Use of chondroitin sulfate for expanding cik cells, preparing cik cell expansion reagents and coating culture vessels
A chondroitin sulfate, cell culture technology, applied in chondroitin sulfate, preparation of CIK cell expansion reagents and coated culture vessels, CIK cells, expansion of CIK cells field, can solve problems such as the application of chondroitin sulfate has not yet been seen, achieve The effect of improving tumoricidal activity and increasing expansion activity
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Embodiment 1
[0023] Example 1: Preparation and Characterization of High Molecular Weight Chondroitin Sulfate
[0024] 1. Preparation of chondroitin sulfate derived from chicken breast cartilage:
[0025] After the fascia is removed from the fresh chicken breast cartilage, it is dried at 55°C and crushed through a 40-mesh sieve to obtain cartilage powder. The cartilage powder is dissolved in a papain solution with a mass volume percentage of 8% (5g cartilage powder corresponds to 1L solution). Extract with papain at 55°C for 6 hours to obtain the enzyme extract, add trichloroacetic acid to a volume concentration of 10%, react for 1.5 hours, remove protein with trichloroacetic acid, and then filter and centrifuge at 4000-5000rpm for 8-12min. After the supernatant is concentrated, it is precipitated with ethanol (the volume of 95% ethanol is 5 times the volume of the supernatant), and the precipitate is collected by centrifugation at 4000-5000 rpm for 8-12 min. After the precipitation was re...
preparation example 1
[0027] Preparation Example 1: Dissolve the above-mentioned chondroitin sulfate raw materials with deionized water to prepare a chondroitin sulfate solution with a mass volume concentration of 3%, add malic acid to a concentration of 0.2mol / L, stir and degrade at 70°C for 10h, and use a sufficient amount of Calcium carbonate powder to terminate the reaction, adjust the pH to 6.5, add ethanol for precipitation (the volume of 95% ethanol is 8 times the volume of the degradation solution), centrifuge and dry at 55°C to obtain the high molecular weight chondroitin sulfate.
preparation example 2
[0028] Preparation Example 2: Dissolve the above-mentioned chondroitin sulfate raw materials with deionized water to prepare a chondroitin sulfate solution with a mass volume concentration of 2%, add malic acid to a concentration of 0.1mol / L, stir and degrade at 60°C for 12h, and use a sufficient amount of Calcium carbonate powder to terminate the reaction, adjust the pH to 6.5, add ethanol for precipitation (the volume of 95% ethanol is 8 times the volume of the degradation solution), centrifuge and dry at 55°C to obtain the high molecular weight chondroitin sulfate.
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