Preparation method for bumblebee peptidoglycan recognition protein
A technology for identifying proteins and peptidoglycan, applied in the field of molecular biology, can solve problems such as hindering the research and application of new antibacterial and immune drugs of bumblebees, and achieve the effects of small protein damage, mild operation process, and simple and fast method.
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[0023] The present invention relates to the establishment of a peptidoglycan recognition protein PGRP-SA in vitro expression, folding renaturation and multi-step purification method; in particular, it relates to the important recognition molecule PGRP-SA in the innate antibacterial immune response of wild plants and agricultural crops. In vitro preparation method of SA protein.
[0024] A preparation method for bumblebee peptidoglycan recognition protein, comprising the steps of:
[0025] 1), connecting the gene fragment of bumble bee PGRP-SA to an expression vector and transforming it into Escherichia coli for expression, collecting the expressed inclusion body protein;
[0026] 2), after washing the inclusion body protein, adding a protein denaturant to dissolve it, and then performing refolding treatment with a refolding solution;
[0027] 3) After the protein is concentrated, it is sequentially eluted and purified through a molecular sieve column and an anion exchange col...
Embodiment 1
[0086] The sequence of the protein expressed in this embodiment is obtained by the following methods:
[0087] The total RNA of Bombus flamingo was extracted by conventional methods, and then reverse-transcribed to obtain cDNA, and the cDNA was used as a template to amplify the bumblebee PGRP-SA gene. The gene fragment size is about 500bp, and the sequence is shown in SEQ ID NO:1.
[0088] The upstream primer used in the amplification is shown in SEQ ID NO:2, and the downstream primer is shown in SEQ ID NO:3.
[0089] Amplification was carried out with LATaq enzyme from Takara Company, and the amplification conditions were as follows:
[0090] ① Denaturation at 95°C for 5 minutes;
[0091] ② Denaturation at 95°C for 30s;
[0092] ③Annealing at 58°C for 1min;
[0093] ④ Extend at 72°C for 30s;
[0094] Repeat ②~④30 times;
[0095] ⑤ Extend at 72°C for 10 minutes;
[0096] ⑥ Keep warm at 4°C.
[0097] The above gene fragments were connected to PET21a+ vector (endonuclease...
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