CdS (cadmium sulfide)/CdTe (cadmium telluride) heterojunction nanorod and preparation method thereof
A nanorod and heterojunction technology, applied in the field of nanomaterials, can solve problems such as photoelectric effect and electroluminescent devices that have not yet appeared, and achieve the effect of fast photon transport
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[0022] Below in conjunction with embodiment the present invention will be further described.
[0023] 1. Dissolve 0.128 g of CdO powder and 0.668 g of n-octadecanyl phosphate in 2 g of tri-n-octylphosphine oxide (TOPO);
[0024] 2. Degas at 150°C for 30 minutes, then heat to 370°C under nitrogen atmosphere to generate Cd-ODPA complex;
[0025] 3. Dissolve 16 mg of S in 1.5 ml of trioctyl (TOP), mix well, and quickly inject it into the product of step 2 at 370°C;
[0026] 4. Stir at 330°C for 20 minutes;
[0027] 5. Cool the reaction mixture to 250°C;
[0028] 6. Dissolve 20 mg of tellurium in 1 ml of TOP; then slowly add to the mixture from step 5;
[0029] 7. After 10 minutes, the reaction mixture was cooled to room temperature, and the obtained cadmium sulfide / cadmium telluride nanorods were precipitated and then dissolved in 4 ml of chloroform;
[0030] 8. Mix 6 ml of octadecene, 1.13 g of oleic acid and 0.184 g of zinc acetate, degas at 150°C for 30 minutes, then stir ...
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