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Processing process for obtaining nanosheet composite material through ultrasonic rolling

A composite material and processing technology, applied in nanotechnology, metal processing equipment, transportation and packaging, etc., can solve problems such as difficulty in uniform dispersion and easy agglomeration of nanoparticles, and achieve the effect of expanding the scope of application and improving the combination.

Active Publication Date: 2017-11-07
NANJING UNIV OF AERONAUTICS & ASTRONAUTICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this method has certain defects. Nanoparticles are easy to agglomerate, and it is difficult to achieve uniform dispersion in the polymer during blending.
In the chemical method, based on the chemical principle, the nanocomposite material is designed, synthesized and prepared from the chemical composition, structure, properties, chemical reaction, compounding principle and its changing law of the nanocomposite material. Usually, different powder raw materials are mixed, And using conditions such as high temperature, high pressure and vacuum to prepare nanosheet composite materials, the process yield is high and suitable for large-scale production, but high temperature and high pressure conditions sometimes have a negative impact on the characteristics of some sensitive nanomaterials, so the existing nanosheet composite materials Processing technology has certain limitations

Method used

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  • Processing process for obtaining nanosheet composite material through ultrasonic rolling
  • Processing process for obtaining nanosheet composite material through ultrasonic rolling

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] The micro-scale flexible ultrasonic tool 1 is a ring surrounded by glass fibers with a diameter of 10 microns. The diameter of the ring is 2 mm. The upper end of the micro-scale flexible ultrasonic tool 1 is pasted on the center of the left end of the vibration transmission rod 2. The rod 2 is made of stainless steel with a diameter of 1.4mm. The vibration transmission rod 2 is welded on the radiation surface of the ultrasonic transducer 3, and the ultrasonic transducer 3 can also be a piezoelectric sheet. The micro-nanoscale material A is a silver nanowire with a diameter of 300 nanometers and a length of 30 micrometers. Nanoscale material B is zinc oxide particles with a diameter of 100 nanometers. When the micro-scale flexible ultrasonic tool 1 is used as a driving part, when it is driven by an external sinusoidal alternating current signal, due to the inverse piezoelectric effect, the piezoelectric sheet is periodically deformed.

[0017] The specific experimental ...

Embodiment 2

[0019] The micro-scale flexible ultrasonic tool 1 is a ring surrounded by carbon fibers with a diameter of 5 microns. The diameter of the ring is 1.5 mm. The upper end point of the micro-scale flexible ultrasonic tool 1 is pasted on the center of the left end of the vibration transmission rod 2. 2 is stainless steel with a diameter of 1.4 mm. The vibration transmission rod 2 is welded on the radiation surface of the ultrasonic transducer 3. The ultrasonic transducer 3 can also be a piezoelectric sheet. The distance between adjacent interdigital electrodes on the IDT electrode substrate is 5 Micron, the electrode width is 5 microns. The micro-nanoscale material A is a silver nanowire with a diameter of 300 nanometers and a length of 30 micrometers. Nanoscale material B is zinc oxide particles with a diameter of 100 nanometers. When the micro-scale flexible ultrasonic tool 1 is used as a driving part, when it is driven by an external sinusoidal alternating current signal, due t...

Embodiment 3

[0022] The micro-scale flexible ultrasonic tool 1 is a ring surrounded by copper fibers with a diameter of 40 microns. The diameter of the ring is 2 mm. The upper end point of the micro-scale flexible ultrasonic tool 1 is attached to the center of the left end of the vibration transmission rod 2. The rod 2 is made of stainless steel with a diameter of 1.4mm. The vibration transmission rod 2 is welded on the radiation surface of the ultrasonic transducer 3, and the ultrasonic transducer 3 can also be a piezoelectric sheet. The micro-nanoscale material A is a silver nanowire with a diameter of 300 nanometers and a length of 30 micrometers. Nanoscale material B is zinc oxide particles with a diameter of 100 nanometers. When the micro-scale flexible ultrasonic tool 1 is used as a driving part, when it is driven by an external sinusoidal alternating current signal, due to the inverse piezoelectric effect, the piezoelectric sheet is periodically deformed.

[0023] The specific expe...

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Abstract

The invention discloses a processing process for obtaining a nanosheet composite material through ultrasonic rolling, and relates to the field of micro-nano manufacturing, and the processing process can be performed at the normal temperature and under normal pressure. The processing process comprises the following steps: rolling a micro-nano-scale material A by a flexible ultrasonic tool 1 with micro scale, and enabling the micro-nano-scale material A to become a sheet-shaped structure; adding a nano-scale material B onto the sheet-shaped micro-nano-scale material A, and performing re-rolling by the ultrasonic tool 1, thereby obtaining the nanosheet composite material which is co-formed by a substrate material formed by the sheet-shaped micro-nano-scale material A and a surface modifying material formed by the nano-scale material B. The processing process is performed at the normal temperature and under normal pressure, does not need any chemical reaction, and is free of requirements on ductility of the modifying material B. A rolling process in the process further can be directly performed on a base plate with an IDT electrode, and bonding between the nanosheet composite material and the base plate electrode is improved while the nanosheet composite material is processed.

Description

technical field [0001] The invention belongs to the field of micro-nano manufacturing, and in particular relates to a processing technology of nanosheet composite material by ultrasonic rolling. Background technique [0002] Driven by basic research and application prospects, people have developed a series of methods for preparing silver nanosheets, such as light-induced chemical reduction method, rapid reduction precipitation method, soft template method and sonochemical method, thermal deposition method, etc. These methods generally complete the preparation of nanosheets by means of chemical reaction or heat treatment, and the shape of the prepared nanosheets is generally triangular. The existing preparation methods of nanocomposites are divided into physical methods and chemical methods, with chemical methods being the most common. The blending method belongs to the physical method, which is to directly add nano-powder to the polymer matrix. It is a commonly used relativ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F1/00B82Y40/00
CPCB82Y40/00B22F1/0551B22F1/054B22F1/14
Inventor 胡俊辉王旭
Owner NANJING UNIV OF AERONAUTICS & ASTRONAUTICS
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