Chrysanthemum morifolium essential oil preparation method for improving aroma quality by enzymatic aroma enhancement and application
A technology of volatile oil and Chrysanthemum chrysanthemum, applied in the field of tobacco additives, to achieve the effects of overcoming irritation, improving aroma quality, and easy operation of process conditions
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Embodiment 1
[0019] A preparation method of Chrysanthemum chrysanthemum volatile oil that enhances fragrance by enzymatic enhancement, comprising the following steps:
[0020] (1) Mix Hangbai chrysanthemum with water at a mass ratio of 1:25, adjust the pH to 4, add food-grade 95% ethanol with 3% of the total mass of the mixture, equilibrate at 35°C for 10 minutes, add the mass ratio of Hangbai chrysanthemum 0.1% compound enzyme (, mix well and keep stirring, incubate at 35°C for 12 hours, the compound enzyme is composed of β-glucosidase and flavor protease in a mass ratio of 1:1;
[0021] (2) The volatile oil was extracted by steam distillation for 5 hours, and the obtained yellow oily substance was the volatile oil of Chrysanthemum chrysanthemum that was enzymatically enhanced to improve the aroma quality.
[0022] The β-glucosidase is food grade, and the enzyme activity is 10000u / g.
[0023] The flavor protease is food grade, and the enzyme activity is 30,000 u / g.
[0024] The ethanol ...
Embodiment 2
[0028] A preparation method of Chrysanthemum chrysanthemum volatile oil that enhances fragrance by enzymatic enhancement, comprising the following steps:
[0029] (1) Mix the white chrysanthemum powder with water at a mass ratio of 1:35, adjust the pH to 5.2, add food-grade 95% ethanol with a total mass of 4.5% of the mixture, balance at 40°C for 20 minutes, and add the white chrysanthemum powder The compound enzyme with a mass ratio of 0.3% is mixed evenly, stirred continuously, and incubated at 40°C for 18 hours. The compound enzyme is composed of β-glucosidase and flavor protease at a mass ratio of 0.5:1;
[0030] (2) volatile oil was extracted by steam distillation for 6 hours, and the yellow oily matter of gained was the volatile oil of Chrysanthemum chrysanthemum enzymatically produced;
[0031] The β-glucosidase is food grade, and the enzyme activity is 5000u / g.
[0032] The flavor protease is food grade, and the enzyme activity is 20,000 u / g.
[0033] The above-menti...
Embodiment 3
[0035] A preparation method of Chrysanthemum chrysanthemum volatile oil that enhances fragrance by enzymatic enhancement, comprising the following steps:
[0036] (1) Mix the white chrysanthemum powder and water at a mass ratio of 1:45, adjust the pH to 6, add food-grade 95% ethanol with 6% of the total mass of the mixture, balance at 48°C for 30 minutes, and add the white chrysanthemum powder The compound enzyme (beta-glucosidase, flavor protease) with a mass ratio of 0.3% was mixed evenly, kept stirring, and incubated at 48°C for 32 hours. : 0.5 composition;
[0037] (2) Steam distillation 12 hours extracts volatile oil, and gained yellow oily matter is the volatile oil of enzymatically producing fragrant Chrysanthemum chrysanthemum;
[0038] The β-glucosidase is food grade, and the enzyme activity is 1000u / g.
[0039] The flavor protease is food grade, and the enzyme activity is 10,000 u / g.
[0040] The above-mentioned chrysanthemum chrysanthemum volatile oil is flavored...
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