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Ultra-long-afterglow energy-storing luminous resin adhesive and preparation method thereof

A technology of energy storage luminescence and resin glue, which is applied in the direction of luminescent paint, coating, etc., can solve the problems of poor storage stability of luminescent resin glue, layering and precipitation of paint, high density of luminescent powder, etc., and achieve significant economic and social benefits , low cost, good storage stability

Inactive Publication Date: 2017-06-13
刘海泉
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Due to the high density of the luminescent powder in the existing luminescent resin glue, the paint is prone to delamination and precipitation, and the storage stability of the luminescent resin glue is poor

Method used

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  • Ultra-long-afterglow energy-storing luminous resin adhesive and preparation method thereof
  • Ultra-long-afterglow energy-storing luminous resin adhesive and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A method for preparing an ultra-long afterglow energy-storage luminescent resin glue, specifically comprising the following steps:

[0031] 1) Use a mixing tank that does not contain metal substances, the stirring speed is not lower than 1500 rpm, the stirring temperature in summer is not higher than 60°C, and the stirring temperature in winter is not lower than 30°C;

[0032] 2) In parts by weight, add 50 parts of acrylic resin glue and 2.8 parts of polyamine wax into the stirring tank, wherein the viscosity of the acrylic resin glue is 2000-5000 poises, and then add 20 parts of luminescent powder, the particle size of which is 100- 300 mesh, after stirring for 15 minutes, add 0.6 parts of defoamer, 0.2 parts of drier, 0.8 parts of ultraviolet absorber, 3.2 parts of coupling agent, after stirring for 10 minutes, add 10:1 curing agent (the ratio of acrylic glue is 10 1. The ratio of curing agent is 1) Stir evenly for 15 minutes to get luminescent resin glue.

Embodiment 2

[0034] A method for preparing an ultra-long afterglow energy-storage luminescent resin glue, specifically comprising the following steps:

[0035] 1) Use a stirring tank that does not contain metal substances, the stirring speed is not lower than 1500 rpm, and the stirring temperature in winter is 35°C;

[0036] 2) In parts by weight, add 60 parts of acrylic resin glue and 4.2 parts of polyamine wax into the mixing tank, wherein the viscosity of the acrylic resin glue is 2000-3000 poises, and then add 30 parts of luminescent powder, the particle size of which is 100- 300 mesh, after stirring for 15 minutes, add 0.9 parts of defoamer, 0.3 parts of drier, 1.2 parts of ultraviolet absorber, 4.8 parts of coupling agent, after stirring for 10 minutes, add 10:1 curing agent (the ratio of acrylic glue is 10 1. The ratio of curing agent is 1) Stir evenly for 15 minutes to get luminescent resin glue.

Embodiment 3

[0038] A method for preparing an ultra-long afterglow energy-storage luminescent resin glue, specifically comprising the following steps:

[0039] 1) Use a stirring tank that does not contain metal substances, the stirring speed is not lower than 1500 rpm, and the stirring temperature in summer is 50°C;

[0040] 2) In parts by weight, add 70 parts of acrylic resin glue and 4.2 parts of polyamine wax into the stirring tank, wherein the viscosity of the acrylic resin glue is 4000-5000 poises, and then add 40 parts of luminescent powder, the particle size of which is 100- 300 mesh, after stirring for 15 minutes, add 1.2 parts of defoamer, 1.05 parts of drier, 1.2 parts of ultraviolet absorber, 4.8 parts of coupling agent, after stirring for 10 minutes, add 10:1 curing agent (the ratio of acrylic glue is 10 1. The ratio of curing agent is 1) Stir evenly for 15 minutes to get luminescent resin glue.

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Abstract

The invention discloses an ultra-long-afterglow energy-storing luminous resin adhesive and a preparation method thereof, and belongs to the field of luminous resin adhesives. The resin adhesive comprises 20-40 parts of luminous powder, 50-70 parts of an acrylic resin adhesive, and 5-15 parts of an aid which does not contain heavy metal compounds, wherein the grain size of the luminous powder is 100-300 meshes; the aid is prepared from an antifoaming agent, a drier, an ultraviolet light absorber, a coupling agent and polyamine wax according to a ratio of (0.3-0.5):(0.1-0.35):0.4:1.6:1.4. The ultra-long-afterglow energy-storing luminous resin adhesive has the advantages that the decoration performance is good, energy is saved, the adhesive is non-toxic and non-radioactive, the long-term luminous performance is excellent, the luminance is adjustable, the storage stability is good, the cost is low, and the economic and social benefits are remarkable. All technical performance indexes of the ultra-long-afterglow energy-storing luminous resin adhesive are superior to other energy-storing luminous coating, and the ultra-long-afterglow energy-storing luminous resin adhesive has a wide promotion prospect.

Description

technical field [0001] The invention relates to an ultra-long afterglow energy storage luminescent resin glue and a preparation method thereof, belonging to the field of luminescent resin glue. Background technique [0002] In order to prolong the afterglow time, the traditional luminescent coatings that use sulfide as the luminescent material often add radioactive elements, which are harmful to the human body and have a short luminescent life. [0003] Luminescent resin glue is made of resin glue, various fillers and additives in a certain proportion through special processing technology. Luminescent resin glue is a kind of luminescent material that absorbs the excitation light energy and stores it, and then slowly releases the stored energy in the form of light energy after the light excitation stops, and can last for several or even ten hours. This process of absorption-luminescence-storage-re-luminescence, which can be repeated indefinitely, is similar to the repeated p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D133/00C09D5/22C09D7/12
CPCC09D133/00C09D5/22C09D7/40C09D7/65C08L79/02
Inventor 刘海泉
Owner 刘海泉
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