connected in series. The primary crystallization system comprises a crystal elimination heater, a crystal elimination mixer, a bag filter and a DTB flash cooling crystallizer which are connected in sequence, and is used for primarily purifying a concentrated solution; the primary centrifugal separation system is used for separating primary crystals; the second-stage crystallization system comprises a crystal dissolving tank, an OSLO cooling crystallizer and the like, and deep crystallization is carried out after the first-stage crystal is dissolved; the secondary centrifugal separation system is used for separating secondary crystals; through two-stage crystallization coupling, mother liquor graded circulation, a unique gradient washing process and active impurity control, efficient and continuous production of battery-grade ammonium dihydrogen phosphate with wet-process phosphoric acid as a raw material is realized, the product purity is high, the process flow is simplified, the cost is low, and the system operation is stable.

The invention discloses a carbon dioxide trapping and sealing device, which belongs to the technical field of carbon dioxide trapping, and comprises a trapping container with a gas outlet pipe arranged at the top and a gas inlet pipe arranged at the bottom, and a control end arranged on the outer wall of the trapping container, and further comprises a stacked reaction tower vertically arranged in the trapping container and formed by stacking multiple stages of conical units, annular air gaps are formed among the multi-stage conical units, an airflow distributor and a central shaft tube are fixedly mounted at the bottom of the multi-stage conical units, and the central shaft tube is fixed with the multi-stage conical units through a bracket; and the alkaline solution supply assembly is arranged at the top of the trapping container. Flue gas with carbon dioxide escapes through the annular air gap of the laminated reaction tower, the alkaline solution is sprayed to the laminated reaction tower through the alkaline solution supply assembly, and after the carbon dioxide escapes from the annular air gap, the carbon dioxide and the alkaline solution are intersected twice, so that the carbon dioxide is fully captured.

To provide a process for forming drug crystals of narrow size distribution and desire dimensions and morphology.SOLUTION: The present invention relates to a process for providing corticosteroid crystals of desired size distribution and morphology, the process comprising the steps of: providing recrystallized ultra-large columnar crystals having aspect ratios of more than 1 and less than 20, the aspect ratio of a given columnar crystal being the ratio of a longest dimension along a lengthwise axis relative to a shortest dimension of a transverse plane perpendicular to the lengthwise axis; and sizing the recrystallized ultra-large columnar crystals to provide a collection of sized crystals having target dimensions, wherein the sizing includes segmenting at least a part of the recrystallized ultra-large columnar crystals along the respective lengthwise axes while retaining the dimensions of the transverse plane perpendicular to the lengthwise axis.SELECTED DRAWING: None

A process for production of both purified recycled aromatic dicarboxylic acid (rCA) and purified aromatic dicarboxylic acid (vCA), said process comprising:Producing a first stream comprising a recycled aromatic dicarboxylic acid by a first process, wherein the first process comprises the depolymerisation of a polymer feedstock comprising a polymer of said aromatic dicarboxylic acid in a first reaction system;Producing a second stream comprising the aromatic dicarboxylic acid by a second process wherein the second process comprises the oxidation of an aromatic hydrocarbon in a second reaction system;Purifying both the first stream and the second stream in a common purification system to thereby produce both purified recycled aromatic dicarboxylic acid (rCA) and purified aromatic dicarboxylic acid (vCA).The present invention also provides an apparatus for the production of both purified recycled aromatic dicarboxylic acid (rCA) and purified aromatic dicarboxylic acid (vCA),

It is provided an environmentally friendly process for recycling metals and nonmetallic components from printed circuit boards (PCBs), without using treatments considered damaging to the environment and minimizing emission of greenhouse gases comprising the steps of shredding the PCBs, micronizing the shredded PCBs producing a micronized powder, removing plastic and epoxy from the micronized powder, leaching, precipitating and recuperating the Al, Fe, Zn, Ni, Cr, Cu, Au, Ag, and Pd from the micronized powder, producing a filtrate from which the Cu is recovered. The solid product of the process is a concentrate of precious metals.

