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Method for improving welding performance of iron-nickel base alloy through grain boundary sawtooth treatment

An iron-nickel-based alloy and weldability technology, which is applied in the field of iron-nickel-based alloy welding, can solve problems such as liquefaction cracks at the grain boundary in the affected area of ​​the joint, poor weldability, etc., and achieve the effect of improving weldability and quality

Active Publication Date: 2017-12-15
INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] The purpose of the present invention is to provide a method for improving the weldability of iron-nickel-based alloys (J75) through grain boundary zigzag treatment, so as to solve the problems of poor weldability of existing iron-nickel-based alloys and easy formation of grain boundary liquefaction cracks in heat-affected zones of joints question

Method used

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  • Method for improving welding performance of iron-nickel base alloy through grain boundary sawtooth treatment
  • Method for improving welding performance of iron-nickel base alloy through grain boundary sawtooth treatment
  • Method for improving welding performance of iron-nickel base alloy through grain boundary sawtooth treatment

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Embodiment 1

[0029] In this embodiment, the grain boundary zigzag treatment and vacuum electron beam welding of a J75 alloy plate with a thickness of 12.0 mm are carried out. The specific implementation process is as follows:

[0030] 1. The J75 alloy sheet is a hot-rolled sheet, and the chemical composition of the hot-rolled sheet meets the requirements of GJB 5724-2006 "Specification for Hydrogen-Resistant Steel Bars". The J75 alloy plate is placed in a vacuum heat treatment furnace and kept at 960-1030°C (1000°C in this embodiment) for 10-20min (18min in this embodiment);

[0031] 2. Cool the J75 alloy plate after heat preservation treatment in step 1 to 840-860°C (850°C in this embodiment) with the furnace, and control the cooling rate to 2-5°C / min (3°C / min in this embodiment) ;

[0032] 3. Insulate the J75 alloy plate after controlled cooling in step 2 at 840-860°C (850°C in this embodiment) for 1-3h (1.5h in this embodiment);

[0033] 4. Cool the J75 alloy plate after the heat pres...

Embodiment 2

[0042] In this embodiment, the grain boundary zigzag treatment and vacuum electron beam welding of a J75 alloy plate with a thickness of 3.0 mm are performed. The difference from Example 1 is that the thickness of the welded J75 alloy plate is 3.0mm, and the sawtooth treatment and welding process parameters are adjusted accordingly.

[0043] A 3.0mm thick J75 alloy hot-rolled plate with the same chemical composition as in Example 1 was used, placed in a vacuum heat treatment furnace, kept at 980°C for 12min, then cooled to 850°C at a cooling rate of 3°C / min and kept for 1h; After the end, the J75 alloy plate was cooled to 740°C at a cooling rate of 8°C / min, and aged at this temperature for 8h, and then placed in air to cool to room temperature. The sawtoothed J75 alloy plate is subjected to vacuum electron beam welding. The welding adopts a single-cycle welding method. The welding process parameters are: accelerating voltage 50KV, welding current 14mA, focusing current 2.325A,...

Embodiment 3

[0048] In this embodiment, the grain boundary zigzag treatment and vacuum electron beam welding of a J75 alloy plate with a thickness of 15.0 mm are performed. The difference from Example 1 is that the thickness of the welded J75 alloy plate is 15.0 mm, and the sawtooth treatment and welding process parameters are adjusted accordingly.

[0049] A 15.0mm thick J75 alloy hot-rolled plate with the same chemical composition as in Example 1 was used, placed in a vacuum heat treatment furnace, kept at 1020°C for 20min, then cooled to 850°C at a cooling rate of 3°C / min and kept for 2h; After the end, the J75 alloy plate was cooled to 740°C at a cooling rate of 8°C / min, and aged at this temperature for 12 hours, and then placed in air to cool to room temperature. The sawtoothed J75 alloy plate is subjected to vacuum electron beam welding. The welding adopts a single-cycle welding method. The welding process parameters are: acceleration voltage 60KV, welding current 29mA, focusing curr...

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Abstract

The invention relates to the field of iron-nickel base alloy welding, in particular to a method for improving welding performance of an iron-nickel base precipitation strengthening austenite alloy (J75) through grain boundary sawtooth treatment. The problems that the welding performance of an existing iron-nickel base alloy is not good, and connector heat affected zone grain boundary liquidation cracks are likely to be formed are solved. The controlled cooling heat treatment method is adopted, high-energy grain boundary sawtooth development is promoted, the distribution state of the boron element and the titanium element segregated at the high-energy grain boundary position is changed, resistance for grain boundary liquidation crack forming is increased, and the welding performance of the alloy is improved. Specifically, the technology process of high-temperature and short-time heat preservation treatment, slow cooling (cooling speed control) treatment, medium-temperature heat preservation treatment, slow cooling (cooling speed control) treatment, aging treatment, air cooling and vacuum electronic beam welding is adopted. The strength of a welding connector of the iron-nickel base alloy treated through the method is 980 MPa or above and even reaches 1,040 MPa or above, the strength coefficient of the welding connector and the base metal can reach 0.9 or above, the impact toughness alpha<kU> of the connector is 1,500 KJ / m<2> or above and even reaches 1,520 KJ / m<2> or above.

Description

technical field [0001] The invention relates to the field of iron-nickel-based alloy welding, in particular to a method for improving the weldability of iron-nickel-based precipitation-strengthened austenitic alloy (J75) through serrated grain boundary treatment. Background technique [0002] With the development of high-tech fields such as aviation, aerospace and nuclear energy utilization, higher requirements are placed on the materials and devices used. Due to the low strength, single-phase austenitic stainless steels such as 304, 310, 316 and 316L no longer meet the requirements of various fields. Precipitation-strengthened austenitic alloys are developed on the basis of single-phase austenitic alloys through the alloying of elements such as Ti and Al. This type of alloy is used in the aging state and strengthened by precipitation with a coherent relationship with the matrix. Phase γ′-Ni 3 (Al,Ti) to obtain high strength and good plasticity matching. The high strength...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B23K15/06B23K37/00
CPCB23K15/06B23K37/00
Inventor 赵明久戎利建闫德胜姜海昌胡小锋宋元元陈胜虎王本贤
Owner INST OF METAL RESEARCH - CHINESE ACAD OF SCI