Unlock instant, AI-driven research and patent intelligence for your innovation.

Low-surface tension acid etching solution for AMOLED (Active Matrix/Organic Light Emitting Diode) and preparation process thereof

A technology of low surface tension, acid etching solution, applied in the field of etching solution, can solve the problems of weak permeability, high production cost, complex components, etc., and achieve the effect of reducing surface tension, low production cost, and increasing permeability

Inactive Publication Date: 2017-09-15
HEFEI HUIKE PRECISION DIE CO LTD
View PDF5 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing etching solution has complex components. Compared with the main components of nitric acid and ammonium fluoride, the amount of surfactant activity is relatively large, and the production cost is high; in addition, when the concentration of nitric acid and ammonium fluoride in the etching solution is high, generally non-ionic Surfactants are difficult to dissolve, cannot adjust the surface tension of the etching solution, and have relatively weak permeability, making it difficult to etch into very small pores

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] Embodiment 1 A kind of low surface tension acidic etchant for AMOLED, it is made up of the raw material of following percentage by weight: nitric acid 23%, hydrochloric acid 11%, acetic acid 7%, inorganic salt chloride 1.2%, ammonium fluoride 8.5%, surface Active agent 11.2%, additive 5% and deionized water.

[0021] The surfactant is one or more mixtures of N-alkyl glucamides, polyisobutene / maleic anhydride derivatives, and N-aryloxy polyhydroxy-fatty acid amides.

[0022] The inorganic salt chloride is potassium chloride, and the purity of the potassium chloride is higher than 95%.

[0023] The additives are polyethylene glycol monoperfluorononenyl ether, polyglycerol perfluorohexylsulfonate, octylamine, polyglycerol perfluorononenyl ether, polyethylene glycol perfluorononenyl methyl ether, One or more of polyethylene glycol perfluorohexylsulfonate.

[0024] The deionized water has a resistivity of at least 22 megohms at 25°C.

[0025] A kind of preparation technol...

Embodiment 2

[0033] Embodiment 2 A kind of low surface tension acidic etchant for AMOLED, it is made up of the raw material of following percentage by weight: nitric acid 25%, hydrochloric acid 13%, acetic acid 9%, inorganic salt chloride 1.8%, ammonium fluoride 9.4%, surface Active agent 14.5%, additives 8% and deionized water.

[0034] The surfactant is one or more mixtures of N-alkyl glucamides, polyisobutene / maleic anhydride derivatives, and N-aryloxy polyhydroxy-fatty acid amides.

[0035] The inorganic salt chloride is potassium chloride, and the purity of the potassium chloride is higher than 95%.

[0036] The additives are polyethylene glycol monoperfluorononenyl ether, polyglycerol perfluorohexylsulfonate, octylamine, polyglycerol perfluorononenyl ether, polyethylene glycol perfluorononenyl methyl ether, One or more of polyethylene glycol perfluorohexylsulfonate.

[0037] The deionized water has a resistivity of at least 22 megohms at 25°C.

[0038] A kind of preparation techno...

Embodiment 3

[0046] Embodiment 3 A kind of low surface tension acidic etchant for AMOLED, it is made up of the raw material of following percentage by weight: nitric acid 24%, hydrochloric acid 12%, acetic acid 8%, inorganic salt chloride 1.5%, ammonium fluoride 8.8%, surface Active agent 12.6%, additive 7% and deionized water.

[0047] The surfactant is one or more mixtures of N-alkyl glucamides, polyisobutene / maleic anhydride derivatives, and N-aryloxy polyhydroxy-fatty acid amides.

[0048] The inorganic salt chloride is potassium chloride, and the purity of the potassium chloride is higher than 95%.

[0049] The additives are polyethylene glycol monoperfluorononenyl ether, polyglycerol perfluorohexylsulfonate, octylamine, polyglycerol perfluorononenyl ether, polyethylene glycol perfluorononenyl methyl ether, One or more of polyethylene glycol perfluorohexylsulfonate.

[0050] The deionized water has a resistivity of at least 22 megohms at 25°C.

[0051] A kind of preparation technol...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
pore sizeaaaaaaaaaa
purityaaaaaaaaaa
Login to View More

Abstract

The invention discloses a low-surface tension acid etching solution for an AMOLED (Active Matrix / Organic Light Emitting Diode). The low-surface tension acid etching solution is prepared from the following raw materials according to weight percent: 23 to 25% of nitric acid, 11 to 13% of hydrochloric acid, 7 to 9% of acetic acid, 1.2 to 1.8% of inorganic salt chloride, 8.5 to 9.4% of ammonium fluoride, 11.2 to 14.5% of surfactant, 5 to 8% of additives and deionized water. Compared with the prior art, the ammonium fluoride and appropriate additives are added to the etching solution, and any metal ion or negative ion is not introduced, so that no residue exists on the surface of an oxidation layer after etching, lower surface tension can be applied to the etching solution, and the permeability of the etching solution is increased; the surfactant has high surface activity and hydrophobic and oleophobic properties, so that compared with the same amount of other surfactants, the surface tension of the solution can be greatly reduced, therefore, the consumption is low, and the production cost is low.

Description

technical field [0001] The invention relates to the technical field of etching solution, in particular to an acidic etching solution with low surface tension for AMOLED and a preparation process thereof. Background technique [0002] There are a large number of thin films and thin layers on the AMOLED substrate, so in order to prevent undesired electrical short circuits between them, it is preferable to evenly incline the cut-off side of the etched substrate, that is, the etching profile, and the lower part is wider than the upper part, forming a blunt cone. shape. This is because the difference in height between the formed two or more thin film layers decreases when the etching profile is in the blunt tapered shape. Etching methods include dry etching using gas and wet etching using etching liquid. Although wet etching has disadvantages, the equipment investment cost required for the process is low, and the etching environment does not need to be maintained in a high vacuu...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C23F1/16
CPCC23F1/16
Inventor 白航空
Owner HEFEI HUIKE PRECISION DIE CO LTD