The application discloses a preparation method of polyaluminum chloride, and is characterized by comprising the following steps: S1, adding aluminum ash and hydrochloric acid solution into an acidification reaction tank, heating and reacting, filtering after the reaction is completed, and passing the filtrate into a polymerization reaction kettle; S2, adding calcium carbonate into the polymerization reaction kettle in batches to carry out polymerization reaction, stopping the reaction after the calcium carbonate is completely dissolved and the PH of the solution is 3-5; S3, adding polyacrylamide and ferric chloride into the polymerization reaction kettle, and precipitating under 1-3 pa low pressure to obtain sludge and upper liquid, concentrating and crystallizing the upper liquid, crushing the crystal, and obtaining polyaluminum chloride. The application increases an automatic blocking mechanism below a crystallization and crushing tank, automatically blocks when the sub-packaging cylinder is filled with crystals, achieves the purpose of quantitative sub-packaging, and does not cause too much or too little crystals in the sub-packaging cylinder, and does not require staff to be always beside the machine.

A recovery system for preparing magnesium sulfate using sulfuric acid waste liquid is provided. [Solution] The recovery system for preparing magnesium sulfate using sulfuric acid waste liquor according to the present invention comprises a reactor 1, a crystallizer 3, a dehydrator 4, and a dryer 5. The reactor 1 removes hydrogen peroxide from the sulfuric acid waste liquor and produces a magnesium sulfate solution. The crystallizer 3 continuously recrystallizes the magnesium sulfate solution by lowering its temperature, obtaining magnesium sulfate crystals and their mother liquor. The dehydrator 4 removes the mother liquor, and the dryer 5 dries the solution at different temperatures to obtain magnesium sulfate hydrates containing different amounts of water of crystallization.

The application discloses a cooling crystallization device for arsenic leaching solution, which comprises a cooling crystallization tank with a corresponding heat exchange jacket arranged on the periphery, a stirring mechanism comprising a hollow rotating shaft, the middle part of the hollow rotating shaft is connected with corresponding arc-shaped stirring plates through a plurality of material collecting pipes, a crystallization material discharging mechanism comprising a discharging one-way valve installed at the bottom of the hollow rotating shaft, a corresponding blocking push plate is installed in the hollow rotating shaft on the upper side of the material collecting pipe and can be lifted, the blocking push plate is rotationally connected to the end of the piston rod of a corresponding lifting drive oil cylinder through a corresponding connecting shaft, at least one liquid discharging one-way valve for discharging liquid material is installed on the blocking push plate, a corresponding filter screen plate is fixedly connected to the bottom side of the liquid discharging one-way valve, and the opening pressure of the liquid discharging one-way valve is smaller than that of the discharging one-way valve. The application can effectively separate the solid and liquid of part of the crystallized material, and can timely output the crystallization material after the solid-liquid separation.

The invention discloses a hydrolysate deacidification-dehydration coupling process and a byproduct recovery method, and belongs to the technical field of hydrolysate treatment. The method comprises the following steps: pretreating a hydrolysate raw material through two-stage filtration; adding the pretreated hydrolysate, a deacidification agent and a dehydration auxiliary agent into a coupling reaction device, and synchronously carrying out deacidification-dehydration reaction under the conditions of 60-120 DEG C and 0.1-0.5 MPa; after the reaction, separating to obtain a deacidification and dehydration product and a mixed solid phase; and dissolving and crystallizing the mixed solid phase to recover high-purity byproducts. The deacidification and dehydration synergistic interaction is achieved, the acidity reduction rate is larger than or equal to 85%, the water content is smaller than or equal to 5%, and the process time consumption is shortened by 28.6%; the byproduct purity is not less than 90%, and the recovery rate is not less than 80 A tail gas treatment system is additionally arranged to ensure that environmental protection reaches the standard. The process is suitable for biomass, polysaccharide and protein hydrolysate treatment, has the advantages of high efficiency, good resource utilization rate and the like, and provides an efficient solution for hydrolysate industrial treatment.

A liquid separation method (10) for separating mono ammonium phosphate ("MAP") (20) in aqueous solution, includes: • a receiving step in which a process liquid which comprises water and MAP is received; • a cooling step in which a controlled cooling process is applied to the process liquid to induce the crystallization (14) of MAP; • a separating step (16) in which the crystallised MAP is separated from the remaining process liquid.

A hybrid process and system for separating water from an inlet brine solution is disclosed. The hybrid process couples at least two different separation processes / systems. The inlet brine solution is fed into a first separation process, which produces a water distillate and a brine concentrate. The brine concentrate from the first separation process is then fed into the second separation process to further recover additional water. The excess heat from the second separation process is supplied to the first separation process.

