Low-temperature oil-resisting nitrile rubber and preparation method and application thereof
A technology of nitrile rubber and nitrile rubber, applied in the field of rubber sealing materials, can solve the problems of inability to have both low temperature resistance and physical and mechanical properties, unable to meet the needs of aerospace sealing materials, and low liquid resistance, and achieve good physical and mechanical properties. Mechanical properties and adhesive strength, solving airborne environmental conditions and sealing without leakage, small effect of liquid resistance
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Embodiment 1
[0019] A kind of preparation method of low temperature oil resistant nitrile rubber of the present invention, comprises the following steps:
[0020] 1) Weigh the raw material components according to the following parts by weight: 100 parts of oligosiloxane modified nitrile rubber, 7.5 parts of zinc oxide, 1 part of stearic acid, 2 parts of anti-aging agent NAPM, 30 parts of high wear-resistant carbon black, Quickly extrude 75 parts of carbon black, 1 part of sulfur, 1 part of DCP, 2 parts of bis-pentasulfurizing agent, 1.5 parts of accelerator TE, 1 part of accelerator DM, and 40 parts of TP-90B;
[0021] 2) Pass the oligosiloxane-modified nitrile rubber thinly for 3 times and set aside; disperse the zinc oxide, stearic acid, anti-aging agent NAPM, composite reinforcing agent, and composite vulcanizing agent evenly with a mixing speed-regulating disperser, spare;
[0022] 3) Add the above-mentioned oligosiloxane-modified nitrile rubber, mixed materials, composite accelerator...
Embodiment 2
[0027] A kind of preparation method of low temperature oil resistant nitrile rubber of the present invention, comprises the following steps:
[0028]1) Weigh the raw material components according to the following parts by weight: 100 parts of oligosiloxane modified nitrile rubber, 7.5 parts of zinc oxide, 1 part of stearic acid, 2 parts of anti-aging agent NAPM, 25 parts of high wear-resistant carbon black, Quickly extrude 85 parts of carbon black, 1 part of sulfur, 1 part of DCP, 2 parts of bis-pentasulfurizing agent, 1.5 parts of accelerator TE, 1 part of accelerator DM, and 30 parts of TP-90B;
[0029] 2) Pass the oligosiloxane-modified nitrile rubber thinly for 2 times and set aside; disperse the zinc oxide, stearic acid, anti-aging agent NAPM, composite reinforcing agent, and composite vulcanizing agent evenly with a mixing speed-regulating disperser, spare;
[0030] 3) Add the above-mentioned oligosiloxane-modified nitrile rubber, mixed materials, composite accelerator ...
Embodiment 3
[0035] A kind of preparation method of low temperature oil resistant nitrile rubber of the present invention, comprises the following steps:
[0036] 1) Weigh the raw material components according to the following parts by weight: 80 parts of siloxane modified nitrile rubber, 5 parts of zinc oxide, 0.5 part of stearic acid, 1 part of anti-aging agent NAPM, 16 parts of high wear-resistant carbon black, fast press 64 parts of carbon black, 0.25 parts of sulfur, 0.25 parts of DCP, 0.5 parts of double pentasulfurizing agent, 0.75 parts of accelerator TE, 0.25 parts of accelerator DM, 20 parts of TP-90B auxiliary agent;
[0037] 2) Pass the siloxane-modified nitrile rubber thinly for 5 times and set aside; disperse the zinc oxide, stearic acid, anti-aging agent NAPM, composite reinforcing agent, and composite vulcanizing agent evenly with a mixing speed-regulating disperser, and set aside;
[0038] 3) Add the above-mentioned siloxane-modified nitrile rubber after thinning, the mixe...
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