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Wet grinding preparation method of electronic smoke oil with tobacco flavor

A technology of e-cigarette oil and wet crushing, which is applied in the fields of tobacco, tobacco processing, application, etc., can solve the problems of sensory quality that cannot meet the requirements of consumers, the extraction of burnt aroma and aroma of tobacco leaves, and the loss of active ingredients, etc., to achieve Prevent dust from contaminating products, increase leaching rate, and improve sensory quality

Active Publication Date: 2017-05-31
ETABONG QINGDAO INDAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The traditional tobacco extract is mainly to extract the tobacco leaves or shredded tobacco with ethanol or water under reflux at a certain temperature, which is difficult to extract the burnt aroma in the tobacco leaves
Patent 201410263756.5 provides a Maillard reaction product of tobacco leaf extract, but the reaction process of Maillard reaction is complicated, there are many intermediate products, and the influencing factors are difficult to control; patent 201410721776.2 provides a method for preparing light components of tobacco extract , the reaction has disadvantages such as complex operation, low extraction rate, and large loss of active ingredients, and the sensory quality of the extract prepared by traditional methods in e-cigarette oil cannot well meet the requirements of consumers
At the same time, most consumers will experience discomfort such as dry mouth and tongue after smoking e-cigarettes, and even dizziness and nausea in severe cases. This problem also needs to be improved urgently.

Method used

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  • Wet grinding preparation method of electronic smoke oil with tobacco flavor
  • Wet grinding preparation method of electronic smoke oil with tobacco flavor

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] (1) Accurately weigh 100 g of dried flue-cured tobacco, pass through a 5-50 mesh sieve after primary crushing, and add 500 g of solvent to the primary crushed flue-cured tobacco. The solvent includes the following components, calculated by mass percentage: Alcohol 20%, propylene glycol 75%, ethanol 2%, the balance is made up to 100% by weight with deionized water, then add 20 g of mulberry and olive mixed extracts, mix well and add to a high-speed cutting type wet pulverizer, control the high-speed The speed of the cutting-type wet pulverizer is 4000 r / min, the pulverization temperature is 20 ℃, and the pulverization time is 6 h. After pulverization, the material is discharged, and the discharged liquid is the base oil of tobacco-flavored e-cigarette oil;

[0024] (2) Stir and mix the 50% by mass tobacco-flavored e-liquid base oil and 50% by mass flavor and fragrance to obtain tobacco-flavored e-liquid.

Embodiment 2

[0026] (1) Accurately weigh 100 g of dried Burley tobacco, pass through a 5-50 mesh sieve after primary crushing, and add 1000 g of solvent to the primary crushed Burley tobacco. The solvent includes the following components, by mass percentage Total: 30% glycerol, 60% propylene glycol, 5% ethanol, the balance is made up to 100% by weight with deionized water, then add 10 g of pomegranate and human face mixed extract, mix well and add high-speed cutting type wet crushing In the machine, the speed of the high-speed cutting wet pulverizer is controlled to be 5000 r / min, the pulverization temperature is 25°C, and the pulverization time is 2 h. After pulverization, the material is discharged, and the discharged liquid is the tobacco-flavored e-cigarette oil base oil;

[0027] (2) Stir and mix the tobacco-flavored e-liquid base oil with a mass percentage of 60% and the flavor and fragrance with a mass percentage of 40% to obtain a tobacco-flavored e-liquid.

Embodiment 3

[0029] (1) Accurately weigh 100 g of dried oriental tobacco, pass through a 5-50 mesh screen after primary crushing, and add 600 g of solvent to the primary crushed oriental tobacco. The solvent includes the following components, calculated by mass percentage: C 50% triol, 30% propylene glycol, 15% ethanol, make up the balance to 100% by weight with deionized water, then add 50 g of mixed extracts of grass jelly and vinegar willow fruit, mix well and add to a high-speed cutting wet pulverizer Among them, the speed of the high-speed cutting wet pulverizer is controlled to be 8000 r / min, the pulverization temperature is 10 ℃, and the pulverization time is 0.5 h. After pulverization, the material is discharged, and the discharged liquid is the tobacco-flavored e-cigarette oil base oil;

[0030] (2) Stir and mix the 70% by mass tobacco-flavored e-liquid base oil and 30% by mass flavor and fragrance to obtain tobacco-flavored e-liquid.

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Abstract

The invention provides a wet grinding preparation method of electronic smoke oil with tobacco flavor. The method comprises the steps of S1, accurately weighing and taking a certain mass of dry tobacco, conducting primary grinding, passing the ground tobacco through a 5-50 mesh net, adding a certain proportion of solution into the ground tobacco, mixing the solution uniformly, adding the solution into a high speed cutting wet grinder, grinding the solution in a certain reaction condition, taking out the solution after the reaction, wherein the solution taken out is the base oil of the electronic smoke oil with the tobacco flavor; S2, mixing the base oil of the electronic smoke oil with tobacco flavor with the mass percent of 50-100% and the essence and perfume with the mass percent of 0-50% uniformly to obtain the electronic smoke oil with tobacco flavor. Compared with the prior art, the electronic smoke oil with tobacco flavor prepared by mixing the base oil with tobacco flavor according to the method has a substantial elevation of sensual quality, can effectively reduce the mouth sweat and sticky feeling brought by the electronic smoke oil, and alleviate the symptoms of drying mouth and dry tongue after smoking.

Description

technical field [0001] The invention relates to the technical field of e-liquid for electronic cigarettes, in particular to a method for preparing tobacco-flavored e-liquid by wet pulverization. Background technique [0002] In recent years, with the increasingly severe international tobacco control and the general improvement of consumers' health awareness, countries around the world have successively restricted the sales of traditional cigarettes through legislation, and the international cigarette sales have maintained a decline of 3%. Under this background, domestic and foreign tobacco companies continue to promote The development of new tobacco products, among which electronic cigarettes, as an important form of new tobacco products, has achieved rapid development. E-cigarette is a non-combustible tobacco substitute product, which has a similar appearance to cigarettes. Electronic cigarette liquid produces mist under the action of an electronic cigarette atomizer, which...

Claims

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Application Information

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IPC IPC(8): A24B15/16
CPCA24B15/16
Inventor 宋新华王钧张书铭刘晓芊宋时浩
Owner ETABONG QINGDAO INDAL
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