The invention discloses a processing method for fractionation and rapid crystallization of palm oil, which comprises the following steps: (1) heating and controlling a palm oil raw material to be fractionated to 55-65 DEG C (crystal breaking), pumping the palm oil raw material into a crystallizing tank, and then cooling the palm oil raw material to about 25 DEG C under the action of rapid cooling of cooling water (or chilled water) and stirring; (2) continuously reducing the temperature of the palm oil raw material in the crystallizing tank by using chilled water, adding a certain proportion of palm oil (solid-liquid mixture) which is completely crystallized and is in an unseparated state into the crystallizing tank at the interval of 25.0-18.0 DEG C as a seed crystal, and controlling the stirring speed of the crystallizing tank at 15-30r / min until the palm oil raw material is completely cooled and crystallized; (3) after crystallization is completed, if seed crystals need to be added into the crystallizing tank which is cooling and crystallizing, pumping the seed crystals into the crystallizing tank which needs to be added with the seed crystals through a pump; otherwise, immediately pumping into a membrane filter for filtering and separating (preventing the tank from being burnt) to obtain liquid oil and stearin. The palm oil seed crystal is added, so that the crystallization time can be shortened; and through seed crystal induction, the formation of stable-form crystals is accelerated, excessive crystallization is avoided, and the interception loss of filtration is reduced, so that the liquid oil yield is improved.

A method for producing mixed metal salts containing manganese ions and at least one of cobalt ions and nickel ions, the method including: an Al removal step of subjecting an acidic solution containing at least manganese ions and aluminum ions, and at least one of cobalt ions and nickel ions, to removal of the aluminum ions by extracting the aluminum ions into a solvent, the acidic solution being obtained by subjecting battery powder of lithium ion batteries to a leaching step; and a precipitation step of neutralizing an extracted residual liquid obtained in the Al removal step under conditions where a pH is less than 10.0, to precipitate mixed metal salts comprising a metal salt of manganese and a metal salt of at least one of cobalt and nickel.

Method for producing electronic grade nickel sulfate from nickel powder, crystallization apparatus, and control thereof The present invention provides a method for producing nickel sulfate, and nickel sulfate produced thereby. The process includes acid leaching, copper removal, acid adjustment, concentration, cooling crystallization, drying and sieving, and secondary leaching. Oxidation In the calcination furnace, the temperature is 400 to 700°C, and 1 kg of compressed air is used for each kilogram of nickel powder. ~5m 3 The reaction time is 1.0 to 2.5 hours, and the temperature during acid immersion is controlled to 45 to 70°C. Then, add dilute sulfuric acid to control the pH to 0.5-1.5 and react for 1-3 hours. The copper removal is to replace the copper with nickel powder, and the acid conditioning is to use nickel hydroxide or The pH is adjusted to 2.5-4.5 using nickel carbonate, and the filtrate is concentrated by The cooling crystallization method is to obtain nickel sulfate crystals and return the mother liquor to the concentrate. Drying and sieving is to add the undersieved material to the crystallizer as seed crystals, and secondary leaching is to Dilute sulfuric acid is added to the leaching slag, and it is reacted with nickel sulfate or hydrogen peroxide until nickel is less than 0.1%. If the first stage is full, the second leaching is continued. The crystallizer is a crystallizer that is connected in series with a second-stage crystallizer and a third-stage crystallizer. A crystallization frame, an oscillator provided under the crystallization frame, and an oscillator provided at the exit end of the crystallization frame. The crystallization frame is a rectangular parallelepiped. The bottom of the ribs are evenly spaced, with a cross section of a circular arc. The distance between two adjacent ribs is S is 1 / 25 to 1 / 15 of the width of the crystallization frame, and either the width b or the height h of the rib The width of the crystallization frame is 1 / 100 to 1 / 150 of the width of the crystallization frame. It does not add any new impurity ions, and does not add any oxidizing agent. The nickel sulfate crystal particles produced are uniform and are free of the static generation. This avoids caking of very large particles, irregularly shaped particles and crystals.

