Preparation method of graphene oxide/bioenzyme nanometer composite material
A nano-composite material and technology of composite materials are applied in the preparation of formaldehyde-degrading nano-composite materials and in the field of anti-haze, which can solve the problems of poor anti-haze effect and weak ability to degrade formaldehyde, and achieve stable and lasting effects and strong ability to degrade formaldehyde. , the effect of low cost
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[0017] first step
[0018] Preparation of biological enzyme: Weigh 10g of soybean peptone and dissolve it in 100ml of deionized water, stir for 12 hours, place the solution in an oil bath, raise the temperature to 80-85°C, and add an appropriate amount of acetic acid, citric acid or formic acid to make the solution The pH value of the solution is 3~5, stirred and hydrolyzed, and the hydrolysis time is 8 hours. After the reaction is completed, the solution is cooled and filtered with a filter membrane to obtain the biological enzyme, which is put into a brown bottle for later use.
[0019] second step
[0020] Preparation of sponge-like three-dimensional graphene oxide:
[0021] (1) Graphene oxide was synthesized by the modified Hummers method. The oxidation process is divided into two stages: the first is the pre-oxidation stage, graphite (3 g), H 2 SO 4 (40 mL, 98%), K 2 S 2 o 8 (2.5 g) and P 2 o 5 (2.5 g) was added to the beaker one by one and stirred, and the oi...
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