Preparation method of nanoscale lophiiformes fish bone meal

A technology of anglerfish and fish bone meal, which is applied in food science and other fields, can solve the problems of food safety hazards of fish bone meal, high hardness of fish bone meal particles, and restrictions on the application of fish bone meal, and achieve the effect of improving utilization value, small pore size, and simple process

Inactive Publication Date: 2018-02-23
ZHEJIANG OCEAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In the existing technology of utilizing fish bones, anglerfish bones are usually prepared into fish bone meal. The commonly used preparation methods include physical and chemical methods, but chemical methods are easy to cause secondary chemical reactions, which may bring food safety hazards to fish bone meal. The physical method generally refers to the change of the physical form of the grinding, no foreign substances are introduced, and the safety is high. However, the particle size of the fish bone meal prepared by grinding is large, usually in the micron or even millimeter level, and the particle size distribution is uneven, which limits the use of fish bone meal. Applications in food, medicine and other fields
Chinese patent 2015110072585, patent name fish bone powder and its preparation method, application date: December 30, 2015, discloses a preparation method of fish bone powder that is steamed, enzymatically hydrolyzed, baked and pulverized, through chemical and physical methods combined to prepare fish bone meal, but the particle size of the fish bone meal prepared by this method is still large, the particle size distribution is uneven, and the particle hardness of the fish bone meal is relatively large

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] A preparation method of nano-scale anglerfish bone powder, comprising the following steps:

[0036] (1) Remove the meat scraps on the discarded anglerfish bones, cut them into 1cm-long fragments, and clean the surface stains to obtain the anglerfish bones;

[0037] (2) Soak the anglerfish bone in an aqueous solution of endopeptidase with a mass concentration of 1% at 50° C. for enzymolysis for 2 hours. The preferred endopeptidase is alkaline protease, and the mass ratio of the anglerfish bone to the aqueous solution of endopeptidase is 1 :1.2;

[0038] (3) Cook the bones of anglerfish at 130° C. for 10 minutes under a high-pressure environment of 200 MPa to soften them;

[0039] (4) the anglerfish bone is dried and pulverized, and then sieved through a 120-mesh sieve to obtain coarse fish bone powder;

[0040] (5) Put the coarse fish bone meal in 4mol / LZnCl 2 Soak in the solution overnight, take it out and dry at 70°C until the water content is 30%;

[0041] (6) Ext...

Embodiment 2

[0044] A preparation method of nano-scale anglerfish bone powder, comprising the following steps:

[0045] (1) remove the meat scraps on the discarded anglerfish bones, and cut into 1.5cm long fragments, clean the surface stains to obtain the anglerfish bones;

[0046] (2) Soak the anglerfish bone in an aqueous solution of endopeptidase with a mass concentration of 1.5% at 40°C for 3 hours for enzymatic hydrolysis. The preferred endopeptidase is alkaline protease, and the mass ratio of the anglerfish bone to the aqueous solution of endopeptidase is 1 :1.4;

[0047] (3) Cook the bones of the anglerfish at 120° C. for 40 minutes in a high-pressure environment of 300 MPa to soften them;

[0048] (4) the anglerfish bone is dried and pulverized, and then sieved through a 120-mesh sieve to obtain coarse fish bone meal;

[0049] (5) Put the coarse fish bone meal in 5mol / LZnCl 2 Soak in the solution overnight, take it out and dry at 70°C until the water content is 40%;

[0050] (6...

Embodiment 3

[0053] A preparation method of nano-scale anglerfish bone powder, comprising the following steps:

[0054] (1) remove the meat shavings on the discarded anglerfish bones, and cut into 2cm long fragments, clean the surface stains to obtain the anglerfish bones;

[0055] (2) Soak the anglerfish bone in an aqueous solution of endopeptidase with a mass concentration of 2% at 50°C for 3 hours for enzymatic hydrolysis, the preferred endopeptidase is alkaline protease, and the mass ratio of the anglerfish bone to the aqueous solution of endopeptidase is 1 :1.5;

[0056] (3) Cook the bones of the anglerfish at 150° C. for 30 minutes under a high-pressure environment of 250 MPa to soften them;

[0057](4) the anglerfish bone is dried and pulverized, and then sieved through a 120-mesh sieve to obtain coarse fish bone meal;

[0058] (5) Put the coarse fish bone meal in 6mol / LZnCl 2 Soak in the solution overnight, take it out and dry at 70°C until the water content is 50%;

[0059] (6...

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PUM

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Abstract

The invention relates to a preparation method of nano-scale anglerfish bone powder, comprising the following steps: removing meat scraps on the discarded anglerfish bone, cutting into pieces, cleaning surface stains, soaking in an aqueous solution of endopeptidase for enzymolysis, Cook and soften in a high-pressure environment, crush and sieve, soak in ZnCl2 solution overnight, take it out and dry it, and thermoplastically extrude fishbone powder with different water contents, and then get nano-scale anglerfish after treatment with atmospheric plasma radio frequency RF Fish bone powder, the particle size range of the angler fish bone powder prepared by the method of the present invention is in the nanometer level, the pore size is small, and the particle size distribution is uniform. it is good.

Description

technical field [0001] The invention relates to a preparation method of nano-scale anglerfish bone powder, belonging to the technical field of fish processing. Background technique [0002] Anglerfish, commonly known as toad fish and sea toad, is a cold-temperate bottom fish widely distributed in the eastern waters of my country (the northern part of the East China Sea, the Yellow Sea and the Bohai Sea). It has extremely high nutritional, edible and medicinal values. popular. In recent years, the demand for export has been strong, and the processing volume of anglerfish in my country has continued to increase, and both output and price have increased significantly. A large number of anglerfish bones produced after industrial processing are discarded as leftovers, or only used as fertilizer or feed, with low added value. [0003] Angler fish bones are rich in nutrients such as calcium, iron, zinc, magnesium, phosphorus, collagen, and chondroitin. If these ingredients are not...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L17/00
CPCA23L17/70
Inventor 王亚宁宋文东纪丽丽郭健蔡璐应知伟林艺鸿
Owner ZHEJIANG OCEAN UNIV
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