The present disclosure provides a preparation system and a preparation method for xylitol crystals. In the preparation system, outlets of a first centrifuge are connected with an inlet of a hot air drying tank and an inlet of a primary mother liquor storage tank through pipelines, respectively. Outlets of a second centrifuge are connected with an inlet of a second fluidized bed dryer and an inlet of a secondary mother liquor storage tank through pipelines, respectively. An outlet of a dicrystalline sugar dissolution tank is connected with an inlet of a blending tank through a pipeline. An outlet of a tricrystalline sugar dissolution tank is connected with the inlet of the primary mother liquor storage tank. The blending tank is provided with an inlet for a raw material of xylitol hydrogenation solution. An output of an outlet of a first fluidized bed dryer is prepared xylitol crystals.

The invention provides a cooling crystal obtaining system for generating a chelated fertilizer, and relates to the technical field of mixed fertilizer manufacturing, the cooling crystal obtaining system comprises a crystallization bin, the middle of the bottom of the crystallization bin is connected with a circulating pipeline, and the front side of the lower end of the circulating pipeline is connected with a discharge pipeline; a chelating bin is fixedly arranged at the top of the crystallizing bin, a top cover is fixedly arranged at the top of the chelating bin, and a feeding pipe is fixedly connected to the front upper part of the top cover; six groups of expansion grooves are integrally arranged below the outside of the chelating bin, and semiconductor refrigeration plates are fixedly arranged outside the expansion grooves; in the system, the chelating bin and the crystallizing bin continuously convey liquid materials through the air pressure and communicating vessel principle, circulating backflow retreatment of the uncrystallized liquid materials is achieved through the circulating device, the flow direction of the liquid materials is accurately regulated and controlled in cooperation with the electric cylinder A and the electric cylinder B, and the whole process of raw material supplementation, crystal generation and crystal separation can be completed without shutdown; the problems that traditional evaporative crystallization is low in efficiency and continuous operation cannot be achieved are solved, and the yield of chelated fertilizer crystals in unit time is remarkably increased.

A production system, production method and application of general-purpose high-purity chemicals are disclosed. The production system includes a raw material tank, and an adsorption system, a crystallizer, a first light-impurity removal tower, a first heavy-impurity removal tower, a second light-impurity removal tower, a motorized tower, a second heavy-impurity removal tower, a vapor permeation device, a membrane separation system and a filling system connected with the raw material tank in sequence. The high-purity chemicals produced by the above system have high purity and excellent quality. Compared with the prior art, the system and method designed by the present disclosure have more pertinence, integrity, progressiveness, energy-saving, precision, high safety coefficient and great industrial promotion value. And the products produced are of excellent quality, which can meet the standards applied to the manufacturing of integrated circuit electronic components and meet the high-end needs of the semiconductor industry market.

The application discloses a kind of phosphoric acid extraction semi-water-two water alternate crystallization system and method, belong to the technical field of wet-process phosphoric acid production, the system is by the reaction tank unit of series connection and semi-water and two water reaction tank alternate arrangement, with the sulfuric acid dilution mixed heat exchanger group connected with reaction tank, simple heat exchanger group is arranged between tank to realize heat transfer.Construction.The method includes: material is temperature-adjusted after passing through sulfuric acid dilution mixed heat exchanger, in turn into the reaction tank sequence of alternate arrangement, heat circulation is carried out in adjacent tank by simple heat exchanger, under the control of PLC in 75~85 DEG C and 88~95 DEG C interval, realize the alternate crystallization of semi-water-two water calcium sulfate.The application replaces traditional flash evaporation external discharge with heat internal circulation between tank, solves the technical problems of high steam energy consumption, low phosphorus recovery rate, insufficient phosphoric acid concentration and high upgrading cost of stock device in traditional process, and has the comprehensive advantages of energy saving, yield, low-cost transformation and phosphogypsum resource.

Methods and systems for the extraction of magnetic material from magnet containing material, and for extraction of rare earth elements (REEs) from the magnetic material are disclosed. An exemplary system includes a milling / washing unit for magnet containing material such as end-of-life motors, hard drives, partially deconstructed motors, magnet-containing end-of-life product, or parts thereof, and outputting magnetic components by exploiting magnetic properties of ferromagnetic and paramagnetic materials in the presence and absence of electromagnetic fields in conjunction with other physical properties such as size and density. The system also includes a chemical processing unit for receiving the magnetic components to extract rare earth elements in the material. Chemical processes are disclosed for separating rare earth elements from magnetic components.