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Low-temperature oil-resisting nitrile rubber and preparation method and application thereof

A technology of nitrile rubber and nitrile rubber, applied in the field of rubber sealing materials, can solve the problems of inability to have both low temperature resistance and physical and mechanical properties, unable to meet the needs of aerospace sealing materials, and low liquid resistance, and achieve good physical and mechanical properties. Mechanical properties and adhesive strength, solving airborne environmental conditions and sealing without leakage, small effect of liquid resistance

Inactive Publication Date: 2017-05-24
青岛颐科密封材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The invention provides a low-temperature oil-resistant nitrile rubber and its preparation method and application, which solves the problem that the oil resistance, low-temperature resistance and physical and mechanical properties of rubber sealing materials in the prior art cannot meet the needs of aerospace sealing materials The problem
[0005] The low-temperature oil-resistant nitrile rubber of the present invention has excellent low-temperature resistance, is suitable for -70~100°C environmental conditions, has good oil resistance, and solves the problem of airborne extremely low-temperature environmental conditions. It is used in 10# aviation The hydraulic oil can withstand a pressure of 13MPa and the seal does not leak, which solves the airborne sealing problem; the low-temperature oil-resistant nitrile rubber has low liquid resistance, and has good resilience and sealing at an altitude of 8,000 meters and at a low temperature of -70°C Performance ensures the safe operation of airborne equipment, improves the flight safety of aircraft, meets the needs of the development of national defense technology and weaponry, and fills the gap in high-low temperature resistant rubber materials

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] A kind of preparation method of low temperature oil resistant nitrile rubber of the present invention, comprises the following steps:

[0020] 1) Weigh the raw material components according to the following parts by weight: 100 parts of oligosiloxane modified nitrile rubber, 7.5 parts of zinc oxide, 1 part of stearic acid, 2 parts of anti-aging agent NAPM, 30 parts of high wear-resistant carbon black, Quickly extrude 75 parts of carbon black, 1 part of sulfur, 1 part of DCP, 2 parts of bis-pentasulfurizing agent, 1.5 parts of accelerator TE, 1 part of accelerator DM, and 40 parts of TP-90B;

[0021] 2) Pass the oligosiloxane-modified nitrile rubber thinly for 3 times and set aside; disperse the zinc oxide, stearic acid, anti-aging agent NAPM, composite reinforcing agent, and composite vulcanizing agent evenly with a mixing speed-regulating disperser, spare;

[0022] 3) Add the above-mentioned oligosiloxane-modified nitrile rubber, mixed materials, composite accelerator...

Embodiment 2

[0027] A kind of preparation method of low temperature oil resistant nitrile rubber of the present invention, comprises the following steps:

[0028]1) Weigh the raw material components according to the following parts by weight: 100 parts of oligosiloxane modified nitrile rubber, 7.5 parts of zinc oxide, 1 part of stearic acid, 2 parts of anti-aging agent NAPM, 25 parts of high wear-resistant carbon black, Quickly extrude 85 parts of carbon black, 1 part of sulfur, 1 part of DCP, 2 parts of bis-pentasulfurizing agent, 1.5 parts of accelerator TE, 1 part of accelerator DM, and 30 parts of TP-90B;

[0029] 2) Pass the oligosiloxane-modified nitrile rubber thinly for 2 times and set aside; disperse the zinc oxide, stearic acid, anti-aging agent NAPM, composite reinforcing agent, and composite vulcanizing agent evenly with a mixing speed-regulating disperser, spare;

[0030] 3) Add the above-mentioned oligosiloxane-modified nitrile rubber, mixed materials, composite accelerator ...

Embodiment 3

[0035] A kind of preparation method of low temperature oil resistant nitrile rubber of the present invention, comprises the following steps:

[0036] 1) Weigh the raw material components according to the following parts by weight: 80 parts of siloxane modified nitrile rubber, 5 parts of zinc oxide, 0.5 part of stearic acid, 1 part of anti-aging agent NAPM, 16 parts of high wear-resistant carbon black, fast press 64 parts of carbon black, 0.25 parts of sulfur, 0.25 parts of DCP, 0.5 parts of double pentasulfurizing agent, 0.75 parts of accelerator TE, 0.25 parts of accelerator DM, 20 parts of TP-90B auxiliary agent;

[0037] 2) Pass the siloxane-modified nitrile rubber thinly for 5 times and set aside; disperse the zinc oxide, stearic acid, anti-aging agent NAPM, composite reinforcing agent, and composite vulcanizing agent evenly with a mixing speed-regulating disperser, and set aside;

[0038] 3) Add the above-mentioned siloxane-modified nitrile rubber after thinning, the mixe...

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Abstract

The invention discloses low-temperature oil-resisting nitrile rubber and a preparation method application thereof, and belongs to the technical field of rubber sealing materials. The rubber is prepared from, by weight, 80-120 parts of siloxane modified butadiene-acrylonitrile rubber, 5-10 parts of zinc oxide, 0.5-1.5 parts of stearic acid, 1-3 parts of an anti-aging agent NAPM, 80-120 parts of composite reinforcing agent, 1-5 parts of composite sulfurizing agent, 1-3 parts of an accelerant and 20-40 parts of TP-90 B auxiliaries. The invention further provides the preparation method of the low-temperature oil-resisting nitrile rubber and application of the low-temperature oil-resisting nitrile rubber in an aviation sealing material. The low-temperature oil-resisting nitrile rubber has the excellent low temperature resistance and good oil resistance, has the good physical and mechanical properties and bonding strength, is applicable to the environment under the temperature of subzero 70 to 100 DEG C, achieves the purposes of onboard environment conditions and sealing non-leakage, ensures safety operation of airborne equipment, and meets the requirement for defense-related science and technology weaponry development.

Description

technical field [0001] The invention belongs to the technical field of rubber sealing materials, in particular to a low-temperature oil-resistant nitrile rubber and its preparation method and application. Background technique [0002] In the field of aerospace, when the aircraft flies at an altitude of 8,000 meters, the ambient temperature will vary between -70 and 100°C; in this environment, oil-resistant sealing materials are required to have excellent oil resistance and Very good low temperature resistance. At present, the ordinary nitrile rubber materials, fluororubber materials and fluorosilicone rubber materials used today cannot meet the requirements of the aerospace field, which brings great safety hazards to aircraft and limits national defense technology and The development of weapons and equipment. Moreover, the production cost of existing fluorosilicone rubber materials is extremely high, and large-scale industrial production has not yet been formed; there are ...

Claims

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Application Information

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IPC IPC(8): C08L9/02C08L83/04C08K13/02C08K3/22C08K5/09C08K3/04C08K5/14B29C35/02
CPCC08L9/02B29C35/02C08K2201/014C08L83/04
Inventor 姜玉华方芳杨伟娜朱仲华姜子凡
Owner 青岛颐科密封材料有限公司
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