K2(C6H7O6)(HSO4) as well as preparation method and application thereof
A technology of potassium ascorbate and ascorbic acid, applied in the field of biochemical medicine, medicine and food, can solve problems such as no reports on potassium ascorbate hydrogen sulfate, and achieve the effects of easy operation, simple preparation method and reduced reagent cost
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Embodiment 1
[0026] The preparation method of present embodiment hydrogen sulfate potassium ascorbate comprises the following steps:
[0027] (1) Take by weighing raw material potassium sulfate K 2 SO 4 174.2g and Ascorbic Acid C 6 h 8 o 6 176.1g, the raw materials are dissolved in deionized water, the amount of deionized water can just completely dissolve the raw materials, and the chemical reaction is carried out at room temperature.
[0028] (2) After fully reacting, absolute ethanol is added in the reaction solution to separate out hydrogen sulfate potassium ascorbate crystals.
[0029] (3) Filter and wash the material obtained in step (2) with absolute ethanol to obtain potassium hydrogen sulfate ascorbate crystals.
[0030] (4) The potassium ascorbate hydrogen sulfate crystal obtained in step (3) is dried at 105° C., weighed after the drying treatment to obtain 245.2 g of potassium hydrogen sulfate ascorbate, and finally packaged as a finished product.
Embodiment 2
[0032] The preparation method of present embodiment hydrogen sulfate potassium ascorbate comprises the following steps:
[0033] (1) Take by weighing raw material potassium sulfate K 2 SO 4 87.1g and Ascorbic Acid C 6 h 8 o 6 88.1g, dissolve the raw materials in deionized water, the amount of deionized water can just completely dissolve the raw materials, and carry out the chemical reaction at room temperature.
[0034] (2) After fully reacting, absolute ethanol is added in the reaction solution to separate out hydrogen sulfate potassium ascorbate crystals.
[0035] (3) Filter and wash the material obtained in step (2) with absolute ethanol to obtain potassium hydrogen sulfate ascorbate crystals.
[0036] (4) The potassium ascorbate hydrogen sulfate crystal obtained in step (3) is dried at 102° C., weighed after the drying treatment to obtain 119.1 g of potassium hydrogen sulfate ascorbate, and finally packaged as a finished product.
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